Full Disclosure Wipes For Disclosing The Presence Of Lead Cat No. 550 001 And 002 Operating Instruction Form 40091 PDF Docum

User Manual: 40091

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Operating Instructions

863 Valley View Road, Eighty Four, PA 15330 USA

Tel: 724-941-9701 Fax: 724-941-1369 e-mail: skctech@skcinc.com

Wipes for Disclosing the Presence of Lead

The Full Disclosure® Kit includes wipes (conform to ASTM E1792), spray bo le of acetic

acid, spray bo les of deionized water, vials of Disclosing Powder, waxed paper sheets, and

pairs of disposable nitrile gloves (pictured above). The Full Disclosure Kit for Laboratory

Analysis includes all the above items, sample collection vials, labels, and disposable templates.

Developed and patented* by the U.S. Center for Disease Control and

Prevention (CDC) and National Institute of Occupational Safety and Health

(NIOSH), Full Disclosure Lead Wipes† indicate the presence of lead quickly and

easily by displaying a pink or red color when lead is present on skin,

specifi cally hands, or surfaces. This indicates that further hand washing or

surface cleaning is necessary to completely remove lead. Lead

Wipes can also be sent to a laboratory for quantitative analysis of lead content.

* U.S. Patent No. 6,248,593

† Specifi ed in NIOSH Method 9105

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Sampling for Lead on Skin or Surfaces

Follow all steps of the instructions carefully.

Use the nitrile gloves provided in the kit when preparing the developing

solution or handling wipes before and after sampling to avoid cross

contamination. If performing successive wipe samples, use a new pair

of clean gloves for each sample.

Handling, storage, and disposal instructions for all materials are on

page 5.

Full Disclosure was designed to detect the presence of elemental lead

and other easily solubilized lead compounds. The extraction solution

will not solubilize all lead compounds. Full Disclosure is suitable for

elemental lead, lead nitrate, lead sulfate, lead acetate, and lead oxides.

Full Disclosure was not designed nor intended to detect lead chromates,

alkyl lead (i.e., tetraethyllead [TEL] or tetramethyllead [TML]), or other

less easily solubilized compounds of lead.

Full Disclosure is not suitable for the detection of lead in paint, paint

chips, on painted surfaces, or embedded in material such as plastic.

1. Preparation:

• Chill the spray bo le of deionized water (labeled Developing Solution

#3) in an ice bath or refrigerator to approximately 35 F (2 C). Do not

freeze.

• While wearing gloves,

tap one vial containing

Disclosing Powder #1

to dislodge adhered

particles from the walls

of the vial. Pour the

entire contents of

the vial containing

Disclosing Powder #1

into the spray bo le of

chilled deionized water

(labeled Developing

Solution #3). Cap the

bo le and shake until

thoroughly mixed. The

solution will turn an

orange color.

Pour one vial of Disclosing

Powder #1 into Developing

Solution #3 spray bo le.

Shake well to mix.

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• Mixed Developing Solution will remain active for several hours at

room temperature and for 10 days in refrigeration. Once expired,

discard solution, rinse and save spray nozzle. Use the additional bo le

of deionized water with saved spray nozzle and additional vial of

Disclosing Powder to mix a second batch of Developing Solution in

the second bo le labeled "Developing Solution #3." Follow Preparation

instructions.

2. Taking the Sample:

• On skin:

Open the wipe packet and unfold the wipe.

Wipe both hands or a selected skin surface for

30 seconds using only one side of the wipe.

Use normal hand washing pressure.

• On surfaces:

With gloved hands,

unfold the wipe.

Using only one

side of the wipe,

thoroughly wipe a

designated area of

the surface using

repeated horizontal

motions. Wipe the

same surface area

again using the same

side of the wipe,

but wiping at a right

angle to the fi rst

wiping motion. Wipes

may also be used on

irregular surfaces such as shoes or frames of glasses.

When taking surface samples that are to be

sent to a laboratory for analysis (Lab Analysis

Kit) use a template to specify the sample area.

Use a new pair of clean gloves for successive

wipe samples.

Wipe surface area horizon-

tally, then vertically using one

side of wipe.

Use a template to specify

sample area for samples to be

sent to a lab.

Wipe safety glasses, phones,

shoes, etc. thoroughly using

one side of wipe.

Wipe hands or skin for 30 sec-

onds using one side of wipe.

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3. Reading the Results:

• Spread the wipe, sample (soiled) side facing

up, on a piece of pre-cut waxed paper.

• Before using either spray bo le, prime by

aiming the nozzle into a garbage can and

depressing it until a fi ne spray appears.

• Using Extraction Solution #2, spray the

area of the wipe with the greatest soiling by

depressing the pump nozzle at least 3 times.

• Using prepared Developing Solution #3, spray the

same area of the wipe by depressing the pump

nozzle at least 2 times.

• Read the results immediately. The presence of lead below the lower

limit of visual identifi cation is indicated in the sample area by a yellow

to deep orange color. The presence of lead above the lower limit of

visual identifi cation is indicated in the sample area by a pink or red

color. The color bloom appears within seconds and begins to fade

quickly as the wipe dries. For information on other compounds that may

cause a color change, see Interferences on p. 7.

Aim at soiled wipe and

depress nozzle 2 times.

Yellow

Lead below lower limit

of visual identifi cation

is present (can also appear

orange or deep orange)

Red

Lead above lower limit

of visual identifi cation

is present

(can also appear pink)

Aim at soiled wipe and

depress nozzle 3 times.

Place wipe, sample side up, on

waxed paper.

Lower Limit of Visual Identifi cation: 18 μg of lead

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Handling, Storing, and Disposing of Full Disclosure

Materials:

Disclosing Powder #1

Powdered potassium rhodizonate compound.

Storing: Keep vial tightly closed and store in a cool, dry place.

Handling: Wear chemical-resistant gloves (included in kit). Avoid contact with eyes,

skin, and clothing. Do not inhale or ingest. Avoid prolonged or repeated

exposure. Wash thoroughly after handling.

Disposing: Whatever cannot be saved for recovery or recycling should be disposed in

an appropriate and approved waste disposal facility. Observe all federal,

state, and local environmental regulations.

For more details, see Material Safety Data Sheet included in kit.

Extraction Solution #2

5% acetic acid and water solution.

Storing: Store in spray bo le at room temperature.

Handling: Non-toxic, however, avoid contact with eyes and mucous membranes and

prolonged inhalation.

Disposing: Non-polluting; can be diluted with water and poured down a sink drain.

Developing Solution #3

Deionized water mixed with Disclosing Powder #1

Storing: After mixing, keep Developing Solution #3 cold [approx. 35 F (2 C)]

whenever possible. In the fi eld, keep the solution in a cooler and isolated

from food.

Developing Solution #3 will remain active for several hours at room

temperature and for 10 days if stored in a refrigerator. It is recommended

that the solution be used as soon as possible. When it deactivates, it changes

color from orange to pale yellow. If solution changes color from orange to

pale yellow, discard (see Disposing) and mix fresh solution.

Handling and

Disposing: See Disclosing Powder #1 above or Material Safety Data Sheet for Disclosing

Powder #1 included in kit.

Full Disclosure Wipes After Testing

Storing: Do not store. Dispose of wipes as outlined below or insert into sample

collection bo les and send to a laboratory for analysis.

Handling: Wear nitrile gloves to avoid contaminating the wipe.

Disposing: Dispose of used Full Disclosure wipes and any unused material observing

all federal, state, and local environmental regulations.

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Using Lab Analysis (Quantitative) Kit

1. Prepare the Developing Solution #3 and take a sample following the instructions for the

Sampling for Lead on Skin and Surfaces on page 2.

When sampling fl at surfaces, use a template to maintain the

size of the sample area. Disposable templates are included

in the Quantitative Kit.

2. Fold the wipe, sample (soiled) side facing in, and place in

the sample collection bo le. Identify the sample using the

labels provided in the kit.

3. Include 1 blank (unused wipe) for the laboratory for each

lot of samples. Place the blank wipe into a clean container

to prevent contamination of the wipe. Identify the blank

using the labels provided in the kit.

4. Package samples, blanks, and all appropriate sample information and ship to an

accredited laboratory for analysis

Analysis (quantitative): Atomic absorption spectroscopy or electroanalysis according

to NIOSH Analytical Method 7082, 7105, or 7701 modifi ed for wipes.

Lower Limit of Visual Identifi cation (qualitative): 18 μg of lead

For a listing of analytical laboratories that analyze Full Disclosure Lead Wipes, go to

www.skcinc.com or contact SKC Technical Support at skctech@skcinc.com.

For a performance report on Full Disclosure, view Publication No. 1485 at www.skcinc.com.

Insert in sample collection

bo le and label.

Use a template to

specify sample area.

7

Interferences

Full Disclosure may also display a color reaction to the following compounds, if

present:

• Silver

• Cadmium

• Barium

• Mercury

• Titanium

However, the reaction would only occur with higher concentrations of these

compounds (less sensitivity than that of lead).

Silver, titanium, and mercury will cause a red hue (reddish-purple to hot pink)

that is diff erent from that displayed with lead. Tin shows an opaque white color

at high concentrations. If it is suspected that these other elements are present,

use other testing methods to determine their presence and concentration prior to

using Full Disclosure for lead.

SKC Limited Warranty and Return Policy

SKC products are subject to the SKC Limited Warranty and Return Policy, which

provides SKC’s sole liability and the buyer’s exclusive remedy. To view the complete

SKC Limited Warranty and Return Policy, go to h p://www.skcinc.com/warranty.

asp.

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www.skcinc.com

Form 40091 Rev 1609

Description Cat. No.

Full Disclosure Kit‡ 550-001

Full Disclosure Kit‡ for Laboratory Analysis 550-002

Replacement Parts

Wipes, conform to ASTM E1792, 10/pk 550-022

Disclosing Powder #1 550-020

Extraction Solution #2 in spray bottle 550-021

Deionized Water for Developing Solution #3 in spray bottle 550-023

Nitrile Gloves, 11/pr 550-024

‡ Limited shelf-life