NMOS LOCOS Manual 2019
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EE 312 Winter 2019 Prof. Krishna Saraswat
NMOS-LOCOS
NMOS Process for EE312
INSTRUCTION MANUAL
Electrical Engineering Dept.
The Stanford Nanofabrication Facility (SNF)
Stanford University
EE 312 NMOS LOCOS Student Manual
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TABLE OF CONTENTS
1!INTRODUCTION ........................................................................................................ 3!
2!LABORATORY SAFETY .......................................................................................... 3!
2.1!Safety Philosophy .................................................................................................. 3!
2.2!General Safety ....................................................................................................... 4!
3!BACKGROUND .......................................................................................................... 5!
4!SUMMARY OF CMOS-LOCOS ................................................................................ 6!
4.1!General Features .................................................................................................... 6!
4.2!Comparison to Typical CMOS Processes ............................................................. 7!
4.3!Modifications from CIS/CMOS to CIS/CMOS-II ................................................ 7!
4.4!Modifications from CIS/CMOS-II to CMOS-LOCOS ......................................... 7!
5!PHOTOLITHOGRAPHY ............................................................................................ 8!
5.1!Description of Mask Levels ................................................................................... 8!
5.2!Mask Alignment Patterns ...................................................................................... 9!
5.3!Mask Alignment Errors ......................................................................................... 9!
5.4!Lithography Procedures ......................................................................................... 9!
6!PROCESSING TECHNIQUES ................................................................................. 10!
6.1!Laboratory Safety ................................................................................................ 10!
6.2!Clean-Room Techniques ..................................................................................... 10!
6.3!Wafer Cleaning Techniques ................................................................................ 10!
7!PROCESS FLOW ...................................................................................................... 11!
7.1!Global Alignment Marks and Blanket Substrate-Implantation ........................... 11!
7.2!Field Oxidation and Active Region Definition .................................................... 11!
7.3!P-Well Formation and Kooi Oxidation ............................................................... 12!
7.4!Gate Oxidation ..................................................................................................... 12!
7.5!Polysilicon Gate Formation ................................................................................. 13!
7.6!Source/Drain Implantations ................................................................................. 13!
7.7!Low Temperature Glass (LTO) Deposition ......................................................... 13!
7.8!LTO Densification and Silicon Anneal ............................................................... 14!
7.9!Contact Hole Formation and Metallization ......................................................... 14!
7.10!Final Passivation for Packaging (Optional) .................................................... 14!
8!SIMULATIONS ......................................................................................................... 16!
8.1!Process Simulations ............................................................................................. 16!
8.2!Device Simulations .............................................................................................. 17!
9!TEST STRUCTURES AND MEASUREMENT METHODOLOGY ...................... 17!
9.1!Fabrication Test Structures .................................................................................. 18!
9.2!Process Test Structures ........................................................................................ 18!
9.3!Device Test Structures ......................................................................................... 21!
9.5!SEM Test Structures (Optional) .......................................................................... 22!
10!REFERENCES ....................................................................................................... 22!
11!APPENDIX A: LIST OF CMOS-LOCOS STRUCTURES .................................. 24!
12!APPENDIX B: Pad Assignments .......................................................................... 30!
13!APPENDIX C: Agilent B1500 User Manual .......................................................... 49!
13.1!Standard Operating Procedure ......................................................................... 49!
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1 INTRODUCTION
The purpose of this document is to serve as a guide for EE312, the Integrated Circuit
Laboratory Course taught at Stanford University. The subject of this course is the
simulation, fabrication and testing of a simplified, 0.45µm gate length NMOS process
developed for EE312 and for use as underlying circuitry for device research. EE312 is
highly recommended for students planning to conduct research in the Class 100 clean
room Stanford Nanofabrication Facility (SNF) at the Center for Integrated Systems (CIS)
or how seek a career in device fabrication. To be admitted into the class, students must
be familiar with IC processing at the level of EE212 and fundamental device physics at
the level of EE216, and must have the consent of the instructor.
NMOS-LOCOS is designed so that in one academic quarter, students have the
opportunity to fabricate complete NMOS IC wafers using the SNF facility and in the
process, learn the practical skills, laboratory techniques and safely in wafer fabrication
and testing. The nominal gate length of NMOS-LOCOS is 0.5µm. While commercially
available gate lengths are much shorter, this dimension is compatible with standard SNF
processing and provides a solid teaching device platform. At the end of the process run,
students will have fabricated functional 0.45µm MOS transistors, inverters, and ring
oscillators along with a variety of process test structures.
The NMOS-LOCOS design is an introductory framework for conventional
semiconductor processing. Students are encouraged to probe further into the principles
and operating details of the equipment, methodology and device physics. It is the
command of such topics that will distinguish successful contributors in your chosen
career. Through courses like EE312, graduate research projects in the SNF lab, and
continuous seminars presented by leading experts from industry and other research
institutions, it is possible for Stanford students to emerge with a level of expertise which
is difficult to acquire even at the most advanced corporate research labs. Thus, it is
critically important for the students to grasp all of the available learning opportunities
presented on campus. Students need to think on their own, to go beyond the scope of this
manual and to challenge, improve or amplify some aspect of NMOS-LOCOS, as was
done previously with the former CMOS-LOCOS, CIS/CMOS and CIS/CMOS-II
processes. It is expect that the NMOS-LOCOS will continue to evolve in coming years
through to the interest and insight of students.
2 LABORATORY SAFETY
2.1 Safety Philosophy
The current safety policies are provided on the SNF web site. The following information
is provided only as an introduction to the safety information and should not be considered
complete or definitive. It is the responsibility of all Lab Members to be skilled, up to
date and practice all safety policies and procedures.
The primary goal of the SNF safety program is to prevent accidents. This can be achieved
if each and every person in the lab observes appropriate safety precautions. However, it
is understood that no system is perfect, and accidents can happen. The second goal of the
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safety program is also to minimize the effect of an accident by educating lab members on
how to respond in emergency situations.
SNF Staff Responsibility
The responsibility of SNF with regard to laboratory safety is to:
• educate and inform lab members of the potential safety hazards and appropriate
response procedures; and
• provide the appropriate tools and resources to use the lab safely.
The tools and resources provided by the SNF staff to lab members includes (but are not
limited to): the MSDS sheets which are provided near the SNF Stockroom; operating
procedures and training in safe operation for each tool; personal protective gear
appropriate for laboratory processing and training in its use; documented and posted
procedures for actions to take in an emergency situation; knowledgeable personnel,
trained in safety and emergency procedures.
Lab Member Responsibility
Your responsibility, as an SNF lab member, is to behave in a safe, conscientious, and
professional manner in all lab activities. The SNF provides you with information and
tools to use the lab safely; however, it is incumbent upon each individual to take
responsibility for his/her own personal safety. Moreover, as the SNF is also a community,
each lab member is responsible for the safety of his/her fellow lab members. At the
discretion of the SNF staff anyone found behaving irresponsibly to the extent of
endangering others may be immediately removed and denied future access to the lab.
It is also your responsibility to report any safety concerns you may have to any SNF staff
member. An alternative is to report any potentially unsafe conditions or practices, or to
offer suggestions for improving safety to safety@snf.stanford.edu.
2.2 General Safety
Lab Behavior
• As in any area where chemicals are in us, eating and gum chewing is prohibited.
Drinking is prohibited in the lab, except at the water dispenser located in the
service area. Individual water bottles are prohibited in the lab.
• Avoid sudden or fast movements. Running or fast walking is not permitted.
Approach corners and turns slowly to avoid collisions with others. Always
remember that lab members around you may be handling sensitive or hazardous
materials, such as chemicals, or their year's worth of work.
• Always clean up after yourself -- remove or store everything that you have
brought into the lab with you.
• Label all personal belongings with your name.
• Always be aware of your work area and be sensitive to what other lab members
are doing around you.
Clothing
• Shoes worn in the lab must fully enclose the feet. No sandals, open toe, high
heels or sling-back shoes are allowed.
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• You will be wearing a bunnysuit over your normal clothing. We recommend your
clothes be light, comfortable and allow free movement. Bare legs (i.e., wearing
shorts and dresses) are not recommended; slacks are preferred as they provide
additional protection.
Eye Protection
• Safety glasses are required at all times in the lab. Safety glasses should be of type
B, C, D, G, or H (with side shields or other side protection) and conform to ANSI
standard (marked "Z87".) Lab members requiring corrective lenses, impact-
resistant prescription safety glasses with side shields may be purchased from most
prescription glasses suppliers.
• Most safety glasses are designed to protect against flying fragments, and not
chemical splash hazards. Full face shields are worn, in addition to glasses when
handling chemicals or working at chemical wet benches.
• SNF abides by the American Chemical Society recommendation that "contact
lenses can be worn in most work environments provided the same approved eye
protection is worn as required of other workers in the area." (C&E News, Vol. 76,
p. 6.) Thus, contact lens wearers need to wear standard safety glasses when
working in the lab, and full face shields in addition to safety glasses when
working at chemical wet benches.
Personal Protective Gear
• While operating certain stations, additional protective wear will be required. Use
of any wet benches or the normal handling or transportation of any chemicals in
the lab requires the use of personal protective chemical wear.
Buddy System
• For safety reasons, a lab member is not allowed to work in the lab alone at any
time. Because the lab runs 24/7, there may be occasions (such as a late night,
early in the morning, over a long holiday weekend) when there are no other
people working in the lab. If you plan to work during a time when the lab might
be expected to be empty, you must plan ahead and coordinate your work schedule
with another lab member. This way, you can be sure to have a buddy and can
work safely.
3 BACKGROUND
During the summer and fall of 2008 a major redesign of the EE410 device structures and
teaching mask set was completed. The redesign was coupled to SNF obtaining the
ASML 5500/60 stepper. Using this stepper platform, it became routine to print 0.5 µm
feature sizes. In order to keep the process robust, a 1 µm minimum, nominal feature size
was chosen.
The major design change introduced with this design revision was to move away from
wet etched, thick field oxide for isolation to LOCOS isolation. The LOCOS added more
steps early in the process flow, but it provides a more traditional isolation without
moving to even more complex shallow trench isolation (STI) The redesign followed a
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ground up approach. Each device design starts with a parameterized Cadence p-cell.
This allows for a rapid, scalable change in device dimensions and the ability to layout
custom designs using the standard device library to meet future research needs. The
device library was designed as a 8 mask process (not counting ASML alignment mark
layer), however to expedite the processing during the EE410 class the compensated
doping approach for the n-well, p-well and n+source, p+drain of earlier designs was
retained, resulting in only 6 masking steps (not counting ASML alignment mark layer).
The die size was limited to 8.3mm x 8.3mm to fit four device layers on each 5” ASML
reticle.
Designs Revisions:
2008, Jae Hyung Lee, J. Jason Lin developed CMOS-LOCOS
1993, Alvin L.S. Loke developed CIS/CMOS-II
1987, Robert Scheer developed CIS/CMOS
In 2018 the NMOS- LOCOS process has been developed by simply omitting the PMOS
from the CMOS-LOCOS with an objective to shorten the processing time so that the
fabrication can be finished in 1 quarter and more time can be spent on electrical
characterization.
4 SUMMARY OF NMOS-LOCOS
4.1 General Features
The CMOS-LOCOS process is characterized by the following:
• EE312 class uses 4 mask levels (not including the ASML global mark exposure)
• 100 mm n-type wafer substrates (pre-implanted for PMOS threshold adjusting)
• 0.45µm gate dimension, 1µm contacts and 2µm poly and metal traces.
• conventional optical lithography using positive resist
• fully automated exposure by 500/60 ASML stepper
• fully automated resist coating and developing
• anisotropic dry etches (LOCOS nitride, polysilicon, contact and metal)
• pad oxide and nitride hard mask for LOCOS process
• 10nm gate oxide, 500nm LOCOS isolation oxide
• shallow p-well implantation for NMOS threshold adjusting
• amorphous "poly"-silicon gates
• n-type poly for NMOS transistors
• source/drain formation by self-alignment
• single level of aluminum/silicon metallization, without passivation
• non-silicided contacts (high metal contact resistance to poly and active regions)
• Low Temperature Oxide (LTO), undoped
The NMOS-LOCOS chip has the following features:
• 8.3mm x 8.3mm die area (84 die per wafer)
• variety of process, device and circuit, test structures
• 150µm X 100µm metal probe pads
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• independent probe pads for all test structures (no shared connections between
adjacent structures)
• very conservative design rule guidelines
4.2 Comparison to Typical CMOS Processes
In order to complete the processing and testing of NMOS-LOCOS in one quarter, many
standard CMOS features have been omitted or simplified. The simplifications in CMOS-
LOCOS will unquestionably reveal compromises in device performance. For example,
industry-standard devices are carefully threshold-adjusted to make device channels more
electrically controllable and more insensitive to process variations. In addition, self-
aligned silicide is used in industry to minimize the contact resistances of metal to gate
and metal to active region. Consequently, for these and other reasons, industrial CMOS
processes usually require at least 8 to 12 masks and certainly much longer time cycles.
As part of the complete EE312 learning experience, the students should understand how
the simplifications made in NMOS-LOCOS will affect device quality and why industry is
justified in pursuing more sophisticated process flows to build the same device structures.
4.3 Modifications from CIS/CMOS to CIS/CMOS-II
For those familiar with the CIS/CMOS process, the updated process is essentially
identical to the former CIS/CMOS process as described in [1] and [2], with the exception
of three important modifications. Firstly, the starting materials are now 4-inch wafers
instead of 3-inch wafers. This entitles the new process to take advantage of more
automated lithographic procedures. Secondly, the wafers are subjected to a phosphorus
blanket pre-implant prior to field oxidation. Lastly, the single deep p-well implant in the
former process is now replaced by a dual p-well implant sequence: a shallow implant to
control the surface threshold and a deep implant to isolate the p-well from the n-type
substrate beneath. The latter process modifications are included since they do not require
additional masking steps and provide a better means of controlling the threshold voltages
of the resulting NMOS and PMOS transistors. The aforementioned variations will be
highlighted again in the process flow description to follow.
4.4 Modifications from CIS/CMOS-II to CMOS-LOCOS
The CMOS-LOCOS is a new design. It is based on the device structures and process
developed using the CIS/CMOS and CIS/CMOS-II. The process still runs on 4” inch
wafers and incorporates the capability of the 5500/60 ASML stepper. The major changes
include LOCOS isolation and eliminating all wet etch steps. The design approach uses
individual, parameterized p-cells for each device. This approach allows researchers to
simply change any critical dimension of any device while retaining contact locations and
metal traces. Gate lengths were reduced to 0.45µm, 1µm contacts and 2µm poly and
metal traces. The size of the die was changed to 8.3mm X 8.3mm and the probe pads
were reduced to 150µm X 100µm.
4.5 Modifications from CMOS-LOCOS to NMOS LOCOS
NMOS- LOCOS process has been developed by simply omitting the PMOS from the
CMOS-LOCOS. All other steps are similar.
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5 PHOTOLITHOGRAPHY
CMOS-LOCOS uses conventional optical lithography techniques throughout the process
flow. All masking steps use the SVG Coater, ASML stepper, and the SVG Developer.
Students are asked to consult the respective manuals in the laboratory for more detailed
information about equipment operation.
5.1 Description of Mask Levels
The 5 mask levels in the NMOS-LOCOS process are summarized in Table 1.
Table 1. Description of the seven ASML mask levels in the CMOS-LOCOS process.
No.
Mask Level
Description
0
GLOBALMARKS
Defines global alignment marks for pattern registration
1
ISO
Defines active areas on wafer surface
2
GATE
Defines polysilicon patterns for wiring and MOS gates
3
CONT
Defines contact holes to active or poly underneath
4
METAL
Defines metal connections for wiring
The 5500/60 ASML stepper is a new optical lithography capability made possible
through a unique partnership with ASML. It is a 5:1 reducing stepper with I-line (365 nm)
lamp source with a minimum resolution is 0.45µm. It also features alignment accuracy
of 60nm.
To avoid confusion, what is conventionally referred to as a mask at SNF is known as n
reticle to the ASML stepper. According to proper ASML terminology, four images are
arranged on to a single 5” reticle. The zero layer global marks are provided on a
dedicated ASML recile called the “combi” reticle. All of the EE312 images are contained
on two ASML reticles as indicated in Table 2. Each of the reticles have a barcode on it
for the ASML workstation to read while a job (exposure) is being executed.
All of the images, with the exception of the GATE and METAL levels are considered to
be data clear. This indicates the gds data is clear on the reticle, ie, most of the image field
is chrome, or dark. The GATE and METAL images are considered to be data dark, ie.
most of the image is clear glass.
Table 2. Image fields on completed ASML masks.
Image Field
Reticle No. 1
(barcode: EE410 2008 1)
ISO
PWELL
GATE
NDOPE
Image Field
Reticle No. 2
(barcode: EE410 2008 2)
PDOPE*
CONT
METAL
FIELDOX*
* The PDOPE and FIELDOX images are for engineering experiments only and are not included in the
EE312 CMOS class process.
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5.2 Mask Alignment Patterns
ASML’s approach to alignment is based on wafer level alignment, then precession stage
movement. The approach is different from many steppers which perform an alignment at
each die. The wafer level approach of ASML is possible due to the laser interferometer
used to determine the exact stage location. The wafer level alignment of ASML is very
successful in maintaining very good overlay performance and enhanced through-put by
minimizing alignment time.
The wafer level alignment approach requires the alignment marks be placed prior to any
device levels. The layer containing the alignment marks is called the zero layer, because
it precedes all device layers. Alignment can be done using between two and 200
alignment marks. Only two are used for optical prealignment in ASML. Additional global
alignment marks can also be positioned as backup in case the primary marks are damaged.
5.3 Mask Alignment Errors
After photoresist is patterned, mask alignment errors (in both X- and Y- directions) can
be determined by inspecting the Vernier scales located in the upper right corner of each
die. The resolution of the alignment Verniers is 0.05µm. A set of five Vernier scales,
shown in Table 3, is provided. Each Vernier scale is consists of Vernier patterns in two
levels: the bottom level is a wafer pattern defined in a prior lithography step and the top
level is the photoresist pattern. It is important that the students check the appropriate
Vernier scale to ensure that each subsequent mask level is aligned properly to the correct
mask level that is already defined on the wafer.
Table 3. Vernier scales on CMOS-LOCOS wafers for determination of alignment errors.
For NMOS-LOCOS F9 is omitted
Vernier Scale
Location
Bottom Level
(Wafer Pattern)
Top Level
(Resist Pattern)
Remarks
F9
ISO
PWELL
PWELL alignment
F10
ISO
GATE
GATE alignment
F11
GATE
NDOPE
NDOPE alignment
F12
GATE
CONT
CONT alignment
F13
CONT
METAL
METAL alignment
5.4 Lithography Procedures
In each lithography sequence, the wafers are first singed and primed in the yes oven to
remove any adsorbed moisture and coat HMDS for improved resist adhesion. Then on
the SVG (Silicon Valley Group) Coater positive resist is spun onto the wafers. The
photoresist coat recipes include a backside wash to remove any photoresist which might
of wicked around the edge of he wafer to the backside and a topside edge bead removal
(EBR). These steps have been integrated in to the coat process to prevent any backside
contamination from being introduced to the ASML stepper. The resist is then exposed
using an ASML stepper (capable of 0.45µm resolution), post-expose baked and
developed on the SVG Developer. In some cases there is an additional post-bake at
110˚C for 25 minutes in an oven. Thereafter, the patterned resist is ready for subsequent
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processing. Once used, the photoresist is removed by a standard resist stripping
procedure involving hot H2SO4 and H2O2. Should the resist be difficult to remove, the
wafers are subjected to oxygen plasma in the gasonic asher prior to the hot bath treatment.
6 PROCESSING TECHNIQUES
6.1 Laboratory Safety
Since laboratory safety can never be overemphasized, the students are reminded again of
the importance of safe practices in the laboratory. In addition, it is to no surprise that
when laboratory work is conducted safely, gross processing mistakes become less
frequent which can only mean better-quality results are likely to be attained. On another
note, incidences could potentially destroy a complete batch of wafers (e.g., acts of God)
do sometimes occur. The students are reminded that in the event of such a catastrophe,
panic leading to careless laboratory conduct will only aggravate the situation. Remember,
your safety (not the wafers' safety) is first and foremost!
6.2 Clean-Room Techniques
The cleanest room in the world cannot protect a wafer against the emissions from a
human mouth. Should one decide to breathe or speak in close vicinity to a wafer, it is
probably better to expectorate at the wafer so that wafer contamination becomes so
clearly obvious that the wafer must be disposed of immediately. Also, remember that one
fingerprint has enough sodium to "threshold-adjust" all your MOS gates and render them
as valuable as the pile of sand from which they are derived. Gloved hands are
unquestionably cleaner than uncovered hands, but consider what they have touched prior
to your wafers. Watch your classmates and see how many times they touch their face or
use the ink pen they brought in the fab without cleaning. The bottom line is "DO NOT
TOUCH THE WAFERS" with any part (or former part) of your body, whether it is
covered or not. Even if you do not come in contact with the wafers, there are certain lab
practices one should follow to reduce particle counts in the laboratory. For instance,
proper and complete gowning before entry into the laboratory is critical. In addition,
while in the laboratory, rapid and abrupt motions (such as running or rushing) are
considered intolerable because not only do they increase local particle counts by orders of
magnitude, they are also very unsafe!
As a final note, remember that the IC laboratory is a work environment where one has to
work in cooperation with all other users of the facility. Hence, courtesy and cooperation
with other fellow users is very important. Keep this is mind as you make your debut
appearances into the clean room.
6.3 Wafer Cleaning Techniques
CMOS-LOCOS, alike all other process flows in the SNF clean room, utilize standard
wafer cleaning practices to ensure wafer and particularly equipment contamination is
minimized as much as possible. Throughout the process flow, the wafers undergo
various non-diffusion and pre-diffusion cleaning steps, designed to remove organic and
inorganic contaminants respectively from the wafer surfaces. In non-diffusion cleaning
(equivalently resist stripping), the wafers are immersed in hot H2SO4 and H2O2. In pre-
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diffusion cleaning (also called a modified reverse RCA cleaning), the wafers undergo a
hot H2SO4/H2O2 bath to further remove organic residues, a quick HF dip is used to remove
any native oxide that formed and the hot HCl/H2O2 bath is used to remove inorganics such
as metals. Since high-temperatures steps aggravate the problem of contaminant diffusion,
the pre-diffusion clean always precedes any furnace cycle and is consequently extremely
important to prevent furnace contamination. If there is metal on the wafers, a different
cleaning procedure is required because the acid solutions will attack the metal. Cleaning
wafers with metal is typically done in a solvent solution at elevated temperatures. Refer
to the process run sheets (separate handout) for specific procedural details.
7 PROCESS FLOW
The starting material for NMOS-LOCOS is a 100 mm, <100>-oriented, Czochralski-
grown, n-type (phosphorus-doped) silicon substrate of 5 to 10 W-cm resistivity and
525µm thickness. Refer to Fig.1 for an illustrative summary of the process flow. Process
details are described to provide students with sufficient knowledge to understand the
purpose of each procedure without delving on specifics such as equipment operation.
The students are asked to consult the process schedule and process run sheets (provided
as separate handouts) for further details.
7.1 Global Alignment Marks and Blanket Substrate-Implantation
The first step in the EE312 process flow is the formation of the ASML global alignment
marks. This requires a photolithographic step and dry etching. Following the dry etch of
the global alignment marks, the wafers undergo the standard non-diffusion and pre-
diffusion cleaning sequences. The wafers are then taken to an ion implantation vendor for
a blanket substrate implant of 30 keV boron ions (B11) with a dose of 3x1013 cm-2. The
blanket implant is designed to control the substrate surface concentration in order to
choose the threshold voltages of both the active NMOS and parasitic field NMOS devices.
Since the NMOS thresholds are governed by the surface implant conditions, making the
process more robust against variations in starting substrate resistivities. The implant dose
introduces an additional degree of freedom in selecting the NMOS thresholds.
7.2 Isolation Implant, Field Oxidation and Active Region Definition
Following the standard pre-diffusion clean, the wafers are oxidized in a wet ambient to
grow 20 nm thick thermal silicon dioxide layer, commonly referred to as the pad oxide.
Specifically, in 5 minutes, the wafers are ramped from 800˚C to 850˚C in a dry
argon/oxygen ambient. Then, the main oxidation occurs at 850˚C during a 12-minute wet
oxidation in steam followed by another 5 minutes in pure O2. The wafers are ramped
down to 800˚C in an inert argon ambient. The wafers are immediately moved from the
oxidation furnace to the LPCVD nitride furnace. It is critical for move immediately from
the oxide furnace to the nitride furnace to avoid a standard pre-diffusion clean which will
also etch the pad oxide. The LOCOS silicon nitride thickness target is 200nm. The
silicon nitride deposition is a LPCVD (Low Pressure Chemical Vapor Deposition) at
785˚C for approximately 45 minutes.
Resist is patterned using the ISO (isolation) image on reticle 1 during the first masking
level. The isolation mask defines the field oxide regions, which is formed after the dry
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etch of the nitride and field oxidation. The nitride etch is done in the applied materials
P5000 Etcher.
The wafers are then taken to an ion implantation vendor for the isolation implant of 30
keV boron ions (B11) with a dose of x1015 cm-2. The blanket implant is designed to control
the substrate surface concentration in order to choose the threshold voltages of both the
parasitic field NMOS devices.
The resist is then stripped in piranha (9:1 H2SO4:H2O2) at 120˚C for 20 minutes, field
oxidation (wet oxidation) is done at 1000˚C for 1 hour and 40 minutes in order to grow
about 540nm thick field oxide. The field oxidation can be done in either in the Tylan or
Thermco furnaces.
During the field oxidation the top surface of the LOCOS nitride is oxidized. This layer
needs to be stripped in HF dip prior to removal of the nitride as the Phosphoric acid used
to strip the nitride does not etch the oxidized layer. Stripping of the nitride is done in the
wbnitride using Phosphoric Acid at 150˚C for approximately 1 hour. It is critical to make
sure all the nitride is removed as this area becomes the gate oxide of the devices. If any
nitride is left behind, the gate oxide will not grow correctly.
In field oxidation and gate oxidation (to be discussed in the next section), the main
oxidation is preceded by a temperature ramp in a 4% oxygen ambient. The purpose of
introducing O2 at low temperatures assists in the formation of good-quality oxide-silicon
interfaces. The mechanism is nucleation of the exposed silicon surface which forms
oxygen-silicon complexes at the low temperatures. At higher oxidation temperatures, the
oxygen becomes super-saturated and the thermodynamics dictates the oxygen in these
complexes will escape into the ambient. Meanwhile, oxygen atoms in the silicon
substrate that have precipitated beneath the surface will leave the bulk and passivate the
oxygen-free surface. This high quality interface results in low junction reverse leakages
as well as high minority carrier lifetimes and mobilities.
7.3 Kooi Oxidation
The wafers are then subjected to a Kooi oxidation at 850˚C for 15min in steam. Growing
and subsequent removing the Kooi oxide is used to eliminate the remnant Kooi ribbon of
nitride which forms around the active area at the LOCOS edge (or field edge) during the
previous field oxidation. (Silicon nitride in a steam oxidation environment decomposes
into ammonia and silicon dioxide. The ammonia diffuses down through the field oxide
until reaching the silicon surface, where it reacts to form a silicon nitride, and leaving a
ribbon of nitride at the silicon/silicon dioxide interface around the edge of the active area.)
7.4 Gate Oxidation
The first step is the removal of the sacrificial oxide (a combination of the pad oxide and
Kooi oxide) in HF. The sacrificial oxide growth and removal results in a high quality
silicon surface for growth of the gate oxide. In addition to maintaining a high quality
silicon surface, it is also important to grow the gate oxide in a very clean oxide furnace.
EE 312 NMOS LOCOS Student Manual
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Part of the gate oxide process is to perform a TLC clean on the oxide tube, just prior to
the growth of the oxide. TLC cleans are used to remove any metallic contamination
which might have accidentally been brought in to the furnace.
The gate oxide growth is a short dry thermal oxidation cycle to grow a thin 10nm thick
gate oxide in the active regions. The wafers are ramped from 800˚C to 900˚C in an
argon/oxygen ambient. The main oxidation sequence consists of a 20-minute dry
oxidation. The wafers are then ramped down to the 800˚C pull temperature. The wafers
must go directly to poly deposition, with out any time between the gate oxide unloading
and poly loading.
7.5 Silicon Gate Formation
Once the gate oxide grown on the silicon active areas, the wafers go immediately to the
next step, a low-temperature conformal blanket silicon. In LPCVD (Low Pressure
Chemical Vapor Deposition) furnaces, silicon deposition results from the thermal
decomposition of silane (SiH4). Since the deposition temperature is only 560˚C, the
resulting film is amorphous and not polycrystalline, but by convention, the term
polysilicon is still used as during the subsequent thermal steps it is crystallized. The
0.2µm thick amorphous Si layer is used in NMOS-LOCOS to prevent ion channeling
through the gate in subsequent source/drain implantations.
Photoresist is patterned on the polysilicon layer using GATE masking level 2 (GATE -
clear field). The photoresist pattern is used as the mask for dry etching on the P5000.
The dry etching process anisotropically etches the polysilicon defining the gate structures.
In prior generations there were concerns that unwanted polysilicon stringers at field oxide
steps may inadvertently form short-circuits. This was not evident with the current
LOCOS structure, but will only be confirmed by running the process many times.
7.6 Source/Drain Implantations
The NMOS source/drain regions are formed using an arsenic implant (dose of 2x1015 cm-2
at 50 keV) which dopes the NMOS gates and creates the n+-source/drain by self-
alignment. (Arsenic is chosen since it is a slow diffuser.) Since the implant dose is quite
substantial, care must be exercised to ensure that the implant beam current is limited to
prevent resist blistering. Following the implant, the resist mask must be stripped in the
Gasonics Plasma Asher as the resist has been considerably hardened during the implant.
If the hardened resist is not removed in the Gasonics Asher, it is likely the typical Piranha
clean will not be able to fully remove the resist.
7.7 Low Temperature Glass (LTO) Deposition
A passivating 0.6µm layer of undoped, low-temperature oxide (LTO) is deposited at
400°C (not thermally grown) on both sides of the wafer using a SiH4/O2 LPCVD system.
The deposited LTO serves the following purposes:
• surface protection of the fragile silicon/oxide features beneath,
• physical barrier to mobile ion and humidity contamination, and
• surface planarization for metallization with reliable continuity.
EE 312 NMOS LOCOS Student Manual
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7.8 LTO Densification and Silicon Anneal
The LTO film is densified and silicon anneal is done in steam at 950˚C for 30 minutes.
This causes some reflow of the LTO to smooth any sharp corners. The densification
anneal also results in changing the physical and chemical properties of the LTO oxide
making it more similar to a thermal oxide.
The silicon anneal portion is used to activate and diffuse the N-Source and P-Dope
implants. The anneal serves the following four purposes:
• activates all N-Source and P-Dope implant,
• drives-in the source/drain regions,
• anneals the gate oxide, and
• allow the LTO glass to reflow and smooth out sharp corners.
7.9 Contact Hole Formation and Metallization
After the LTO densification, the wafer surface topography should have been smoothed
slightly as metal lines have a strong tendency to break at abrupt corners and edges. The
contact hole openings are defined using the CONT mask, layer 3 (CONT - dark field.)
The contact alignment is the most critical alignment in the process flow. The contacts are
1µm in diameter and they must be correctly placed on 2µm structures. Standard
lithography is performed to pattern a resist mask and is followed by a vertical reactive-
ion etch (CHF3/O2 plasma) to open up the contacts in the LTO. The contact etch sequence
ends with the resist strip.
Once the contact holes are created, a 1 µm thick aluminum/silicon alloy is deposited on
the wafers in the Gryphon sputtering chamber. Here, 1% silicon is intentionally added to
the aluminum to prevent aluminum from spiking into the exposed source/drain areas.
In defining the metal features using the Metal mask, layer 4 (METAL1 - clear field) is
used to pattern a resist mask against aluminum etching. The aluminum alloy is
isotropically etched using dry reactive ion etching in chlorine chemistry. The etch wafers
must be immediately immersed in water once they come out of the dry etch tool. There
will be residual chlorine ions attached to the aluminum, photoresist and oxide surfaces.
These ions react with the moisture in the air to form HCl which rapidly attacks the
aluminum pattern. This phenomena is frequently called corrosion in the industry. The
resist is removed using an PRS-3000 (at 40˚C for 20 minutes). (The standard hot
H2SO4/H2O2 solution cannot be used since the acid component will attack the aluminum
layer.)
7.10 Final Passivation for Packaging (Optional)
In the fabrication of integrated circuits, after the metal is patterned, a thick passivating
layer of low-temperature silicon nitride is deposited over the entire wafer. A pad mask,
(PAD - dark field), is used to create openings in the metal pads for external connection
schemes such as wire bonding. The purpose of the nitride is clearly to protect metallized
areas of the die from the atmosphere and contamination, thus improving the overall
reliability of the chip. However, since the NMOS-LOCOS dies will not be packaged no
passivation layer will be deposited.
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EE 312 NMOS LOCOS Student Manual
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Fig. 1. NMOS-LOCOS process summary. Refer to text for details.
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EE 312 NMOS LOCOS Student Manual
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8 SIMULATIONS
As with any undertaking in device fabrication, the role of simulations cannot be
underemphasized. Simulations promote both understanding of the process flow and
consideration of the process limitations. In EE312, students are required to use
SENTAURUS to simulate the process flow and extract relevant electrical parameters
such as MOS threshold voltages and sheet resistivities. In addition, students should
estimate basic profiles and device electrical parameters using standard equations derived
from processing/device physics (which can be found in [3], [4] and [5]) and subsequently
formulate comparisons between hand calculations and simulation results.
8.1 Process Simulations
The NMOS-LOCOS process flow must be simulated using SENTAURUS. Given the
chronological sequence of a process flow at a particular one-dimensional cross-section of
the wafer, SENTAURUS determines the resulting material layers/thicknesses and
impurity profiles [6]. To model NMOS-LOCOS thoroughly, one must model at least the
following 4 one-dimensional cross-sections as shown in Fig.2. Cross-sections are
referenced in Table 6.
Fig. 2. NMOS-LOCOS wafer cross-sections of 1. NMOS Source/drain region, 2. NMOS
gate/channel region and 3. Field oxide region (parasitic metal-field NMOS channel and
parasitic n-poly-field NMOS channel) to be simulated by SENTAURUS.
1
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2
3
4
p-substrate
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EE 312 NMOS LOCOS Student Manual
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Cross-section
number
Description
1
NMOS source/drain
2
NMOS channel
3
Parasitic metal-field NMOS channel
4
Parasitic n+-poly-field NMOS channel
Table 4. Description of cross-sections shown in Fig.2.
As an extension, students are welcome to use THE two-dimensional process simulator, to
simulate two-dimensional effects such as lateral source/drain diffusions and etch
isotropy/anisotropy.
8.2 Device Simulations
SENTAURUS can also be used to calculate simple device parameters such as MOS
threshold voltages and sheet resistivities. Threshold voltages are to be calculated for both
active area devices and parasitic devices in the field regions. For more accurate
estimations of the electrical parameters, students may choose to use SENTAURUS
DEVICE, a one-dimensional device simulator, to obtain more accurate estimates of the
relevant electrical parameters.
9 TEST STRUCTURES AND MEASUREMENT METHODOLOGY
Upon completion of the process flow, each NMOS-LOCOS wafer will contain a variety
of (1) fabrication, (2) device, (3) process, (4) circuit, and (5) research test structures in the
general arrangement shown in Fig. 3. There are several replicas of each test structure on
each wafer. Except for the fabrication, the various terminals of each test structure are
connected to large 150µm x 100µm rectangular aluminum pads for probe testing. Please
refer to Appendices A and B for a complete description of the chip contents and pad
assignments.
Fig. 3. General arrangement of test structures on a CMOS-LOCOS die.
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EE 312 NMOS LOCOS Student Manual
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Please note that a complete set of independent probe pads has been provided for each test
structure, i.e., there are no shared connections between adjacent structures. Also, much
care and effort was taken to ensure that the test structures and their respective pad
connections are arranged as systematically as possible to simplify testing.
This section provides some brief documentation on the types of test structures that are
found on the NMOS-LOCOS wafers and where appropriate, short descriptions of the
methodologies involved in testing particular structures. The students are directed to
consult [8] for a more complete description of testing methods.
9.1 Fabrication Test Structures
Two sets of fabrication test structures are located at the top corners of each die. These
structures consist of large areas provided for consistent thickness measurements of the
different layers, such as field oxide, gate oxide and polysilicon, during the fabrication
process only.
9.2 Process Test Structures
Process test structures are very simple structures designed to obtain very specific pieces
of information about the process flow and also to evaluate specific electrical parameters
that would be otherwise be very difficult to extract from more sophisticated structures
such as transistors. In the NMOS-LOCOS die, five kinds of process test structures are
provided, namely sheet resistivity structures, contact chains, 6-point Kelvin contact
structures, continuity structures and isolation structures.
The sheet resistivity structures of various wafer layers are provided in two varieties: 4-
point probe and van der Pauw structures (Fig. 4).
(a) (b)
Fig. 4. Layout of (a) 4-point probe and (b) van der Pauw structure.
I-1 FORCE I-2 FORCE
V-1 SENSE V-2 SENSE
L
W
VDP-1
VDP-2 VDP-3
VDP-4
Metal Contact Hole
Specified Wafer Layer
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EE 312 NMOS LOCOS Student Manual
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In the 4-point probe structures, a current IFORCE is forced through the I-1 FORCE and I-
2 FORCE pads, resulting in a voltage VSENSE developed across the V-1 SENSE and V-
2 sense pads. The sheet resistivity can then be obtained using (1) where W and L are the
dimensions of the 4-point probe structure.
(1)
Here, 4-point probes are used instead of 2-point probes to circumvent the problem of
series contact resistances. In calculating sheet resistivities, since two structures of
different widths are provided for each layer, students should correct for the width of each
structure by using Weff = W - ∆W (due to lateral diffusions, undercutting, etc.). The van
der Pauw structures consist of four contacts (labeled VDP-1, VDP-2, VDP-3 and VDP-4
in counterclockwise sense) symmetrically arranged around an octagonal area. The sheet
resistance can be obtained by forcing a current across two adjacent terminals and
measuring the resulting voltage developed across the other two and by subsequently
applying (2).
(2)
A more detailed treatment of the van der Pauw analysis is found in [8].
A contact chain consists of a continuous chain of 100 contacts alternating between metal
to an active (or poly) layer and of that layer back to metal. See Fig. 5. Each chain has
taps at 10 and 100 contacts so that students can verify the linear relationship between
total chain resistance and the number of contacts.
Fig. 5. Layout of poly/active-to-metal contact chain section.
Although the resistance per contact obtained from contact chain measurements is a good
indicator of the contact resistance, one should technically subtract the resistance of the
active/poly segments in series with the contacts to evaluate the true contact resistance. A
better determination of the contact resistance can be obtained using the 6-point Kelvin
contact structure, shown in Fig. 6.
Rsheet =R
meas
W
L
=VSENSE
IFOR CE
W
L
Rsheet =
p
ln2
Rmea s =
p
ln2
V12
I43
Contact Hole Active/PolyMetal
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EE 312 NMOS LOCOS Student Manual
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Fig. 6. Layout of 6-Point Kelvin contact structure for measuring contact resistance.
A current is forced from K-1 to K-3. The potential established across K-2 and K-4, i.e.,
voltage difference directly above and beneath the middle contact, is measured. The
contact resistance is then the simple ratio given by (3).
(3)
Kelvin structures with four contact hole sizes are provided to facilitate the study of
contact resistance as a function of contact size. Other contact resistance parameters can
also be obtained by probing the other pads [8]
Transfer Length Method structures consists of several contacts between metal and n+
doped Si, spaced at different intervals. This structure provides information about the
contact resistance and specific contact resistivity. The detail information is provided at
Appendix 1.
Continuity and isolation structures complement each other to provide information about
the integrity of interconnections within a specified layer. See Fig. 7.
(a) (b)
Fig. 7. Layout of (a) continuity and (b) isolation structures.
K-1
K-2
K-3 K-4
K-5
K-6
Active/Poly
Contact Hole
Metal
R
con ta ct =V13
I24
A
B
A
B
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EE 312 NMOS LOCOS Student Manual
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The continuity structures, designed to detect unwanted open circuits, consist of long
snakes of various materials. For verification of metal step coverage over sharp edges,
some metal snakes traverse over a variety of surface features. Isolation structures serve
to detect unwanted short circuits and consist of two isolated combs that interpenetrate
into each other. Here, some metal combs are situated over various wafer terrains to
ensure that residual traces of unwanted metal do not exist. To test both types of
structures, simply apply a voltage (or current) across terminals A and B, and observe the
resulting current (or voltage) to extract a resistance value for the structure in question.
Structures that fail continuity tests will obviously exhibit high resistances while structures
that fail isolation tests will exhibit low resistances.
9.3 Device Test Structures
NMOS-LOCOS design contains a variety of basic devices: NMOS transistors, parasitic
NMOS transistors, parasitic NPN and PNP bipolar junction transistors (designed for
CMOS process only), diodes and MOS capacitors.
The students are welcome to study all relevant aspects of the fabricated MOS transistors,
such as device thresholds, body effects, channel-length modulation, and breakdown
mechanisms to name a humble few. To test these structures, appropriate biases must be
applied to the source, gate, drain and p-well/n-substrate pads. (It would be very useful
here to consult standard literature; for example, [3], [8] and/or EE216 notes.) For active
NMOS, shown in Fig. 8, there exist two arrays of transistors: the L (length) series array
(gate width fixed at 100µm while length is varied) and the W (width) series array (gate
length fixed at 5µm while width is varied). These arrays permit investigation of short-
and narrow-channel effects as well as extractions of effective gate lengths and widths.
Fig. 8. Schematics for n-channel MOSFET.
There are also various minimum size transistors (as small as W/L = 4µm/0.45µm) located
in the W and L series arrays. The author included these structures in an ambitious
attempt to test the limits of the NMOS-LOCOS process flow.
Metal and polysilicon interconnects running over the wafer field regions automatically
form parasitic MOS transistors. These devices need to be investigated because for proper
active device isolation, these parasitic transistors must be in their off states. Equivalently,
the threshold voltages of the parasitic channels must exceed circuit supply voltages.
GAT E
SO URCE
DR AIN
P- WEL L
W/ L
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Parasitic poly gate transistors are separated from the substrate beneath by the field oxide
while parasitic metal gate transistors are separated from the substrate by the field oxide
and LTO glass layers. Testing procedures for parasitic MOS transistors are identical to
those for active MOS devices.
Different combinations of pn-junction diodes are available for standard diode
characterization (analysis of I0 and reverse leakage currents). See Fig. 9.
Fig. 9. Determination of I0.
For each type of pn-junction, both area- and edge-intensive diodes are fabricated so that
the area and edge components of I0, and those of reverse biased leakage current Irev can
be evaluated.
(4,5)
(6)
In addition, the behavior of the fabricated p+poly-n+poly diode should be investigated.
9.4 SEM Test Structures (Optional)
On the continuity structures, cross-sections of important test structures have been
integrated for SEM analysis. To inspect these structures using the scanning electron
microscope, the wafer must be cleaved to isolate a particular die. Next, the selected die
must be cleaved vertically along the array of SEM structures. Standard SEM sample
preparation must then be followed. It might be necessary to subject the exposed cross-
section cuts to certain etch solutions in order to improve the contrast of the SEM images.
Detailed contents of the SEM cross-sections are provided in Appendix A.
10 REFERENCES
[1] Robert F. Scheer, “CIS/CMOS: A Very Simple, Two-µm, CMOS Process
Developed for Stanford EE410”, Dec. 1987.
ln (I)
ln (I0)
Forward Voltage
IDiode =I0´eqV/kT -1
( )
I0=I0,Area ´Area +I0, Ed ge ´Perimeter
Irev
=Irev,Area
´Area +Irev,Ed g e
´Perimeter
EE 312 NMOS LOCOS Student Manual
Page 23 of 52 Revision Date: Jan. 2018
[2] S. Simon Wong, “EE410 Handout #7: EE410 CMOS Process (Run Sheets)”, Jan.
1993.
[3] Richard S. Muller and Theodore I. Kamins, “Device Electronics for Integrated
Circuits”, John Wiley & Sons, 1986.
[4] Simon M. Sze, “VLSI Technology”, McGraw-Hill, 1988.
[5] Krishna Saraswat, "EE212 Course Notes ", Sept.1992.
[6] SENTAURUSTM,
“http://www.synopsys.com/Tools/TCAD/CapsuleModule/sentaurus_ds.pdf”.
[7] B. Johnson et al., "SPICE3 Version 3D2 User's Manual", Oct. 1990.
[8] Dieter K. Shroder, “Semiconductor Material and Device Characterization”, John
Wiley & Sons, 1990.
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11 APPENDIX A: LIST OF CMOS-LOCOS STRUCTURES
Electronic Devices
1. N-Channel MOSFET (D-1 to D-4)
D-1 Length Series (Gate W/L in um)
! 100/100 100/25 100/5 100/2.5 100/1
D-2 Length Series (Gate W/L in um)
! 100/0.75 100/0.6 100/0.55 100/0.5 100/0.45
D-3 Width Series (Gate W/L in um)
! 100/5 25/5 10/5 6/5 4/5
D-4 Minimum Size Series (Gate W/L in um)
! 4/1 4/0.8 4/0.65 4/0.55 4/0.45
D-5 Length Series (Gate W/L in um)
! 100/100 100/25 100/5 100/2.5 100/1
D-6 Length Series (Gate W/L in um)
! 100/0.75 100/0.6 100/0.55 100/0.5 100/0.45
D-7 Width Series (Gate W/L in um)
! 100/5 25/5 10/5 6/5 4/5
D-8 Minimum Size Series (Gate W/L in um)
! 4/1 4/0.8 4/0.65 4/0.55 4/0.45
3. Parasitic MOS & BJT Transistors (D-9 to D-9)
D-9 MOS Transistors (All W/L = 100um/100um)
! N+ Poly / Field Oxide/ P-Well
! Metal / Field & LTO / P-Well
! P+ Poly / Field Oxide / N-Sub
! Metal / Field & LTO / N-Sub
D-10 BJT Transistors (10um x 10um emitters, 4um base width)
! N+ Active / P-Well / N-Sub
! N+ Active / P-Well / N+ Active
! P+ Active / N-Sub / P-Well
! P+ Active / N-Sub / P+ Active
4. MOS Capacitors (D-11)
D-11 (Gate W/L in um)
! Metal / Field & LTO / P-Well (500/500)
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! Metal / LTO / N+ Poly (500/500)
! N+ Poly / Field Ox / P-Well (500/500)
! N+ Poly / Gate Ox / P-Well (100/100)
! Metal / Field & LTO / N-Sub (500/500)
! Metal / LTO / P+ Poly (500/500)
! P+ Poly / Field Ox / N-Sub (500/500)
! P+ Poly / Gate Ox / N-Sub (100/100)
5. Diodes (D-12 to D-15)
D-12 (N+ Active / P-Well Diodes)
! 250um x 250um Area Diode
! 50um x 50um Area Diode
! 10um x 10um Area Diode
! 10 fingers x 5um x 500um Edge Diode
D-13 (P+ Active / N-Substrate Diodes)
! 250um x 250um Area Diode
! 50um x 50um Area Diode
! 10um x 10um Area Diode
! 10 fingers x 5um x 500um Edge Diode
D-14 (P-well / N-Substrates Diodes)
! 250um x 250um Area Diode
! 50um x 50um Area Diode
! 10um x 10um Area Diode
! 10 fingers x 5um x 500um Edge Diode
D-15 (P+ Poly / N+ Poly Diode)
! 10um wide diode (thickness is poly thickness)
Process Test Structures
1. Contact Chains (P-1 to P-2)
P-1 Tap after 10, 100 contacts
! Metal to N+ Active
! Metal to P+ Active
P-2 Tap after 10, 100 contacts
! Metal to N+ Poly
! Metal to P+ Poly
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2. Sheet Resistivity Structures
All 4-point probes are 10um wide and distance between the two inner voltage probes is
300um, except where noted. All van der Pauw structures are 50um in diameter.
P-3 Sheet Resistivity Structures
! N+ Active 4-point probe and van der Pauw
! P+ Active 4-point probe and van der Pauw
! N+ Poly 4-point probe and van der Pauw
P-4 Sheet Resistivity Structures
! P+ Poly 4-point probe and van der Pauw
! P-well under gate oxide and poly 4-point probe and van der Pauw
! P-well under gate oxide with N+ pinch 4-point probe and van der Pauw
P-5 Sheet Resistivity Structures
! P-well under field oxide 4-point probe and van der Pauw
! Metal 4-point probe (10um x 30,000um)
3. Kelvin Structures
P-6 Metal to N+ Active
! 4um x 4um, 2um x 2um, 1.5um x 1.5um, 1um x 1um contacts
P-7 Other Contact Resistance Probes
! Metal to N+ Active (Transfer Length Method; contacts spaced 10um, 20um, 40um, 80um, and
160um apart)
! Metal to P+ Active (2um x 2um contact only)
! Metal to N+ Poly (2um x 2um contact only)
! Metal to P+ Poly (2um x 2um contact only)
4. Continuity Structures + Integrated SEM structures
P-8 Continuity Structures
Left Column
! N+ Active (4 x 5000)
! P+ Active (4 x 5000)
! N+ Poly (0.5 x 5000)
! P+ Poly (0.5 x 5000)
! N+ Poly over Active steps (0.5 x 5000)
! P+ Poly over Active steps (0.5 x 5000)
! Metal (0.5 x 5000)
Right Column
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! Metal over N+ Active & Poly tilted at 5º (0.5 x 5000)
! Metal over all horizontal N+ topography (0.5 x 1200)
! Metal over all vertical N+ topography (0.5 x 1200)
! P-Well in Active region (1 x 2000)
! P-Well in Field region (1 x 2000)
P-9 SEM structures
! NMOS
! PMOS
5. Isolation Structures
P-10 Isolation Structures (4um spacing between 4um-wide fingers)
Left Column
! N+ Active
! P+ Active
! N+ Poly
! P+ Poly
! N+ Poly over N+ Active Stripes
! P+ Poly over P+ Active Stripes
Right Column
! Metal
! Metal over N+ Active Stripes
! Metal over N+ Active Region
! Metal over N+ Poly Stripes
! Metal over N+ Poly Region
Circuit Structures
C-1 CMOS Inverters
! (W/L)NMOS = 8/2, (W/L)PMOS = 4/2
! (W/L)NMOS = 8/2, (W/L)PMOS = 8/2
! (W/L)NMOS = 8/2, (W/L)PMOS = 16/2
! (W/L)NMOS = 8/2, (W/L)PMOS = 32/2
! (W/L)NMOS = 8/2, (W/L)PMOS = 64/2
Fabrication Test Structures
Layer Thicknesses
F-1 Field Oxide over N-Substrate
F-2 Gate Oxide over N+ Active
EE 312 NMOS LOCOS Student Manual
Page 28 of 52 Revision Date: Jan. 2018
F-3 Gate Oxide over P+ Active
F-4 N+ Poly over Field Oxide
F-5 P+ Poly over Field Oxide
F-6 N+ Poly over Gate Oxide
F-7 P+ Poly over Gate Oxide
Exposure Resolution & Alignment Structures
F-8 Field Oxide Resolution
F-9 P-well to Field Oxide Vernier, P-well Resolution
F-10 Poly Gate to Field Oxide Vernier, Poly Resolution
F-11 N+ Doping to Poly Gate Vernier, N+ Doping Resolution
F-12 Contact to Poly Gate Vernier, Contact Resolution
F-13 Metal to Contact Vernier, Metal Resolution
F-14 N-well to Field Oxide Vernier, N-well Resolution (Not used in EE410)
F-15 P+ Doping to Poly Gate Vernier, P+ Doping Resolution (Not used in EE410)
F-16 (For future use) Vernier to metal
F-17 (For future use) Vernier to metal
F-18 (For future use) Vernier to metal
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Research Structures
R-1 NMOS Length Series (Gate W/L in um)
! 4/100 4//25 4/10 4/6 4/4
R-2 NMOS Length Series (Gate W/L in um)
! 4/1 4/0.8 4/0.65 4/0.55 4/0.45
R-3 PMOS Length Series (Gate W/L in um)
! 4/100 4//25 4/10 4/6 4/4
R-4 PMOS Length Series (Gate W/L in um)
! 4/1 4/0.8 4/0.65 4/0.55 4/0.45
R-5
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12 APPENDIX B: Pad Assignments
Pad Assignments
NMOS LENGTH SERIES
D-1
W/L = 100um / 100um
W/L = 100um / 25um
W/L = 100um / 5um
W/L = 100um / 2.5um
W/L = 100um / 1um
D-2
W/L = 100um / 0.75um
W/L = 100um / 0.6um
W/L = 100um / 0.55um
W/L = 100um / 0.5um
W/L = 100um / 0.45um
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
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NMOS WIDTH SERIES NMOS MINIMUM SIZE SERIES
D-3
W/L = 100um / 5um
W/L = 25um / 5um
W/L = 10um / 5um
W/L = 6um / 5um
W/L = 4um / 5um
D-4
W/L = 4um / 1um
W/L = 4um / 0.8um
W/L = 4um / 0.65um
W/L = 4um / 0.55um
W/L = 4um / 0.45um
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
GATE
DRAIN
P-WELL
SOURCE
![](asset-20.png)
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PMOS LENGTH SERIES
D-5
W/L = 100um / 100um
W/L = 100um / 25um
W/L = 100um / 5um
W/L = 100um / 2.5um
W/L = 100um / 1um
D-6
W/L = 100um / 0.75um
W/L = 100um / 0.6um
W/L = 100um / 0.55um
W/L = 100um / 0.5um
W/L = 100um / 0.45um
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
![](asset-21.png)
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NMOS WIDTH SERIES NMOS MINIMUM SIZE SERIES
D-7
W/L = 100um / 5um
W/L = 25um / 5um
W/L = 10um / 5um
W/L = 6um / 5um
W/L = 4um / 5um
D-8
W/L = 4um / 1um
W/L = 4um / 0.8um
W/L = 4um / 0.65um
W/L = 4um / 0.55um
W/L = 4um / 0.45um
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
GATE
N-WELL
DRAIN
SOURCE
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EE 312 NMOS LOCOS Student Manual
Page 34 of 52 Revision Date: Jan. 2018
PARASITIC MOSFET
All W/L = 100um/100um
D-9
N+ Poly /
Field Oxide/
P-Well
Metal / Field
& LTO / P-
Well
P+ Poly /
Field Oxide /
N-Sub
Metal / Field
& LTO / N-
Sub
GATE
SOURCE
/N-WELL
DRAIN
N/C
GATE
SOURCE
/N-WELL
DRAIN
N/C
SOURCE
/N-WELL
GATE
N/C
DRAIN
SOURCE
/N-WELL
GATE
N/C
DRAIN
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EE 312 NMOS LOCOS Student Manual
Page 35 of 52 Revision Date: Jan. 2018
BIPOLAR JUNCTION TRANSISTORS
Base Width = 4um
Emitter Area = 10um x 10um
D-10
N+ Active / P-Well / N-Substrate
N+ Active / P-Well / N+ Active
P+ Active / N-Substrate / P-Well
P+ Active / N-Substrate / P+ Active
POLY MASK
BASE
COLLECTOR
EMITTER
POLY MASK
BASE
COLLECTOR
EMITTER
POLY MASK
BASE
COLLECTOR
EMITTER
POLY MASK
BASE
COLLECTOR
EMITTER
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EE 312 NMOS LOCOS Student Manual
Page 36 of 52 Revision Date: Jan. 2018
MOS CAPACITORS
500um x 500um for 3 rows
100um x 100um for last row
D-11
Metal / Field & LTO
/ P-Well
(500um x 500um)
Metal / Field &
LTO / N-Sub
(500um x 500um)
Metal / LTO / N+
Poly
(500um x 500um)
Metal / LTO / P+
Poly
(500um x 500um)
N+ Poly / Field Ox /
P-Well
(500um x 500um)
P+ Poly / Field Ox
/ N-Sub
(500um x 500um)
N+ Poly / Gate Ox /
P-Well
(100um x 100um)
P+ Poly / Gate Ox /
N-Sub
(100um x 100um)
GATE
P-WELL
GATE
N-WELL
GATE
N-WELL
GATE
N-WELL
GATE
P-WELL
GATE
N-WELL
GATE
P-WELL
GATE
N-WELL
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DIODES (1/2)
D-12
N+ Active / P-Well
Area Diode (250um x 250um)
Area Diode (50um x 50um)
Area Diode (10um x 10um)
Edge Diode
(10 fingers x 5um x 500um)
D-13
P+ Active / N-Substrate
Area Diode (250um x 250um)
Area Diode (50um x 50um)
Area Diode (10um x 10um)
Edge Diode
(10 fingers x 5um x 500um)
P-WELL
N+
ACTIVE
P-WELL
N+
ACTIVE
P-WELL
N+
ACTIVE
P-WELL
N+
ACTIVE
P+
ACTIVE
N-SUB
P+
ACTIVE
N-SUB
P+
ACTIVE
N-SUB
P+
ACTIVE
N-SUB
![](asset-26.png)
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DIODES (2/2)
D-14
P-Well / N-Substrate
Area Diode (250um x 250um)
Area Diode (50um x 50um)
Area Diode (10um x 10um)
Edge Diode
(10 fingers x 5um x 500um)
D-15
P+ Poly / N+ Poly
Area Diode (250um x 250um)
P-WELL
N-SUB
P-WELL
N-SUB
P-WELL
N-SUB
P-WELL
N-SUB
P+ POLY
N+ POLY
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EE 312 NMOS LOCOS Student Manual
Page 39 of 52 Revision Date: Jan. 2018
SHEET RESISTIVITY (1/2)
All 4-Point Probes (4PP) are 10um x 300um
All van der Pauw structures (VDP) are 50um in diameter
P-3
N+ Active 4PP
N+ Active VDP
P+ Active 4PP
P+ Active VDP
N+ Poly 4PP
N+ Poly VDP
P-4
P+ Poly 4PP
P+ Poly VDP
P-Well 1 4PP
P-Well 1 VDP
P-Well 2 4PP
P-Well 2 VDP
P-Well 1: Gate Oxide & Poly on top
P-Well 2: Gate Oxide with N+ Pinch
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
VDP-1
VDP-4
VDP-2
VDP-3
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
VDP-1
VDP-4
VDP-2
VDP-3
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
VDP-1
VDP-4
VDP-2
VDP-3
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
VDP-1
VDP-4
VDP-2
VDP-3
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
VDP-1
VDP-4
VDP-2
VDP-3
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
VDP-1
VDP-4
VDP-2
VDP-3
![](asset-28.png)
EE 312 NMOS LOCOS Student Manual
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SHEET RESISTIVITY (2/2)
All 4-Point Probes (4PP) are 10um x 300um, except where noted
All van der Pauw structures (VDP) are 50um in diameter
P-5
P-Well 3 4PP
P-Well 3 VDP
Metal 4PP
(10um x 30,000um)
P-Well 3: Field Oxide on top
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
VDP-1
VDP-4
VDP-2
VDP-3
I-1 FORCE
I-2 FORCE
V-1 SENSE
V-2 SENSE
N/C
N/C
N/C
N/C
N/C
N/C
N/C
N/C
N/C
N/C
N/C
N/C
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EE 312 NMOS LOCOS Student Manual
Page 41 of 52 Revision Date: Jan. 2018
CONTACT CHAINS STRUCTURES
Tap after 10, 100 contacts
P-1
Metal to
N+ Active
Metal to P+
Active
P-2
Metal to
N+ Poly
Metal to P+
Poly
100 contact
100 contact
10 contact
10 contact
start
start
100 contact
100 contact
10 contact
10 contact
start
start
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EE 312 NMOS LOCOS Student Manual
Page 42 of 52 Revision Date: Jan. 2018
KELVIN CONTACT STRUCTURES
P-6
Contact to N+ Active (4um x 4um)
Contact to N+ Active (2um x 2um)
Contact to N+ Active (1.5um x 1.5um)
Contact to N+ Active (1um x 1um)
P-7
Contact to N+ Active (TLM)*
Contact to P+ Active (2um x 2um)
Contact to N+ Poly (2um x 2um)
Contact to P+ Poly (2um x 2um)
*TLM: Transfer Length Method. See EE410 CMOS Manual for measurement tips. The
lengths denote distance between START pad and current pad. The order of pads on the
structure is START – A – B – C – D – E.
K-1
K-2
K-3
K-6
K-5
K-4
K-1
K-2
K-3
K-6
K-5
K-4
K-1
K-2
K-3
K-6
K-5
K-4
K-1
K-2
K-3
K-6
K-5
K-4
A-10um
C-70um
E-310um
START
B-30um
D-150um
K-1
K-2
K-3
K-6
K-5
K-4
K-1
K-2
K-3
K-6
K-5
K-4
K-1
K-2
K-3
K-6
K-5
K-4
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EE 312 NMOS LOCOS Student Manual
Page 43 of 52 Revision Date: Jan. 2018
CONTINUITY STRUCTURES
P-8
N+ Active
(4 x 5000)
Metal over N+
Active & Poly
tilted at 5º
(4 x 5000)
P+ Active
(4 x 5000)
Metal over all
horizontal N+
topography
(4 x 1200)
N+ Poly
(0.5 x 5000)
Metal over all
vertical N+
topography
(4 x 1200)
P+ Poly
(0.5 x 5000)
P-Well in Active
region
(2 x 2000)
N+ Poly over
Active steps
(0.5 x 5000)
P-Well in Field
region
(2 x 2000)
P+ Poly over
Active steps
(0.5 x 5000)
Metal
(4 x 5000)
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
N/C
N/C
COMB A
COMB B
N/C
N/C
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EE 312 NMOS LOCOS Student Manual
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ISOLATION STRUCTURES
Two interpenetrating combs, each consisting of 15 4um x 300um stripes with 4um
spacing between stripes
P-10
N+ Active
Metal
P+ Active
Metal
On
N+ Active Stripes
N+ Poly
Metal
On
N+ Active
P+ Poly
Metal
On
N+ Poly Stripes
N+ Poly
On
N+ Active Stripes
Metal
On
N+ Poly
P+ Poly
On
P+ Active Stripes
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
COMB A
COMB B
N/C
N/C
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EE 312 NMOS LOCOS Student Manual
Page 45 of 52 Revision Date: Jan. 2018
CIRCUITS
C-1
CMOS INVERTERS
N/P = WNMOS / WPMOS
L = 2um for all devices (NMOS & PMOS)
N/P = 8um / 4um
N/P = 8um / 8um
N/P = 8um / 16um
N/P = 8um / 32um
N/P = 8um / 64um
VDD
OUT
IN
GND
VDD
OUT
IN
GND
VDD
OUT
IN
GND
VDD
OUT
IN
GND
VDD
OUT
IN
GND
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EE 312 NMOS LOCOS Student Manual
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RESEARCH
NMOS
N-Channel MOSFET shorted
R-1
W/L = 4um / 100um
W/L = 4um / 25um
W/L = 4um / 5um
W/L = 4um / 2.5um
W/L = 4um / 1um
R-2
W/L = 4um / 0.75um
W/L = 4um / 0.6um
W/L = 4um / 0.55um
W/L = 4um / 0.5um
W/L = 4um / 0.45um
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
GATE
DRAIN
N/C
SOURCE
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EE 312 NMOS LOCOS Student Manual
Page 47 of 52 Revision Date: Jan. 2018
PMOS
P-Channel MOSFET shorted
R-3
W/L = 4um / 100um
W/L = 4um / 25um
W/L = 4um / 5um
W/L = 4um / 2.5um
W/L = 4um / 1um
R-4
W/L = 4um / 0.75um
W/L = 4um / 0.6um
W/L = 4um / 0.55um
W/L = 4um / 0.5um
W/L = 4um / 0.45um
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
SOURCE
N/C
GATE
DRAIN
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EE 312 NMOS LOCOS Student Manual
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R-5
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EE 312 NMOS LOCOS Student Manual
Page 49 of 52 Revision Date: Jan. 2018
13 APPENDIX C: Agilent B1500 User Manual
13.1 Standard Operating Procedure
0. Turn on the LCD monitor
1. Launch EasyEXPERT
Click ‘Start EasyEXPERT’ button and wait until the EasyEXPERT main screen or
workspace selection screen is displayed.
2. Create Workspace (if you don’t have one yet)
Enter the name of the new workspace into the above-entry field. Check Allow other users
to access this workspace box if you want to create a public workspace that is opened for
all users.
If you are the owner of the existing workspace, you can change the name of the existing
workspace. If you want to rename the existing workspace, enter the name into the below-
entry field.
3. Select Workspace
Select your own existing Workspace
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EE 312 NMOS LOCOS Student Manual
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4. Contact Probe Tips to your device contact pad
5. Perform Measurement
I. Click the Classic Test tab on the main screen. The tab is in the leftmost column on the screen.
II. The I/V Sweep Channel Setup screen is displayed. Set the Channel Setup parameters.
III. Click the Measurement Setup tab and set the parameters
IV. Click the Display Setup tab and set the parameters
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EE 312 NMOS LOCOS Student Manual
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If you set the List display, those data can be saved later
V. You can save the parameter setup by pressing the button Save on the right side. You can also
retrieve the setup by pressing the button Recall on the right side later.
VI. Click Auto Scale if needed
If you prefer to use in a different mode please read the following manuals:
I. Agilent Technologies B1500A Semiconductor Device Analyzer User’s Guide
II. Agilent Technologies B1500A Semiconductor Device Analyzer Self-paced Training Manual
You can find those from the following website:
http://www.home.agilent.com/agilent/product.jspx?nid=-34161.536905585.00&lc=eng&cc=US
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EE 312 NMOS LOCOS Student Manual
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6. Save/Retrieve Data & Graphs
I. Copy Data
Make sure you have set the List display properly
II. Copy Graph
Displayed graph can be saved directly to bmp, tiff etc file format.
If you want to store your data & graph in this system, make your own directory under
d:/user/”yourcoralID”
7. Use USB memory stick to get your data from this system (computer).
8. Exit the EasyEXPERT and turn off the monitor when you are done.