SOIL MOISTURE PROFICIENCY SAMPLE PROGRAM SHA 730 X SHRP P 619

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Acknowledgments
Abstract
Summary of Research
Appendix I--Descriptive test results on materials used by AMRL for samples
Appendix II--AMRL report on SHRP Moisture Content Proficiency Sample Program
Appendix III---Correspondence regarding transmitting AMRL report
Appendix IV--Correspondence concerning analysis of data
Appendix V--Memorandum on variance component analysis
Appendix VI--Example of report distributed to each participant
Appendix VII--AASHTO/ASTM format precision statements

SHRP-P-619

Soil Moisture Proficiency

Sample Program

Garland W. Steel, P.E.

Steel Engineering, Inc.

Strategic Highway Research Program

NationalResearch Council

Washington,DC 1993

PUBL. NO. SHRP-P--619

Program Manager: Neil Hawks

Production Editor: Marsha Barrett

Program Area Secretary: Cindy Baker

February 1993

key words:

base course aggregates

cohesive soils

Strategic Highway Research Program

National Academy of Sciences

2101 Constitution Avenue N.W.

Washington, DC 20418

(202) 334-3774

The publication of this report does not necessarily indicate approval or endorsement of the findings,

opinions, conclusions, or recommendations either inferred or specifically expressed herein by the National

Academy of Sciences, the United States Government, or the American Association of State Highway and

Transportation Officials or its member states.

350/NAP/293

Acknowledgments

The research described herein was supported by the Strategic Highway Research

Program (SHRP). SHRP is a unit of the National Research Council that was authorized

by section 128 of the Surface Transportation and Uniform Relocation Assistance Act of

1987.

°°°

Contents

Acknowledgments .................................................. iii

Abstract ........................................................... vii

Summary of Research ................................................ 1

Appendix I--Descriptive test results on materials used by AMRL for samples ....... 5

Appendix II--AMRL report on SHRP Moisture Content Proficiency Sample Program 13

Appendix III---Correspondence regarding transmitting AMRL report ............ 103

Appendix IV--Correspondence concerning analysis of data ................... 107

Appendix V--Memorandum on variance component analysis .................. 113

Appendix VI--Example of report distributed to each participant ............... 135

Appendix VII--AASHTO/ASTM format precision statements ................. 143

Abstract

This report describes the developmentofthe Long-Term Pavement Performance (LTPP)

soil sample selection process based on the American Association of State Highway

Transportation Officials (AASHTO) model. Lab results present the bias in determining

moisture content in cohesive soil and base course aggregate samples.

vii

SUMMARY OF RESEARCH

FINAL RESEARCH REPORT

on the

SHRP SOIL MOISTURE PROFICIENCY SAMPLE PROGRAM

One element of QualityAssurance (QA) for laboratory testing that

was deemed to be of key importance by SHI_P, as a resultof Expert

Task Group (ETG) recommendations, is the American Association of

State Highway and Transportation Officials (AASHTO) accreditation

program (AAP) for laboratories. All laboratories providinglong

term pavementperformance (LTPP) testingservices were required

to beaccredited by AAP. Most ofthe laboratorytests on LTPP

fieldsamples were addressed by the AAP, which includes onsite

inspections of equipment and procedures,and participation in

applicable proficiency sample series. However, a few critical

tests in the SHRP LTPP studies were not fully addressed. After

extensive consultation and careful study,it was determined that

supplemental programs should be designed to provide assurance of

quality testdata in a manner similar to that provided by AAP for

other tests.

The Soil Moisture Proficiency Sample Program was one of the

supplemental programs approved for implementation. The program

was designed to provide precision and bias data concerning

standard tests for moisture content of subgrade soils and base

course aggregates.

The soil moisture program was modeled after the familiar AASHTO

Materials Reference Laboratory (AMRL) proficiency sample

programs at the National Institute of Standards and Technology

(NIST). The moisture samples were prepared and distributed to

participants, the raw test data was collected and collated, and a

report documentingthe program was issued for SHRP by the AMRL.

Two different cohesive soils were supplied for the program by the

Maryland Department of Transportation's Materials Laboratory.

These soils were from the same sources that were used in the Type

II Soil Proficiency Sample Program. Soil classification data is

contained in appendix I.

Two different base course aggregates were supplied for the

program by the University of Nevada-Reno. The aggregates were

from the same sources that were used in the Type I Proficiency

Sample Program. It is also noted that these materials were

obtained from SHRP reference material sources,Watsonville

Granite at Monterey, California and Kaiser at Pleasonton,

California. Classification data for the materials used is

contained in appendix I.

AMRL thoroughly blended, then split each of the four primary

materials into two approximately equal parts,one part to

eventually provide material for dry samples and the other part to

eventually provide material for wet samples. Each of these 8

parts was then split again into two approximately equal portions

designated as split A and split B. Each of the 16 splits(8 A and

8 B) was then split to yield 64 test samples. 8 of the sets of

64 samples were finally processed for distribution in an air

dried condition and the other 8 sets were processed for

distribution in awet condition.Finally, 20groups of3test

samples each were randomly selected from each of the 16 sets of

64 test samples and identified for shipment to each participating

laboratory. Every participant received a total of 48 test

samples (16 groups of 3test samples each).

All samples were selected and identified in accordance with

statistically acceptable random procedures. The entire

experiment was designed in consultation with SHRP statisticians

to allow a completecomponents of variance analysis to be

conducted as resources allowed.

Instructions to the participants (appendix II,page 7) provided

directions concerningtest sequencing,identification and

procedure to follow (AASHTO T265).

Raw test data was returned to AMRL for collation and

incorporation into the AMRL report(appendix If). The report was

forwarded to the SHRP Quality Assurance Engineer when all data

had been received. It was then transmitted to the SHRP

Statistician for analysis and determination of test precision and

bias.

The Statistician's report (appendixV) provides a full

explanation of the data analysis alongwith complete information

derived therefrom.

Precision statements (appendix VII) were drafted in the standard

AASHTO\ASTM format for use by standards writingcommittees as

they deem appropriate.

The appendices to this report contain the complete set of

supportingdocuments for this program as listed in the table of

contents.

Seventeen (17) laboratories participated in this experiment.

Each participant has made a substantial contribution to the

successful completion of SHRP research in the LTPP program.

The participants are listed in Appendix II, page 11.

APPENDIX I

SHA-73 0-32

\REVISED 3-75 MATERIALSAND RESEARCH

LaboratoryWorksheet

COMBINED HYDROMETER, SIEVE ANALYSIS AND TEST DATA SHEET

o_ LOG NO.= /../(2. 728c'f CONTRACT=/40- 2(72 - ZO7- "7"7fFIELD CLASS: .a,__ _ ,/?.f.

c, LOCATION - STA. (_7_ _ So /5o '/TT. I# g'_/_( DEPTH:. O,& '7o

E_.

EST. MOIST.: /4 OPT. MOIST.DATE: 6-5- 9o CUT _ FILL rl NC/NF []

OPERATOR _.-7_ DATE G,-?o-90CHECKED BY _, _ DATE /;/7e/'_-

CLASSIFICATION : MSMT/_.(t'.7 ")('- AASHO/_ .C ¢_ _ EST. C.B.R. VALUE

LIQUID LIMIT D: 3"-- SHRINKAGE LIMIT: /_ SHRINKAGE'} 95%T-180

PLASTICITY INDEX: //. SHRINKAGE RATIO: /,"7_ r-I FACTOR j" 98% T- 99

MOISTURE DENSITY_[_-180 C MAX.DEN.= pcfOPT. MOIST.=%

RELATIONS Jr'IT-99 MAX. DEN. = pcf OPT. MOIST. = %

GRADATION (PERCENT PASSING by WEIGHT)PERCENT OFSOIL MORTAR

2_'. _z" _'? #40 "7/ *COARSE SAND:(2.0- 0.42ram) /_ l _G

<_2" 3/o" ,_60(p3 _FINESAND: (0.42- O.075mm) Z-_ J

r_ lY_"_4_ =riO0 --%-_ SILT=(0.075-0.005mm)

I" //00 _I 0 8_/==200 ¢/'7 "CLAY =(0.005 -0.001 ram) _ __/

34- 9"?#30 #270 COLLOIDS,(O.OOImm Minus) J_

MOISTURE AT ( )=%( ); MOISTURE AT ( )=%( )

I-I ORGANIC TEST=%, [] P.H. , [] OTHER TESTS._-_t_ _ _.-(.- 7

[] COLOR rl C.B.R. %, ( ),r-i VOL. CHANGE %

REMARKS;_- "f-_. ,,'_/_ ._olc S'[,_/L / 7/7/o/_[ ,_77-h'.I._ k.'cC_:_t¢

I]_24 Hr.Bath [] MSMT El=_40Wash El _200 Wash [] No Bath Required

MECHANICAL ANALYSIS DATA

o'(Wo) 23./2-TEST SAMPLE

(We)- ?__i__ .... W=x I00 +(% HYGRO =Ws

"" (W,)2_, xlOO+Ws = _'-I% HYGROWo= 3-,3_. /? W== _,.._

SEDIMENTATION TEMP I I(R/Ws)XlO0 EST.MAX.

_RA_ 'COARSE SAND

__ STA.T Jw,NOF HCT R[%CLAY"SlZEmm P_,I0 - P_40 =/_

m CFINE SAND_

/..oo_ Pp40 - Pp200=

FINE SIEVE ANALYSIS NOMENCLATURE

WHERE, Pp=Wp X I00 Pp I0=100 MAX.

Ws _AIN WHERE :

u)IS_ZE

% TOTAL mm

__ SIEVE w,= ._j.<_'P_ ;: s/'oo%A,_L(_ASS Wo=Air Dry (gin)

t--W, = Oven Dry (gm)

_-50 w, -- 0.60 W,'= WaterWt. (gin)

w_= ¢H = HydrometerReading

J " C = Tamp.Correction Factor

<_: -#'40w_ -- _ _./

(J w_'_= _.7_ _'_ 03 _:_7_ ._7 7/0.425 R=Corrected Hydrom. Reading

•PR= % Setup.Retained onSieve

#60 w,-- 3"-_Pp=%Sample Passing Sieve

w,= 37._-<" "7/._ (_ * 7Z _'_' ('_ o.2_o

- W== Wt. RetainedonSieve (gin)

-#'lO0 w,-- _ ._,/S ='%Total Sample Passing

w,= 3_'.'/?--(..1. D..{:I:G_ . g7 550.150 # I0 Sieve

w, -- _.D_ W_= Wt Possing Sieve (gm)

#z_o ,,= 2?._3_<3_73:_54 ._7 =..7 o.o7_

w,-- 0.053

LOG.NO. /JO • lze,-?24 HOUR HYDROMETER ANALYSIS

P=-_s X I00 d =dI=K,xKGx K.

WHERE ; WHERE :

'_P= % Soil in Suspension d = Corrected GrainDiameter

..J

:D R=Corrected Hydrometer Readingd, = Max.Groin Die. UnderAssumedConditions

rr a =Constant -Depending on Specific Gravity KL=Correction for Elevation of Hydrometer (H)

OWs=OvenDry Weight of Test Sample KG= Correction for Variationof Specific Grovity

H = Hydrometer Reading, Uncorrected. K.= Correction for Variation ofViscosityof

C = Correction Factor for Temperature Suspending Medium.

S= % Total Sample Passing#10Sieve

S, = % Totol Somple Passing

o = (_._ Ws= 5_..E_ %Total Sample Passing #10(S} _7 Sp. Gr. 7.. _7

OBS. T

TEMPoF ( H + C = R ) IOOo = Px S/IO0= S, i KL x KG K.

! Ws TIME MIN.d, =

I-30 .o811

_L_ _/.._ _- 21 I .057o4o

o ._ z z(,-.3 /_z3 q7.ct_'?,... @_ . o_ i .o3_.

5 .o26 ._'_'c ,o,.q"7.'1.o:j

<7.;- 3_'.o-5._- zq._, yEz-37

..J

.Ji

<o 7;27.5-S.'__2.¢ . ,_.3 3_"_5 .or5 i.e___ .0¢4# 1.0/?.-:

60 .0074 I " O'_.obT/ ',.o_C-2I

_I" Zl . O i_ i ;i i

_<._ l)_-.u z_.P -_,/ 250 1.0036 .8-_.'.o_3.EI.oo3/]

!- ' I !

7¢¢e_ i-_.(-[/_.'/I.'_=3i;,=.*_

MECHANICAL ANALYSIS (AASHO DESIGNATIONS M146 AND T.88}

U.S. STANDARDSIEVE SIZE THYDROMETER ]

,oo -_ "_ --_"_ "_ _ _ :_ =_ =_ _" :_ _" to

90 i ' "_ hO

li!I ; , z

BO:-7_.'_..•,.2C

"tO , 1 ''' .... ' ' '3C

so' '_,' = ' .,;c,-_

_0 50 5C >-

I!I'i,_ m

_. ,80

I0_- ,' I190 _

I{'_'00

-- _ e_ _r 0 _ o _ o Qvoo o

GRAIN SIZE INMILLIMETERS

COARSEIMEOUMt.,.E COARSEI.,.E SILT

% SOIL MORTAR=READINGFROMCURvE+S/Io0 REMARKS:O.O0--C _--27. d-- ,q.,7-._31

-.,"

,-r'Al._•=,_

SHA-730-32

REVISED 3-7_MATERIALSAND RESEARCH

Loborotory Worksheef

COMBINED HYDROMETER, SIEVE ANALYSISANDTEST DATA SHEET

o_ A A-)_r #

LOG NO.: CONTRACT' r"/J// FIELD CLASS:

uLOCATION - STA. DEPTH:

EST. MOIST.'OPT. MOIST. DATE'CUT[] FILL [] NC/NF []

__ OPERATOR/..'r _ DATE 3 -I _, -_0CHECKED BY _._=_ DATE ,,_-z/-?o

CLASSIFICATION : MSMT "_ AASHO/,"-_ EST. C.B.R. VALUE /

LIQUID LIMIT [] : _'_/SHRINKAGE LIMIT= _" SHRINKAGE_95%T-180

PLASTICITY INDEX://" SHRINKAGE RATIO: /. /_ i_ r-i FACTOR J" 98% T- 99

MOISTURE DENSITY_Ig_-180 _- MAX. DEN.= _7/._tpcfOPT. MOIST. = 3/.g" %

RELATIONS JnT-g9__ MAX. DEN. =pcfOPT. MOIST. =%

GRADATION (PERCENTPASSING by WEIGHT) _(PERCENT OFSOIL MORTAR

12_:_z" "40 *COARSE SAND ' (2.0-0.42mm) ._ _)_)

_'8"_e60 _ *FINE SAND=(0.42- O.075mm) 7. _ t

1Y="w48100 73_ SILT : (0.075 - O.O05mm ) =/5

I" ,_I 0 /0 L_ =200 (_ _ "CLAY: (0.005 - 0.001 mm)

_-_/,"#30 #270COLLOIDS_(O.OOImmMinus)

MOISTURE AT__ ( )=__.%(); MOISTURE AT__( )=%()

r-I ORGANIC TEST: %, I'1 PH. , I-I OTHER TESTS =_/o _p.Z. 73

[] COLOR rl C.B.R %, ( ),E3 VOL. CHANGE %

REMARKS:

2B_4 Hr. Bath r-; MSMT El _40 Wash r'l +200 Wash [] No Bath Required

MECHANICAL ANALYSIS DATA

9! '(W=)_(=,. 3._ .... TEST SAMPLE

_! CW,)-'" _'_i"'_"_" WaX100 lHYGRO+I00)= W,

= (W,) .'7#xlOO ¨DhZ?% HYGRO Wo= .._'.E._Z/W== _.3-_"

_[ SEDIMENTATION [TEMP H-I C IR (R/Ws)XIO0 EST'"AX"

o.*'. "COARSE SAND

START llllN.°F T % CLAY" S/ZmE Pp IO- Pp 40= -/

i/.oo5P,40 -P,200=

FINE SIEVE ANALYSIS NOMENCLATURE

WHERE' P_= _ X I00 PpI0=100 MAX.

=_A,, WHERE :

SIZE

(nSIEVE *,";PP ::s/Ioo .s_u.pt.=pAs_ Wo = Air Dry(cjm)

W, = Oven Dry (gin)

<w, -- W, "= Water Wt. (gin)

.J _30 0.60

:3 wp=H=HydrometerReading

o¢

..J C =Tamp• Correction Factor

<#4o *--'- Lt,'tC,

iwp" L(? _ _ I /_:1: _/ /.0 _/0425R : Corrected Hydrom. Reading- - P_ = % S_mp.Retained on Sieve

*._ -- _ .3/P_= % SamplePassing Sieve•W= = Wt. Retained onSieve (gin)

#_oo ,,-- _ __0S=% Total Sample Passing

'_"_o z_,"T_ e)O :_ 7_f.o 7So.,50 _elO Sieve

" " Wp = WtP_ssin9 Sieve(gin)

#200 ._ -- (. ?//

'_"3_ .'_7_. _-_ , (.o7.- f.G G_"oo7s

-_270 w, -- 0.053

LOG.NO. /_rT._ .-F _24 HOUR HYDROMETER ANALYSIS

P = _XlO0 d = dlxKLxK_x K.

WHERE :WHERE:

<1 P =% Soil in Suspension d = Corrected Groin Diameter

R=Corrected Hydrometer Reading d, =Max. Grain Did.UnderAssumedConditions

a=Constant -DePendingon Specific Gravity KL= Correction for Elevation ofHydrometer (H)

_i W== Oven Dry Weight of Test Sample Ks.-- Correction for Variation of Specific Gravity

"1H=Hydrometer Reading,Uncorrected. K. =Correction for Variation of Viscosity of

C=Correction Factor for Temperature Suspending Medium.

S= % Total Sample Passing#10 Sieve

S, = % Total Sample Passing

a = O. _ W_= _3._:_C"%Total Sample Passing#10(S)/dO Sp. Gr. 2..'/.-_

[ ! j j I MIN.I I ) I

TEMP. (H + C = R) x IOOo =pxS_IO0=S, OBS. T d, x KLx K_K. =d

-tTIME i t

°FIW,I r

'I'I

3o_. .osiI,I I

/ I ii- , .027 I I

7.'7;_.o-_,._-.o26i._z_t .o_7 !.o_-_

;[I- ''

.I,!I

I i-'I

-_?.l_';.oI-".:,'_';I ,,7._!rr Go .oo74,._i._==?oo_.II

! ' ' i

_o Io.oi/o.dlozso .oo_6!.15o .do33

' i _ i

I'i

MECHANICAL ANALYSIS(AASHO DESIGNATIONS M.146 AND T.88]

U.SSTANDARD SIEVE SIZE IHYDROMETER1

I00 0

ll!t!I I I; t !I: _ Iii I_ _1 I _"----_!1111:1Ii _ I ;!:1 Ii!!ti! i I! t ! I! , liiii1!i + _,,, _ -

_ _o_:i;_,,__.1_ _4o__"

t I I

;i;i i I ii !!1i'Ii,_I!tl,%. '_

,• , ',=;=

= !1!!! !! ! ..t! !1 I I i;_ z.

'°li!!, ii_ _li li 1 J: i[!i___i =

!iliIi: .i i _', ,, _IIII III I -_,oc

,,,_ _ o _ _ o

-_GRAIN SIZE INMILLIMETERS

GI_AVEL_AN[) II1COARSE MEDIUM tFINE COARSE 1FINE SILT CLAY

%SOIL MORTAR-READINGFROMCURVE+_o0 REMARKS: O.OID_ _ /(_.8 _', I.(_ _1, t'7

SHRPPROFICIENCY SAMPLES

FOR RESILIENT MODULUS TESTING

OF UNBOUNDED MATERIAL

(Gradation)

__ii!ii iiiiii:i_iiiii:iiii:iiii]iililii!_i:i_!iiiiii_i_:ii!iiiii!iii!!iiii_:ii i!iii!ii!iiiiil!!_ _:

:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::

1.5" 100

r' 82

3/4" 73

1/2" 61

3/8" 52

#4 39

#8 27

#16 21

#30 15

#50 10

#100 8

#200 6

AASHTO Soil Classification Unified Soil Classification

A-l-a GW-GM

PLASTIC INDEX

Material Identification Specific Gravityof Specific Gravity of

Material Passing #4 Material Retained on #4

WatsonviUe 2.777 2.865

Pleasonton 2.713 2.748

APPENDIX II

SHRPMoisture Content

Proficiency Sample

Program

S.H.1LP. Moisture - Content Proficiency Sample Program

CONTENTS

Correspondence Document

The correspondance document that wasmailedto the 17 laboratories participating

in the S.H.R.P. Moisture Content Proficiency SampleProgram, consists of an

Instruction page, a copy of the Standard Test method, and a Data sheet to be used

for recording testresults.

* Although only 17 complete samples weredistributed by AMRL, (17 laboratories

participated in the Proficiency Sample Program) 20 completesamples were

prepared, leaving 3 complete samples toserve as replacements in case of loss or

damage during shipment. As a result, the following report reflects the in-house

data recorded for 20 complete samples. (A complete sample is defined as 16 Sets

of 3 sub-samples each, with oneSet coming from eachof the 16 Sample Types).

Section 1 - Master Identification Record

Laboratory Identification Sheet

This sheet identifies each laboratory participating in the program. Each

laboratory was assigned a number which is used to identify and trace the

laboratories data.

TestSample Splitting Procedure

Thisdocument illustrates the process used to split the material fromthe Split

A or Split B portion to yield 64sub-samples. Each ofthe 4 Primary materials was

blended and then splitinto 2 approximately equal portions. Each of these

portions was then split to yield 2 portions,onehalfbeingidentified as Split

A, and the otherhalf being identified asSplit B. Each ofthe splits,(SplitA

or Split B) was then split toyield 64sub-samples. Each laboratorywas shipped

3 randomly selectedsub-samplesfromthe 64sub-samples. (3 sub-samples

constitute one Setfor a particular material type.

Sample TTpe Identification Sheet

This document describes the attributes of each of the 16 different sample types.

It also identifies the four primary materials that were used to in preparing the

samples. Eachlaboratory was shipped one set, (3sub-samples) from each of the

16 Sample Types.

Each Sample Type is described by the following criteria:

* Primary material type. (Aggregate 1 or Aggegate 2, Soil 1 or Soil 2)

* Which half of the split the sample originated from. (Split A or Split B)

* Moisture condition of the material. (Air dry, Plastic Limit or Saturated

Surface Dry.

Toapproximate the plasticlimitorsaturatedsurface dry condition, the

following moisture contents were added to the air dry samples:

*Aggregate 1 --> 2.00 ! .04% moisture.

* Aggregate 2 --> 3.00 _ .04% moisture.

* Soil 1 --> 15.00 ± .04% moisture.

* Soil 2 --> 25.00 ± .04% moisture.

Laborator7 Sub-Sample Identification Sheet

These sheets identify the 3randomly selectedsub-samples that were assigned to

each laboratory for a particular sample type. The sub-samples thateach

laboratory received are identified bysample type number and the letter a, b or

c on the data sheets. The sheets also identify the proper set testingsequence

for that set of 3 sub-samples. The numbers were assigned usingthe Lotus random

number generator function.

Example: For Sample Type No. I, Laboratory No. 1 was assigned sub-sample No.'s

12, 42 and 57. These 3 sub-samples are identified as Sample#'s la, ib and Ic

respectively. These 3 sub-samples were labeled Set #II,meaningthat from the

total group of 16 sets received by the laboratory, Sample Type No. 1 would be

the eleventh set tested.

Laboratory Set Testln K Sequence Table

This table shows the Set TestingSequence for all of the laboratories. There is

acolumn for each sample type and arow for each laboratory.

Section 2 - Master Data Record

Master Data Record

These are the data tables used to record the mass and the amount of moisture

added to the sub-samples prepared by AMRL. These data sheets may be compared with

the Returned DataSheets shown in Section3.

Section 3 - Returned Data Sheets

Returned Data Sheets

These datasheets were filled out by participating laboratories and returned to

AMRL.

Returned Tare Weights

*Note that Laboratory No. 's3, 7, 9, 10, Ii, 13 and 19 did not comply with the

request to record the tare weights of the bags on the back of the DataSheet.

* When comparingthe respective masses of the sub-samples on the Master Data

Shee_s with the masses of the sub-samples submitted from the laboratories on

the Returned Data Sheets, it appears that some of the laboratories may nothave

used the entire sub-sample when testingfor moisture content.

Errors in processing

Notei:Laboratory No. 15 receivedtwo sets identified as Set _I.The Set

containing Sub-Samples 9a, 9b and 9c was inadvertantly identifiedasSet #I when

it should havebeen Set #3.The situation was explained to the laboratory prior

to testing and is considered resolved.

Note 2: Laboratory No. II, Set 8,Sample 9b hadanexcessive amount of moisture

added to the sample. This error is reflected in the laboratories returned data

sheet.

Gregory V.Uherek, AMRL Research Associate

October, 1990

Correspondence Document

Date

Name of laboratory manager

Laboratoryname and address

Subject: SHRPMoisture ContentProficiency TestSamples

Dear (insert name):

SHEPhas engaged theAASHTO Materials ReferenceLaboratory to prepareand distribute

proficiency test samples for moisturecontentdetermination. In connection withthis effort,

we are sending two boxescontaining16 setsofmaterial to your laboratory.Each set of

material isidentified with a Set Number from 1 to 16 and contains three double-bagged test

samplesidentified with a Sample Number. The twoboxes you receiveshould contain forty-

eighttestsamples (16 sets containing3 samples each).

Please determine the moisture content of each sample in accordance with Section 5 of AASHTO

T265-86. A copy ofthis standard is attached for your convenience. Test each set

individually and in numerical order according to theSet Number(i.e. Begin testingwith Set

Number 1 and end testingwith SetNumber 16.). Donotopen the bags containingatest sample

until the testsample is ready to be tested. Opening the sample bags too soonmayaffect the

moisture contentof the samples.

Please use the enclosed data sheet to record your testresults. (Additional copiesof this

letter, test method T265 and the data sheethave been included in each boxofmaterialbeing

sent to your laboratory.)Set and Sample Numbers have been entered in the appropriate

columns on the data sheetand are exclusive to your laboratory. Record all weightstothe

nearest0.I gand calculate and report the moisturecontent to thenearest 0.01%. After

testingrecord the weight ofthe bagcontainingeach sample and the applicable Setand Sample

Number onthe back ofthedata sheet.

Please testall samples assoon as possible, butnolater than thirtydaysafter receipt, and

return a completed data sheet: GregoryUherek, AASHTO MaterialsReferenceLaboratory,

Building226, RoomA365,Gaithersburg, Maryland 20899.

Ifyou have anyquestions, orifthesamples received are damaged or incomplete,please

contactGreg Uherek at (301)975-6704.

Sincerely,

Peter A.Spellerberg, Assistant Manager

AASHTOMaterials Reference Laboratory

Enclosures

Z_"

z_- ._o _ tiff fl _ _

Section 1

Master Identification Record

S.H.R.P.MOISTURE CONTENT PROFICIENCY SAMPLE PROGRAM

ParticipatingLaboratories

Braun Engineering Testing, Inc.

Minneapolis, Minnesota55435

CaliforniaDepartmentof Transportation

Sacramento, California 95819

Federal Highway Administration

Denver,Colorado80225

Florida Departmentof Transportation

Gainesville, Florida 32602

Iowa Departmentof Transportation

Ames,Iowa50010

Kansas Department of Transportation

Topeka, Kansas 66611

Law Engineering

Atlanta, Georgia 30324

MarylandState Highway Administration

Brooklandville, Maryland 21022

Minnesota Department of Transportation

Maplewood,Minnesota55109

Nevada Departmentof Transportation

Carson City, Nevada 89712

Oregon State Highway Division

Salem, Oregon 97310

PSI

Pittsburgh, Pennsylvania 15220

Southwestern Laboratories

Houston, Texas 77249

Texas State Departmentof Highways and

Public Transportation

Austin, Texas 78731-6033

University of Nevada-Reno

Reno, Nevada 89557-0030

WestVirginia Departmentof Transportation

Charleston, WestVirginia 25311

Western Technologies Inc.

Phoenix, Arizona 85036

i-:,

I.T.i

r-i,

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-- !{l,,

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i.l.I

r..T.l,,_

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f..l.I

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S.H.R.P. Moisture Content Proficiency Sample Program

Sample Type Identification Sheet

SAMPLE TYPE NO. SAMPLE DESCRIPTrlON

1........................................... Aggregate 1, Split A, SSD Condition

2........................................... Aggregate 1, Split B, SSD Condition

3........................................... Aggregate 2, Split A, SSD Condition

4........................................... Aggregate 2, Split B, SSD Condition

5........................................... Aggregate 1, Split A, Air Dry Condition

6........................................... Aggregate 1, Split B, Air Dry Condition

7........................................... Aggregate 2, Split A, Air Dry Condition

8........................................... Aggregate 2, Split B, Air Dry Condition

9........................................... Soil 1, Split A, Plastic Limit Condition

10.......................................... Soil 1, Split B, Plastic Limit Condition

11.......................................... Soil 2, Split A, Plastic Limit Condition

12.......................................... Soil 2, Split B, Plastic Limit Condition

13.......................................... Soil 1, Split A, Air Dry Condition

14.......................................... Soft 1, Split B, Air Dry Condition

15.......................................... Soil 2, Split A, Air Dry Condition

16.......................................... Soil 2, Split B, Air Dry Condition

PRIMARY

MATERIALS USED

Aggregate1 - Watsonville, Supplied by University ofReno, Nevada

Aggregate2 - Pleasonton, Supplied by University of Reno, Nevada

Soil 1 - **, Supplied by the Department of Highways, Maryland

Soil 2 - **, Supplied by the Department of Highways, Maryland

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO. 1

Aggregate No. 1, Split A, Saturated - Surface - Dry Condition

_EMAINDERS: 23, 22,40, 63

,.. ,_ ,. , '_._i_ _ ,,_'_"_; ,

S.H.ILP. Moisture Content Proficiency Sample Program

LaboratorySub-SampleIdentificationSheet

SAMPLE TYPE NO.2

Aggregate No. 1, Split B, Saturated-Surface - Dry Condition

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.3

Aggregate No. 2,SplitA, Saturated - Surface - Dry Condition

S.H.R.P. Moisture Content Proficiency Sample Program

LaboratorySub-SampleIdentificationSheet

sa_eze nee NO.4

AggregateNo. 2, Split B, Saturated -Surface- Dry Condition

i:!_i:i_:_i:i:_:_:i:i:_:i:i_i:i:i:!_!:i:_:i:i:i:i:_:!:!:!:i:i:_:_:i:_:_j:i:i:i:i:_:i:i:i:i:i:i:i:_:i:i:_:i:i:i:i:_:i:_:i:i:_:_:!:_:i:_:_:i:_:_i:_:!:_:_:i:_:_:_:i:_:i_:_:i_i_i_!_i:i_i_i_i_i:i_i:i:i_i:!_!_i_i_i_:!:i:_3_i:_:_!:_:!:!:_:_:i:_:_:_:_:_:i:_:i:_:i:i:i:i:!:i:i:i:i:!:i:i:i:i:i:i:i:i:!:!_!:i:!:i:j:i:_:_:i`._:_:_:_:i:i:i:i:_:i:i:i:_:!:i:i:i:i:i:i:i_i:i_:i:j:i:i:i:i:i:!:i:!:_:i:i:i:!:!:i:i:_:[:i:_:_:_:_:i:i:_:_:_:_:_:_:i:_:_:i_:i:i:i:_:_:_:_:i:_:_:::::::::::::::::::::::::::::::::::i:i:i:i:i:i:i_i:i:i:i:i_.:.:.:.:.:.:.:.:.:.:._:.:_.:+::.:

_%EMAINDERS : 31,52,5,54

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.5

AggregateNo.1, SplitA, Air- DryCondition

REMAINDERS:56, 53, 62,50

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.6

AggregateNo. 1,Split B,Air - Dry Condition

REMAINDERS : 57, 63, 42, I0

S.H.R.P. Moisture ContentProficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.7

AggregateNo. 2, Split A,Air - Dry Condition

iiiiiiiiiiiiiiiiii!iiiiiiiiiiiiiiiiiiiii_i_iiiiiiiiiiiiii!iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii_giiiiiiiii21i!i!!ii!iiiiiiii[iiiiiii_ iii i_ i _ i iilii _ii 1

REMAINDERS : 13, 63, 14,3

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.8

Aggregate No. 2,SplitB,Air-DryCondition

i:_:i:i:i:_:_:i:!:!:::i:i:i:i:!:_8_:!:!:i:i:!:!:i:i:_:i:!:i:i:i:_:i:i:_:_:i:_:i:i:_:i:i:i:_:_:i:i:i:_:i:i:i:!:i:i:_:i:_:i:i:!:_:::::::::::::::::::::::::_:_:i:£!:i:_:!:_:_:!:i:_:i:i:_:_:_:_:_:_:_:3:i:_:_:!:_:_:_:_:_:i:i:i:i:i:_:i:_:i:i:_:!:_:_:_:!:!:!:_:_:i:_:!:!:i:!:_:i:i:i:_:!:_:_:_:_:_:_:i:i:_:i:33i:_:!

REMAINDERS:54, 30, 63, 46

S.H.ILP.Moisture Content Proficiency Sample Program

Laboratory Sub-SampleIdentification Sheet

SAMPLE TYPE NO.9

Soil No. 1, Split A, Plastic- Limit Condition

i:i:i:_:i:i:_:i:i:.:_:i:i:::::::::::::::::::::i::i:J:i:_:!:i:i:_:i:i.i:i:i:_:!:i:!::i:i:i:i:i:i:i:i:i:i:i:!:i:i:i:_:_:_:_:!:i:i:i:::?:i:i:_:i:_:i:i:i:i:i:i:i:_::i:!.i:i:i.i:i:i:i:i:i:i::_:i:i:i:i:i:i:i:_:i.i:_:i:!:i:i:J:i:!:i:i:_:i:i:i:_:_:i:_:_:i:i.3:_:_:i:_:i:_:i:_:_:i:i:i:_:_:i:_',i:!:_:!:!:!_i:i:i:i:i:i:_:_:i:_:i:_:i:_:_:i:_:i:!:_:i:_:i:J:_:i:i:i:i:i:!:_:i:i:i:_:i:i:i:i:i_:_:i:i:i:i:i:i:J:i:_:i:J:_:!:_:i:_;_:_:i:_:_:_:_:i:i:i:::::::::::::::::::::::::::::::::::::::::::_:i:i:_:i:i:i:::i:i:!:i:i:i:i:i:i:i:_:_:!:i:::!:ii:i:::::::::::::::::::::::::::i:i:::

ZEMAINDERS :21, 22, 36,6

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.10

Soil No. 1, Split B,Plastic - Limit Condition

_EMAINDERS : 45, 64, 49, 15

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.I1

Soil No. 2, Split A, Plastic - Limit Condition

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.12

Soil No. 2, SplitB,Plastic -Limit Condition

REMAINDERS: 26, 2, 47, 37

S.H.R.P. Moisture ContentProficiency Sample Program

LaboratorySub-SampleIdentification Sheet

SAMPLE TYPE NO.13

Soil No. 1, SplitA,Air - Dry Condition

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-SampleIdentification Sheet

SAMPLE TYPE NO.14

Soil No.1, Split B,Air - Dry Condition

REMAINDERS : 55, 17, 33, ii

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO.15

Soil No. 2,Split A, Air - Dry Condition

S.H.R.P. Moisture Content Proficiency Sample Program

Laboratory Sub-Sample Identification Sheet

SAMPLE TYPE NO. 16

Soil No. 2, SplitB, Air - Dry Condition

REMAINDERS : 50, 64, 33, 46

Section 2

Master Data Record

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Returned Tare Weights

LAB No. 1

SET # SAMPLE BAG WT. SET # SAMPLE BAG WT.

1 5 A 7.8 13 2 A 7.3

B 7.7 B 7.6

C 7.3 C 7.4

2 3 A 7.1 1416 A 7.9

B 7.6 B 7.9

C 7.7 C 7.9

312 A 7.7 1511 A 8.3

B 8.1 B 8.2

C 8.5 C 7.9

4 13 A 7.1 16 7 A 7.2

B 7.1 B 7.6

C 7.0 C 7.3

5 4 A 9.7

B 8.2

C 9.1

615 A 7.4

B 7.9

C 7.5

7 14 A 7.7

B 7.3

C 7.4

8 9 A 8.3

B 8.0

C 7.7

910 A 7.4

B 7.6

C 7.7

10 6 A 7.4

B 7.7

C 7.7

11 1 A 7.6

B 7.4

C 7.1

12 8 A 7.7

B 7.6

C 7.1

LAB No. 2

1. 9a-8.5 14.10a-8.3

9b-7.6 10b-8.5

9c-8.1 10c-8.1

2. 3a-7.4 15. lla-9.1

3b-7.7 11b-8.9

3c-7.411c-8.2

3. 16a-7.9 16. 5a-7.2

16b-7.9 5b-7.6

16c-7.8 5c-7.8

4. 12a-8.4

12b-8.0

12c-8.1

5. 13a-7.3

13b-7.5

13c-7.6

6. 8a-7.9

8b-7.9

8c-7.8

7. 15a-8.0

15b-7.6

15c-7.5

8. 2a-7.1

2b-7.2

2c-7.8

9. 14a-7.4

14b-7.4

14c-7.5

10. la-7.2

lb-7.4

lc-7.4

11. 7a-7.6

7b-7.2

7c-7.3

12. 4a-8.5

4b-7.8

4c-8.0

13. 6a-7.4

6b-7.4

6c-7.5

LAB No.4

SAMPLE # BAG WEIGHT SAMPLE # BAG WEIGHT

10 A 8.08 6 A 7.20

B 7.60 B 7.24

C 7.57 C 7.31

3 A 7.60 1A 7.15

B 7.28 B 7.43

C 7.17 C 7.10

9 A 7.37 16 A 7.40

B 7.67 B 7.33

C 7.24 C 7.76

13 A 7.07 11 A 8.17

B 7.03 B 8.45

C 7.40 C 9.02

7 A 7.59

B 7.52

C 7.27

8 A 7.34

B 7.23

C 7.22

15 A 7.38

B 7.78

C 7.71

2 A 7.51

B 7.05

C 7.48

12 A 7.87

B11.41

C7.90

5 A 7.36

B 7.61

C 7.36

14 A 7.61

B7.18

C 7.22

4 A 7.67

B7.86

C7.66

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102

APPENDIX I,II

October 17, 1990

Robin High

TRDF

2602 Dellana Lane

Austin, TX 78746

Dear Robin:

Subject: SHRP Soil Moisture Proficiency Sample Program.

Enclosed is a report which summarizes implementation activities

to date concerningthe subject program. All test data sheets

are contained under the blue page titled Section 3,Returned Data

Sheets. Information needed to construct the data array for a

components of variance analysis as previously discussed is

contained in other sections of the report.

Please proceed with the analysis as soon as possible. As

indicated in the past,participating laboratories should be

identified only by a number in the final report compiled for

distribution tointerested parties.

Call me if anythinghas been overlooked or further elaboration is

needed. I will review the analysis report upon receipt and

contact you by telephone if questions arise.

Yours very truly

Garland W. Steele, P.E.

President, Steele Engineering, Inc.

enclosure: SHRP Soil H20 Proficiency Sample Report

cc: Adrian Pelzner (letteronly)

105

Box 173 • Tornado, West Virginia 25202 • Tele. (304) 727-8719

APPENDIX IV

January ii,1991

Virgil Anderson

48 Oaks Place

Lago Vista,TX 78645

Dear Virgil:

Subject: SHRP Soil Moisture Proficiency Sample Program.

This will confirm the substance of telephone discussions with

Robin duringthe past few days concerning the format for

presentingprecision data which can be determined from the

analyses now underway of test data from the subject program.

The most desirable approach is to use a format that is generally

used by AASHTO and ASTM. Examples are contained in ASTM C670,

Standard Practice for PreparingPrecision and Bias Statements for

Construction Materials. For example, if the analysis yields an

estimate of 2.1%for _ within laboratories by single operators,

the statement could read-

Precision-The within laboratory single operator standard

deviation has been found to be 2.1%.A Therefore, results of

two properly conducted tests by the same operator in the

same laboratory on the same soil with the same moisture

content should not differ by more than 5.94%.A

AThese numbers represent,respectively,the IS and D2S

limits as described in ASTM Practice C670, for Preparing

Precision Statements for Test Methods for Construction

Materials.

The data available from the subject program will, of course,

yield considerably more information concerning the components of

variance and, as discussed with Robin,will hopefully allow an

estimate of bias to be determined.

As originally discussed during the design of this program, the

within sample variance could be quantified by comparing the odd

numbered (i through 63) samples to the even numbered (2 through

64) samples for each of the 16 sample types. The between sample

variance could be quantified by comparing the first two samples

(I and 2) of each group of four samples to the second two samples

(3 and 4) of the same group of four etc. for all 16 groups of

four in each of the 16 sample types. Likewise, the within

material-same condition variance can be quantified by comparing

the 64 samples from split A to the 64 samples from split B for

each of the 8 pairs of A and B splits.

Box 173 • Tornado, West Virginia 25202 • Tele (304) 727-8719 1 09

In addition,the within material-different condition variance of

variances could be quantified by comparing the variance of the

128 samples from sample types I and 2 to the variance of the 128

samples from sample types 5 and 6 and similarly for each of the

other three sets. Further the between material-same condition

and the between material-different condition variance of

variances could be quantified in a similar manner.

Each of the above would provide valuable insight to SHRP and to

other researchers and practitioners concerning a necessary and

widely used test procedure.

Enclosed is a copy of a proposed revision to ASTM D2216 which

Adrian suggested should be made available to you and Robin for

information. Note particularly section 13on page ii of the

proposed revision. Apparently, SHRP results will provide

information of considerable interest to those responsible for

such standards.

Please call if you have further suggestions or ifmy terminology

needs clarification.

I appreciate very much your and Robin's efforts to expedite the

statistical analyses necessary to allow the highest and best use

of data now available from this program.

Yours very truly

Garland W.Steele, P.E.

President, Steele Engineering Inc.

enclosures: 12 pages

cc: Robin High

Adrian Pelzner (letter only)

Bill Hadley (letter only)

110

February 7, 1991

Virgil Anderson

48 Oaks Place

Lago Vista, TX 78645

Dear Virgil:

Subject: SHRP Soil Moisture Proficiency Sample Program.

This will confirm the substance of a previous telephone

discussion with Robin concerning an "AMRL style" scatter diagram

report to be distributed to the participants in the subject

program.

Enclosed, as promised, is a copy of some information concerning

such reports. It is my understanding, based on discussions with

AMRL, that the quadrants are now formed by intersecting mean

lines rather than intersecting median lines. Also, that

laboratory results eliminated (last paragraph of attachment) are

those results outside the 3a limits of the data as calculated

using all results. The remaining results are then recalculated

and no further eliminations are made.

Such a report would only be compiled after the currently

scheduled analyses are completed.

Please let me know if there are any questions or recommended

modifications to the above.

Yours very truly

Garland W.Steele

President, Steele Engineering, Inc.

cc: Adrian Pelzner(letter only)

Bill Hadley(letter only)

Box 173 • Tornado, West Virginia 25202 • Tele. (304) 727-8719 111

APPENDIX V

TECHNICAL MEMORANDUM

TRDF SHRP • LONG TERM PAVEMENT PERFORMANCE PROGRAM

TECH MEMO: AU-181 ._,_/DATE: June12,1991

AUTHOR: Robin High _&/_L_ FILE: P-O01

DISTRIBUTION: Garland Steele, Bill Hadley

SUBJECT: Variance Components and Bias Estimation for SHRP Moisture Content

Proficiency Sample Program

This memorandum s-mmarizes the test results from the analysis of the SHRP

moisture content proficiency sample program. When a test procedure is applied

repeatedly to a set of identical material samples the same results rarely

occur. An experimental design was structured to evaluate this variability

when testing both aggregate and soil material samples for moisture content.

Its purpose is to present the within-laboratory and between-laboratory

variance components estimated from the data collected during this experiment.

The different factors of the experiment which represent sources of

variability and how the materials were to be processed in each laboratory were

originally developed as Design 4 in Technical Memorandum AU-95 (Ref I). The

analysis of data from these designs were described in Technical Memorandum

AU-108 (Ref 2). The word "material" in this analysis represents both

aggregate and soil samples and will be used throughout this report to refer

to the applicable type of sample.

Due to the lack of an accepted reference value, an estimate of the amount

of bias in the testing procedure for moisture content in the samples has not

previously been evaluated. This study presents a unique opportunity to

estimate the amount of bias due to the moisture measurement process. Results

corresponding to this portion of the study will also be provided.

DATA DESCRIPTION

A brief description of the data is included in this report for

completeness. Further details are available in the AMRL report (Ref 3). In

this document a description of the experimental design, testing procedures,

2602DelIanaLane Austin,Texas • Telephone 512/327-4211 • Fax512/328-7246

11S

and and a list of all of the data provided by AMRL collected by the 17

laboratories who participated in the experiment were provided.

Twotypes of material were used in the experimental plan (aggregates and

soils). For both aggregates and soils, material from two different sources

was acquired for the study. At each of the two levels of the factor

representing the source of the material (MATL) the batch was randomly split

into two portions (A or B).

For one-half of each split, moisture was added to the samples; the

remaining samples were air dried. One level of the moisture factor refers to

the Saturated Surface Dry (SSD) condition for aggregates and Plastic Limit

(PLM) condition for soils. The other level for each material refers to the

air dry condition.

Table i gives a brief summary the factors in the design. Sixteen

different types of samples were created and then shipped to the laboratories.

Sample numbers i through 4 refer to aggregates in the wet condition and

samples 5 through 8 refer to aggregates in the dry condition. Sample numbers

9 through 12 refer to soils in the wet condition and 13 through 16 refer to

soils in the dry condition. Each laboratory received 3 sets of the nearly

identical subsamples from each of the sixteen samples processed by AMRL.

Since the magnitude and the variability in the test results for soils was much

larger than for aggregates, two separate analyses for each type of material

will be given.

VARIANCE COMPONENT ANALYSIS

The experimental plan was developed to estimate the variance components

associated with testing the moisture content of both aggregate and soil

samples. Three replicate sets of material samples for each combination of the

design factors were provided to the seventeen laboratories.

The analysis phase for the determination of moisture content first

creates an analysis of variance table (ANOVA). The results are then used to

116

Table I. Factor levels and sample type identification.

FACTOR DESCRIPTION TYPE OF EFFECT

MST Moisture Fixed

MATL Material Fixed

LAB Laboratory Random

SAMPLE

TYPE NO. SAMPLE DESCRIPTION

AGGREGATES

SSD Condition

i .......................... Aggregate i, Split A

2 .......................... Aggregate i, Split B

3 .......................... Aggregate 2, Split A

4 .......................... Aggregate 2, Split B

Air Dry Condition

5 .......................... Aggregate I, Split A

6 .......................... Aggregate I, Split B

7 .......................... Aggregate 2, Split A

8 .......................... Aggregate 2, Split B

Aggregate I: WA - Supplied by University of Reno, Nevada

Aggregate 2: PL - Supplied by University of Reno, Nevada

SAMPLE

TYPE NO. SAMPLE DESCRIPTION

SOILS

Plastic Limit Condition

9 .......................... Soil i, Split A

i0 .......................... Soil i, Split B

Ii .......................... Soil 2, Split A

12 .......................... Soil 2, Split B

Air Dry Condition

13 .......................... Soil I, Split A

14 .......................... Soil i, Split B

15 .......................... Soil 2, Split A

16 .......................... Soil 2, Split B

Soil i: MI - Supplied by Department of Highways, Maryland

Soil 2:M2 - Supplied by Department of Highways, Maryland

117

estimate the magnitudes of the between- and the within-laboratory testing

variations (a2L,S and 02respectively) for both types of materials.

Estimation of the Variance Components

The experimental design under which the data were collected has a direct

impact on how the statistical analysis should proceed. The statistical model

used to summarize these data takes the following form:

MSTLAB - _ + MST + MATL + LAB + SPLT(MATL) + ERROR

The terms MST, MATL, and SPLT(MATL) remove the variability due to the

planned moisture content and material type. This allows more accurate

estimates of the random variation due to laboratories (LAB) and the random

variation due to other unknown factors (ERROR).

Tables 2 and 3 provide the Analysis of Variance (ANOVA) tables for the

results. From these summary statistics the two variance components

representing the between-laboratory (_LAB) and the within-laboratory (0"2)

components are estimated and appear in the lower portion of the tables.

Differences Among Means

Tables 2 and 3 are also used to identify the laboratories which produce

statistically different results from other laboratories. The average test

results from each laboratory are presented in a column and are ranked from

largest to smallest. Groups of laboratory means are underlined to indicate

which ones are not statistically different from one another. The averages to

be most concerned with are those which lie on either end of the row. If one

continuous line does not appear underneath these averages, there is evidence

to suggest the mean from that laboratory exceeds the two standard deviation

control limits and does not conform with the remainder of the data.

The mean results from laboratory 17 for aggregates appears to be

considerably smaller than the means from the other laboratories. A closer

118

Table 2.Variance component analysis for aggregate samples.

Degrees of Sum of Mean

Source Freedom Squares Square F Value Pr > F

....................................................................

Model 18659.049 36.6138 470.41 0.0001

MST i 614.220 614.2196 7891.49 0.0001

MATL I 43.343 43.3428 556.87 0.0001

LAB 16 1.486 0.0929 1.19 0.2699

Error 385 29.966 0.07783

Corrected Total 403 689.015

Variance Components

OaLAB= 0.0006345

02 =0.07783

Student-Newman-Keuls test for variable: MSTLAB

Means with the same underline are not significantly different.

SNK Grouping Mean LAB

1 5937 09

1 5583 07

1 5562 01

1 5467 04

1 5467 12

1 5438 15

1.5246 16

1.5221 05

1.5208 02

1.5154 06

1.5096 08

1.4974 14

1.4909 13

1.4871 03

1.4817 i0

1.4379 Ii

I1.1677 17

119

Table 3. Variance component analysis for soil samples.

Degrees of Sumof Mean

Source Freedom Squares Square F Value Pr > F

.....................................................................

Model 18 66999.245 3722.180 292.19 0.0001

MST I 45014.471 45014.471 3533.67 0.0001

MATL I 21723.755 21723.755 1705.33 0.0001

LAB 16 261.019 16.314 1.28 0.2059

Error 388 4942.622 12.739

Corrected Total 406 71941.867

Variance Components

CY2LAB-- O.1493

a2=12. 739

Student-Newman-Keuls test for variable: MSTLAB

Means with the same underline are not significantly different.

SNK Grouping Mean N LAB

17.628 24 ii

17.621 23 13

17.583 24 09

17.554 24 Ol

17.390 24 14

17.354 24 07

17.301 24 02

17.252 24 04

17.154 24 08

17.017 24 03

16.780 24 16

16.598 24 15

16.255 24 06

15.932 24 17

15.904 24 12

15.388 24 i0

14.95824 05

120

examination of the raw data for this laboratory is required to determine a

reason for this difference.

PRECISION STATEMENTS FOR MOISTURE CONTENT

The within laboratory variance components for the moisture contents of

the two material types are given in Tables 2 and 3. This section provides the

within-laboratory precision statements for moisture content testing. The two

standard deviation limits for the difference between two observations are

given. These values imply that within one laboratory, a pair of measurements

selected at random will differ by more than 2 4/-_ in only 5% of all cases.

Aggregates

Precision - The within-laboratory single operator standard deviation for

aggregates is determined to be _ - J 0.07783 B 0.2790.

Therefore, results of two properly conducted tests by the

same operator in the same laboratory on this aggregate should

not differ by more than 2 4_ - 0.7891 from each other.

These numbersrepresent, respectively, theIS and D2S limits as described

in ASTMPractice C670, for Preparing Precision Statements for Test Methods for

Construction Materials.

Soils

Precision - The within-laboratory single operator standard deviation for

aggregates has been found to be _ - J 12.739 _ 3.5692.

Therefore, results of two properly conducted tests by the

same operator in the same laboratory on this aggregate should

not differ by more than 2 J 2 _ =10.0951 from each other.

These numbers represent, respectively, the IS and D2S limits as described

in ASTMPractice C670, for Preparing Precision Statements for Test Methods for

Construction Materials.

121

BETWEEN LABORTORIES PRECISION STATEMENTS FOR MOISTURE SAMPLES

The between-laboratory variance components for the moisture content of

the two material types, are given in Tables 2 and 3. This section provides

between-laboratory precision statements based on these results for resilient

modulus testing. The two standard deviations limits for the difference

between two observations from different laboratories are given. These values

imply that the difference between one measurement selected at random from each

of two laboratories will differ from each other by more than 2 _2(_LA B+02)

in only 5% of all cases.

A_EreEates

Precision - The between laboratory single operator standard deviation for

moisture content has been found to be JOaLA B + O 2=0.28012.

Therefore, the results of properly conducted tests from two

laboratories on the same aggregate should not differ by more

than 2 J2 (O2LAB + 02) -- 0.7923 from each other.

These numbers represent, respectively, the IS and D2S limits as described

in ASTM Practice C670, for Preparing Precision Statements for Test Methods for

Construction Materials.

Soils

Precision - The between laboratory single operator standard deviation for

moisture content has been found to be J_LA8+02 3.5900.

Therefore, the results of properly conducted tests from two

laboratories on the same soil should not differ by more than

2 J 2 (_2LA8+02) = 10.1541 from each other.

These numbers represent, respectively, the IS and D2S limits as described

in ASTM Practice C670, for Preparing Precision Statements for Test Methods for

Construction Materials.

122

ESTIMATION OF BIAS

The precision of the standard test method for the determination of

moisture content of aggregates and soils in a laboratory was the primary topic

of the two previous sections. These results showed the degree of mutual

agreement of individual measurements both within and across laboratories. The

accuracy of a test procedure takes the precision statements one step further.

It covers both the precision and bias of the test method. The bias of a

result, often called the systematic error, involves consistent deviations from

a reference value. That is, the mean of the test will consistently be larger

or smaller than its true value. Further explanations of precision and

accuracy can be found in the ASTM publication E177 (Ref 3).

In order to have a valid statement on the bias of a test procedure, a

reference value is required. Because data to support this requirement have

not been available no estimate of bias has ever been determined. If an

acceptable reference value for moisture content can be derived, then the data

obtained from these test results may be used in estimating the bias of the

test procedure.

The material samples, processed by AMRL, were bagged and shipped to the

participating laboratories. An important requirement for estimating moisture

content is to test the samples as soon as possible so that they do not remain

in the bags for long periods of time. They should also have been stored at

the proper temperature and kept away from direct sunlight. If any of these

conditions were not satisfied, the possible impact on the bias calculations

remains unknown.

Moisture samples constructed by AMRL were developed such that water was

added in a known quantity to one-half of the samples and no water was added

to the other half. Since no water was added to the "dry" samples, the

moisture determined by the test results in the laboratories for these samples

is the best estimate possible of the amount which occurs naturally in air-

dried material.

123

The following procedure for estimating the bias in the moisture content

test method for aggregates was followed. Each laboratory was sent 3

subsamples for each of the 8 samples of material for a total of 24 subsamples.

The only difference between sample i and sample 5 materials is the added

moisture content. The same association exists between sample pairs (2,6),

(3,7), and (4,8).

For each laboratory the average moisture content was found for the three

subsamples of material produced by AMRL for sample number i. This average was

added to the average moisture content found by each laboratory for sample

number 5. This total represents the best estimate of the average moisture

content contained in the "wet" samples. The average moisture content of the

3 subsamples for sample I as determined by the respective laboratory was

subtracted to determine a bias term. The same procedure was used for "wet"

samples 2 through 4 and "dry" samples 6 through 8.

The resulting means for the aggregate samples from the 17 laboratories

across the different levels of factors in the study are shown in Table 4. The

analysis of variance performed on these data is given in Table 5. The results

indicate that only a small amount of bias exists for the aggregate samples.

The overall average is 0.03113. This positive number indicates the

laboratories did not estimate as much water in the sample as one would have

expected to find. The individual means found in the right hand column of

Table 4 indicate most of the laboratories produced a positive bias with

laboratory ii having the largest bias of 0.1200. Another interesting result

is that material from source WA generally produced large positive results

(average - 0.0615) and material from source PL generally produced both

positive and negative results (average - 0.0007). Thus, the magnitude of the

bias depends on the source of material used.

The same procedure was also followed for the soils. Sample numbers 9

through 12 had specific amounts of moisture added by AMRL. The corresponding

pairs are given by sample numbers 13 through 16 left in the air-dry condition.

124

Table 4. _ Bias estimates for aggregate samples 1 through 8 (SSD condition).

S A

eT ............................................

L L L WA PL

A I ......................................................

B T A B C D Mean

01 0.14000 0.18000 0.08333 -0 10333 0.0750

02 0.17667 0.03667 0.16333 -0 06667 0.0775

03 0.16333 0.02667 0.04667 -0 06667 0.0425

.........................................................

04 0.04000 0.01000 0.03333 -0 13333 -0.0125

05 0.00000 0.01667 0.02667 -0 02333 0.005

.........................................................

06 0.02333 0.02000 -0.00333 -0 04667 -0.0017

.........................................................

07 -0.00333 0.09667 0.05667 -0 06667 0.0208

.........................................................

08 0.01667 0.01000 0.06333 -0 03667 0.0133

09 0.06667 0.02667 0.13333 -0 09667 0.0325

.............. , .......... ° .......... , .......... , .........

I0 0.02000 0.01000 -0.01333 -0 09000 -0.0183

.........................................................

ii 0.13333 0.15667 0.14000 0 05000 0.1200

.........................................................

12 0.10333 0.02667 0.ii000 0 01333 0.0633

I .............. ° .......... , .......... , .......... , .........

I 13 0.07333 0.10500 0.05333 -0 07333 0.0396

I 14 0.08000 0.00000 0.00667 -0 06167 0.00625

I .........................................................

I 15 0.03333 0.01333 -0.01667 -0 12000 -0.0225

I .........................................................

I 16 0.11333 0.03667 0.08333 -0 02667 0.05170

I .............. ° .......... , .......... , .......... , .........

I17 0.11333 0.02667 0.01333 -0 00667 0.03667

...........................................................

Averages 0.0761 0.0470 0.0576 -0 0562

..................... , .....................

0.0615 0.0007

...........................................

0.03113

.............................................

125

Table 5. Analysis of Variance for bias estimates in aggregate samples.

Degrees of Sum of Mean

Source Freedom Squares Square F Value Pr > F

.................................................................

Mode] 17 0.1576 0.00927 2.23 0.0143

LAB 16 0.0948 0.00592 1.43 0.1675

MATL i 0.0628 0.06281 15.14 0.0003

Error 50 0.2075 0.00415

Corrected Total 67 0.3650

Student-Newman-Keuls test for variable: BIAS

Means with the same underline are not significantly different.

SNK Grouping Mean N LAB

0.1200 4 II

0.0775 4 02

0.0750 4 01

0.0633 4 12

0.0517 4 16

0.0425 4 03

0.0396 4 13

0.0367 4 17

0.0325 4 09

0.0208 4 07

0.0133 4 08

0.0063 4 14

0.0050 4 05

-0.0017 4 06

-0.0125 4 04

-0.0183 4 I0

-0.0225 4 15

126

The resulting means for the soil samples from the 17 laboratories across

the levels of the factors in the study are shown in Table 6. The analysis of

variance performed on these data is given in Table 7. The results indicate

that a larger amount of bias exists for the soil samples, except now the

difference is the negative value of -0.9834. This negative number indicates

the laboratories overestimated the amount of water in the sample one would

have expected to find. The individual means found in the right hand column

of Table 6 indicate most of the laboratories produced a negative bias.

However, laboratory 05 has a very large positive overall bias term of 1.614.

Another interesting result is that material from source MI generally produced

positive results (average - 0.4749) and material from source M2 generally

produced large negative results (average - -2.4418). Thus, the magnitude of

the bias depends on the source of material used.

In sl,mmary, an interesting contrast emerges from these results. Bias is

positive for aggregates and therefore the laboratories did not estimate as

much water in the sample as one would have expected to find. The negative

bias for soils indicates the laboratories overestimated the amount of water

in the sample one would have expected to find. Also, for both aggregates and

soils the source of the material influenced the size and the magnitude of the

bias term.

PRECISION STATEMENTS FOR BIAS

The average laboratory bias components for the moisture contents of

aggregates and soils are given in Tables 4 and 6. These means provide the

basis for statements concerning the precision of the moisture content

estimate. The appropriate standard deviation to apply depends upon the

desired inference. Table 8 summarizes the calculations of the appropriate

mean squares. Given the data provided for this experiment, confidence

intervals for the true bias estimates will be provided.

127

Table 6. Bias estimates for soil samples 9 through 16 (PLM condition).

S A

PT.............................................

L L L MI M2

B T A B C D Mean

01 1.07667 -0.ii000 -2.70667 -3.10333 -i 2108

.............. , .......... , .......... , .......... ].........

02 1.66333 -0.39000 -3.52000 -2.65667 -i 2258

03 0.80333 0.21333 -5.23333 -3.47000 -I 9217

04 0.69667 -0.22333 -2.84667 -2.62667 -I 2500

05 0.92000 -0.07333 5.56667 0.04333 I 6142

.............. J .......... ,.......... ,.......... ,.........

06 0.80667 0.12000 -0.19667 -0.76333 -0 0083

07 1.13333 -0.04333 -3.30667 -2.95000 -i 2917

08 1.05333 -0.13333 -2.99667 -3.10000 -i 2942

09 1.52333 0.09000 -3.24000 -2.99333 -i 1550

I0 1.23333 -0.39333 -3.79000 -0.73333 -0 9208

ii 0.70000 0.19667 -3.94333 -2.97000 -i 5042

12 0.89333 0.36000 -0.26333 -0.96333 0 0067

........................................................

13 0.81000 -0.19000 -2.88667 -2.78667 -i 2633

14 I.I0000 0.67333 -2.94667 -3.29667 -i 1175

15 0.36333 -0.05000 -2.24000 -2.33667-i 0658

16 1.75667 0.33667 -4.23333 -3.87333 -i 5033

.............. ].......... i..............................

17 -0.38667 -0.38333 -4.02000 -1.63667 -I 6067

..... , .......... ........... . .......... . .......... , .........

Averages 0.9498 0.0000 -2.5178 -2.3657

..................... ......................

0.4749 -2.4418

...........................................

-0.9834

.............................................

128

Table 7. Analysis of Variance for bias estimates in aggregate samples.

Degrees of Sum of Mean

Source Freedom Squares Square F Value Pr > F

.................................................................

Model 17 188.612 11.0948 6.56 0.0001

LAB 16 43.993 2.7496 1.62 0.0966

MATL I 144.618 144.6181 85.46 0.0001

Error 50 84.6079 1.6922

Corrected Total 67 273.2194

Student-Newman-Keuls test for variable: BIAS

Means with the same underline are not significantly different.

SNK Grouping Mean N LAB

1.614 4 05

0.007 4 12

-0.008 4 06

-0.921 4 i0

-1.066 4 15

-1.117 4 14

-i.155 4 09

-1.211 40l

-1.226 4 02

-1.250 4 04

-1.263 4 13

-1.292 4 07

-1.294 4 08

-1.503 4 16

-1.504 4 ii

-1.607 4 17

-1.922 4 03

129

Table 8. Mean square calculations for the bias of aggregates and soils.

_GGREGATES

Sumof Mean

Source DF Squares Square

..............................................

Error 67 0.3650 0.005448

Corrected Total 67 0.3650

Total 68 0.4309

Sum of Mean

Source DF Squares Square F Value Pr > F

....................................................................

AGGR i 0.0628 0.06281 13.72 0.0004

Error 66 0.3022 0.004578

Corrected Total 67 0.3650

Total 68 0.4309

SOILS

Sum of Mean

Source DF Squares Square

.............................................

Error 67 273.2194 4.0779

Corrected Total 67 273.2194

Total 68338.9847

Sum of Mean

Source DF Squares Square F Value Pr > F

........ .............................................................

SOIL I 144.6180 144.6180 74.22 0.0001

Error 66 128.6013 1.9485

Corrected Total 67 273.2194

Total 68 338.9847

130

Precision Statements of Bias for Aggregates

Aggregates. Table 8 shows the within-laboratory single operator standard

deviation for aggregates is determined to be _ = J 0.005448

- 0.0738. Therefore, the bias of a properly conducted test

by one operator in the same laboratory on an aggregate

material should not differ by more than 2 o- 0.1476 from the

true value of the bias. When the experimental results were

compared with a known reference value, the 95% confidence

limits for the bias of a moisture test on an aggregate

material was found to lie between 0.0311 ± 2 a or (-0.116,

0.179).

Aggregates

from Source WA. The within-laboratory single operator standard deviation for

aggregates from source WA is determined to be a =J 0.004578

- 0.06766. Therefore, the bias of a properly conducted test

by one operator in the same laboratory on an aggregate from

this source should not differ by more than 2 _ - 0.1353 from

the true value of bias. A 95% confidence interval for the

bias of the moisture content of aggregates from this source

is 0.0615 ± 2 _ or (-0.074, 0.197).

Aggregates

from Source PL. The within-laboratory single operator standard deviation for

aggregates from source PL is determined to be a =_0.004578

= 0.06766. Therefore, the bias of a properly conducted test

by one operator in the same laboratory on an aggregate from

this source should not differ by more than 2 _ - 0.1353 from

the true value of bias. A 95% confidence interval for the

bias of the moisture content of aggregates from this source

is 0.0007 ± 2 oor (-0.135, 0.136).

These numbers represent, respectively, the IS and 2S limits as described

in ASTM Practice C670, for Preparing Precision Statements for Test Methods for

Construction Materials.

131

Precision Statements of Bias for Soils

Soils. Table 8 shows the within-laboratory single operator standard

deviation for soils is determined to be _ - J 4.0779 -

2.0194. Therefore, the bias of a properly conducted test by

one operator in the same laboratory on a soil material should

not differ by more than 2 _ - 4.0388 from the true value of

the bias. When the experimental results were compared with

a known reference value, the 95% confidence limits for the

bias of a moisture test on a soil material was found to lie

between -0.983 ± 2 _ or (-5.022, 3.056).

Soils from

Source MI. The within-laboratory single operator standard deviation for

soils from source MI is determined to be o = J 1.9485 =

1.3959. Therefore, the bias of a properly conducted test by

one operator in the same laboratory on a soil from this

source should not differ by more than 2 a = 2.7918 from the

true value of bias. A 95% confidence interval for the bias

of the moisture content of soils from this source is 0.475

± 2 aor (-2.317, 3.267).

Soils from

Source M2. The within-laboratory single operator standard deviation for

soils from source M2 is determined to be _ = J 1.9485 =

1.3959. Therefore, the bias of a properly conducted test by

one operator in the same laboratory on a soil from this

source should not differ by more than 2 a =2.7918 from the

true value of bias. A 95% confidence interval for the bias

of the moisture content of soils from this source is -2.442

± 2 O or (-5.234, 0.350).

These numbers represent, respectively, the IS and 2S limits as described

in ASTM Practice C670, for Preparing Precision Statements for Test Methods for

Construction Materials.

132

REFERENCES

I. High, R., "Materials Testing Sampling Designs", Technical Memorandum AU-

95, TRDF, December, 1989.

2. Anderson, V., "Analysis of Material Testing Sampling Designs", Technical

Memorandum AU-108, TRDF, January, 1990.

3. Uherek, G., "SHRP Moisture Content Proficiency Sample Program", AMRL,

October, 1990.

4. American Society .for the Testing of Materials, "Use of the Terms

Precision and Accuracy as Applied to Measurement of a Property of a

Material", E177, 1980.

133

APPENDIXVl

November !8_ 1991

Fred Martinez

South Western Laboratories

222 Cavalcade Street

PO Box 8768

Houston. TX 77249

Dear Fred:

Subject: SHRP Soil Moisture Proficiency Sample Program

Enclosed for your information is a copy of followingfourscatter

diagrams showing results of tests on the subject Program.

°Aggregate(SHRP Type !)-air dry condition

°Aggregate(SHRP Type I)-saturated surface dry condition

°Soii(SHRP Type II)-air dry condition

°Soii(SHRP Type II)-piastic limit condition

The vertical and horizontal lines on each diagram are the means

of the A and B samples respectively for each of the four

conditions noted above.

The test data derived by your laboratory is identified by the

letter H.

Yours very truly

Garland W. Steelej P.E.

President, Steele Engineering inc.

enclosure: 4 pages

co: Neii Hawks(letter only)

Paul Teng(letter only)

Dave Esch(ietter only)

Bill Hadley(letter only)

Robin High(letter only)

Box 173 • Tornado, West Virginia 25202 • Tele (304) 727-8719 13 7

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APPENDIXVii

Moisture Content-Aqgregates

Precision

The within-laboratory single operator standard deviation for

moisture content of aggregates has been found to be _ = A0.2790%.

Therefore, results of two properly conducted tests by the same

operator in the same laboratory on the same type of aggregate

sample should not differ by more than 2_2 a= 80.7891%from each

other.

The between-laboratory single operator standard deviation for

moisture content of aggregates has been found to be _(a21_b+a 2) =

A0.28012%. Therefore,results of properly conducted tests from

two laboratories on the same aggregate should not differ by more

than 2_(2(_21ab+a2)) = 80.7923%from each other.

These numbers represent, respectively, the AIS and _D2S limits

as described in ASTM Practice C670,Preparing Precision

Statements for Test Methods for Construction Materials.

Bias

When experimental results are compared with known values from

accurately compounded specimens:

The bias of moisture tests on one aggregate material has been

found to have a mean of +0.0615%. The bias of individual test

values from the same aggregate material has been found with 95%

confidence to lie between -0.074%and +0.197%.

The bias of moisturetests on a second aggregate material has

been found to have a mean of +0.0007%. The bias of individual

test values from the same aggregate material has been found with

95%confidence to lie between -0.135%and +0.136%.

The bias of moisture tests overall on both aggregate materials

has been found to have a mean of +0.0311%. The bias of

individual test values overall from both aggregate materials has

been found with 95%confidence to lie between -0.116%and

+0.179%.

145

Moisture Content-Soil

Precision

The within-laboratory single operator standard deviation for

soils has been found to be a = A3.5692%. Therefore,results of

two properly conducted tests by the same operator in the same

laboratory on the same type soil should not differ by more than

2_2 _ = _i0.0951%from each other.

The between-laboratory single operator standard deviation for

moisture content of soils has been found to he _(a21ab+_2) =

A3.5900%. Therefore,results of properly conducted tests from

two laboratories on the same soil should not differ By more than

2_(2(a_l_h+a2)) = Bi0.1541%from each other.

These numbers represent, respectively, the _IS and _D2S limits

as described in ASTM Practice C670, Preparing Precision

Statements for Test Methods for Construction Materials.

Bias

When experimental results are compared with known values from

accurately compounded specimens:

Thebiasof moisture tests on one soil material has been found to

have a mean of +0.475%. The bias of individual test values from

the same soil material has been found with 95%confidence to lie

between -2.317%and +3.267%.

The bias of moisture tests on a second soil material has been

found to have a mean of -2.442%. The bias of individual test

values from the same soil material has been found with 95%

confidence to lie between -5.234%and +0.350%.

The bias of moisture tests overall on both soil materials has

been found to have a mean of -0.983%. The bias of individual

test values overall from both soil materials has been found with

95% confidence to lie between -5.022%and +3.056%.

146

SOIL MOISTURE PROFICIENCY SAMPLE PROGRAM SHA 730 X SHRP P 619

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