TT 136 Pure Monomer Resins TT136
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Pure monomer resins Extending hydrogenated hydrocarbon resins with pure monomer resins in SIS-based nonwoven construction pressure sensitive adhesive formulations Technical tip Pure monomer resins Extending hydrogenated hydrocarbon resins with pure monomer resins in SIS-based nonwoven construction pressure sensitive adhesive formulations Introduction Data Nonwoven construction adhesives based on SIS-type polymers traditionally use hydrogenated hydrocarbon resins such as Eastotac™ resins as the tackifier of choice due to their compatibility, thermal stability, and hightemperature properties. Eastman has investigated the possibility of extending hydrogenated hydrocarbon resins in these types of formulations with pure monomer resins (PMRs), with results that indicate PMRs can be added up to 13% by resin volume without negatively affecting adhesive performance or thermal aging properties. Pure monomer resins offer excellent thermal stability, high-temperature resistance, and low molecular weight. Traditionally used to selectively modify the styrenic end blocks to balance cohesion and viscosity, PMRs can be effectively used in synergy with hydrogenated hydrocarbon resins in SIS-based adhesives without negatively affecting performance. Typical properties of selected hydrogenated hydrocarbon resins and PMRs are given in Table 1. Values shown are an average of typical samples and should not be interpreted as product specifications. Table 1. Typical properties of resinsa a b Ring & ball softening point (°C) Mn/Mw/Mz (Daltons) Tg (°C) Gardner color/YIDb Resins Type Eastotac™ H-100W Hydrogenated hydrocarbon resin 100 450/1000/2150 41 <1/8 Kristalex™ 3085 PMR 85 650/1150/1900 41 <1/4 Piccotex™ LC PMR 91 750/1350/2200 46 <1/8 Piccolastic™ A75 PMR 74 700/1300/2250 35 1/- Obtained from Eastman publication WA-86A, Spectrum of Hydrocarbon Resins; WA133, Eastman Hydrocarbon resins YID = Yellowness Index An SIS-based disposable diaper construction adhesive formulation was prepared with Eastotac™ H-100W hydrogenated hydrocarbon resin as the control. Effects of three different PMRs (Kristalex 3085, Piccotex LC, and Piccolastic A75) as extenders for Eastotac H-100W were evaluated at two different levels; 4% and 8% by weight (in formulation) or 7% and 13% extension with respect to the total hydrogenated hydrocarbon resin amount (Eastotac H100W:PMR, 93:7 and 87:13 ratios). Table 2 shows the formulations used in this study. Table 2. Disposable diaper construction adhesive formulations with PMRs (shown in weight %) Kristalex™ 3085 Piccotex™ LC Piccolastic™ A75 Eastotac™ H-100W control 93:7 H100W:3085 Kraton™ 1165a 20 20 20 20 20 20 20 Eastotac™ H-100Wb 59.5 55.5 51.5 55.5 51.5 55.5 51.5 Kristalex™ 3085b – 4 8 – – – – Piccotex™ LCb – – – 4 8 – – Piccolastic™ A75b – – – – – 4 8 Calsol™ 5550c 20 20 20 20 20 20 20 Irganox™ 1010d 0.5 0.5 0.5 0.5 0.5 0.5 0.5 Formulation ingredient 87:13 93:7 87:13 93:7 87:13 H100W:3085 H100W:LC H100W:LC H100W:A75 H100W:A75 a KRATON Polymers LLC (polymer) Eastman Chemical Company (resins) c Calumet Specialty Products (naphthenic oil) d BASF (antioxidant) b Study formulations were prepared using a Brabender mixer and evaluated for the following properties: • Adhesive property evaluation—1-mil-thick adhesive coating on Mylar™ • Viscoelastic properties—Using Dynamic Mechanical Analysis (DMA) – 180 degree peel on stainless steel substrate (peel rate @ 4 inches/min) • Viscosity profiles at different temperatures (before and after aging [177°C for 72 h])—Brookfield Viscometer – Loop tack on stainless steel substrate The viscoelastic performance analysis (DMA) of the PMR extended formulations at two different levels, along with the control formulation is shown in Figure 1. Figure 1. Viscoelastic properties of formulations extended with PMRs. With 4% by weight PMR (93:7 H100W:PMR) 1.E+10 10 Tg and Tan d peak value 3rd crossover temp. 1.E+08 1 1.E+07 1.E+06 Tan delta G' (dynes/cm2) 1.E+09 0.1 Tan d min. value and Tan d min. temp. 1.E+05 0.01 1.E+01 −50 −30 −10 10 30 50 70 90 110 130 Temperature (°C) Eastotac H100W control 93:7 H100W:LC 93:7 H100W:3085 93:7 H100W:A75 With 8% by weight PMR (87:13 H100W:PMR) 10 1.E+10 4° to 6°C change in 3rd crossover temp. 1 1.E+08 1.E+07 Tan delta G' (dynes/cm2) 1.E+09 0.1 1.E+06 1.E+05 0.01 1.E+04 −50 −30 −10 10 30 50 70 90 110 130 Temperature (°C) Eastotac H100W control 87:13 H100W:LC 87:13 H100W:3085 87:13 H100W:A75 As shown in Figure 1, the viscoelastic characteristics, Tg, and elastic modulus are not significantly affected by the addition of PMRs to the control formulation. The single Tg exhibited by the extended formulations is also an indication of good compatibility between the polymer and tackifiers. The only notable exception is a slightly lower melting temperature (approximately 4° to 6°C) when the formulation is extended with PMRs at the highest loading level weight (8%). Figure 2 illustrates the absolute values of important parameters such as Tg, Tan d minimum value at Tan d minimum temperature (an indication of cohesive property), 3rd crossover temperature (indication of melting temperature), and Tan d peak value at Tg (indication of tack). The only significant difference noted is for the 3rd crossover temperature with the 8% PMR extended formulations (87:13) with Eastotac™ H-100W. All other properties are comparable. Figure 2. Viscoelastic property comparison values from DMA. Tan d value comparisons Different DMA temperature properties 120 5.00 4.46 0.17 0.19 0.19 0.18 0.20 0.20 0.17 93:7 H100W:LC 93:7 H100W:A75 87:13 H100W:3100 87:13 H100W:LC 87:13 H100W:A75 4.37 4.19 4.00 94.4 92.3 92.4 98.3 94.4 94.3 98.3 80 4.49 4.22 93:7 H100W:3100 100 4.57 4.33 Tan d value 70.4 70.4 68.4 72.4 72.4 70.3 60 72.4 2.00 40 38.4 16.4 16.4 34.4 36.4 38.4 40.4 38.4 38.4 Temperature (°C) 3.00 20 1.00 14.4 16.4 18.4 16.4 16.4 0 Estotac H100W control 87:13 H100W:A75 87:13 H100W:LC 87:13 H100W:3100 93:7 H100W:A75 93:7 H100W:LC Estotac H100W control 93:7 H100W:3100 0.00 3rd crossover Tan d min. temp. Tan d peak value @ Tg 2nd crossover Tg Tan d min. value @ Tan d min. temp. Figures 3 and 4 summarize the adhesive property evaluation results, which were performed with 0.9–1-mil-thick Mylar™coated films on a stainless steel substrate. While most extended formulations exhibit similar performance to the control, a notable exception is Piccotex™ LC at 7% loading with Eastotac™ H100W. Improvement is shown in both adhesive peel and loop tack. The higher loop tack shown for Piccolastic™ A75 extended formulations can be attributed to the slightly lower softening point characteristics of Piccolastic™ A75 compared to the other PMR resins. Figure 4. Loop tack on stainless steel Figure 3. 180 degree peel on stainless steel (peel rate at 4 inches/min) 6.00 Brookfield viscosity (cps) 87:13 H100W:LC 87:13 H100W:A75 4,000 2,000 0 130 150 170 190 Temperature (°C) 210 87:13 H100W:A75 87:13 H100W:3085 6,000 7.37 93:7 H100W:A75 87:13 H100W:LC 93:7 H100W:LC 8,000 6.96 93:7 H100W:3085 87:13 H100W:3085 Eastotac H100W control 7.57 10,000 93:7 H100W:A75 Initial viscosity profiles before aging 12,000 8.28 Figure 5. Brookfield viscosity (cps) profiles of formulations at different temperatures. 93:7 H100W:LC Figure 5 illustrates there are no significant differences above 150ºC in the viscosity profiles at 5 different temperatures between the control formulation and PMR extended formulations, even after aging at 177°C for 72 h. 7.60 93:7 H100W:3085 87:13 H100W:A75 87:13 H100W:LC 87:13 H100W:3085 93:7 H100W:A75 93:7 H100W:LC 93:7 H100W:3085 Eastotac H100W control Eastotac H100W control 0.00 6.39 1.00 6.80 3.78 4.65 4.89 4.16 4.27 2.00 5.26 3.00 lb 4.00 4.74 lb/inch 5.00 10.00 9.00 8.00 7.00 6.00 5.00 4.00 3.00 2.00 1.00 0.00 Figure 6. Aging studies of the formulations at 177°C for 72 h. Initial (before aging) Initial (before aging) Aged pictures of formulations extended with 7% PMRs (93:7 H100W:PMRs) Aged pictures of formulations extended with 13% PMRs (87:13 H100W:PMRs) Depicted in Figure 6 are the before and after color-aging characteristics for both the control and PMR extended formulations, which also exhibit similar or better performance. Conclusion SIS-based nonwoven adhesive formulations that utilize hydrogenated hydrocarbon resins can be extended with pure monomer resins from 7%–13% (with respect to hydrogenated resin level) without negatively affecting the adhesive performance and thermal aging properties. Benefits include: • Improved adhesive peel and loop tack • Higher amount of PMRs gives a slightly lower viscosity and melt transition (4° to 6°C from DMA) • Good thermal stability (color and viscosity) on aging Eastman Chemical Company Corporate Headquarters P.O. Box 431 Kingsport, TN 37662-5280 U.S.A. Telephone: U.S.A. and Canada, 800-EASTMAN (800-327-8626) Other Locations, (1) 423-229-2000 Fax: (1) 423-229-1193 Eastman Chemical Latin America 9155 South Dadeland Blvd. Suite 1116 Miami, FL 33156 U.S.A. Telephone: (1) 305-671-2800 Fax: (1) 305-671-2805 Eastman Chemical B.V. Fascinatio Boulevard 602-614 2909 VA Capelle aan den IJssel The Netherlands Telephone: (31) 10 2402 111 Fax: (31) 10 2402 100 Eastman (Shanghai) Chemical Commercial Company, Ltd. Jingan Branch 1206, CITIC Square No. 1168 Nanjing Road (W) Shanghai 200041, P.R. China Telephone: (86) 21 6120-8700 Fax: (86) 21 5213-5255 Eastman Chemical Japan Ltd. MetLife Aoyama Building 5F 2-11-16 Minami Aoyama Minato-ku, Tokyo 107-0062 Japan Telephone: (81) 3-3475-9510 Fax: (81) 3-3475-9515 Eastman Chemical Asia Pacific Pte. Ltd. #05-04 Winsland House 3 Killiney Road Singapore 239519 Telephone: (65) 6831-3100 Fax: (65) 6732-4930 Material Safety Data Sheets providing safety precautions that should be observed when handling and storing Eastman products are available online or by request. You should obtain and review the available material safety information before handling any of these products. If any materials mentioned are not Eastman products, appropriate industrial hygiene and other safety precautions recommended by their manufacturers should be observed. Neither Eastman Chemical Company nor its marketing affiliates shall be responsible for the use of this information or of any product, method, or apparatus mentioned, and you must make your own determination of its suitability and completeness for your own use, for the protection of the environment, and for the health and safety of your employees and purchasers of your products. NO WARRANTY IS MADE OF THE MERCHANTABILITY OR FITNESS OF ANY PRODUCT, AND NOTHING HEREIN WAIVES ANY OF THE SELLER’S CONDITIONS OF SALE. Eastman, Eastotac, Kristalex, Piccolastic, and Piccotex are trademarks of Eastman Chemical Company. All other brands are the property of their respective owners. © Eastman Chemical Company, 2012. www.eastman.com TT-136 10/12
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15:23:58-04:00, 2010:07:30 09:10:04-04:00, 2010:07:30 09:10:28-04:00, 2010:07:30 09:57:16-04:00, 2010:07:30 09:59:28-04:00, 2010:07:30 09:59:40-04:00, 2010:07:30 10:10:39-04:00, 2010:07:30 10:11:08-04:00, 2010:07:30 15:01:34-04:00, 2010:08:06 14:28:39-04:00, 2010:08:09 12:04:11-04:00, 2010:08:09 12:09:34-04:00, 2010:08:09 12:09:40-04:00, 2010:08:09 12:10:36-04:00, 2010:08:09 12:11:29-04:00, 2010:09:15 13:58:43-04:00, 2010:09:15 14:24:24-04:00, 2010:09:15 14:34:55-04:00, 2010:09:15 14:35:36-04:00, 2010:09:15 14:35:59-04:00, 2010:09:15 14:42:44-04:00, 2010:09:15 14:47:48-04:00, 2010:09:15 14:54:20-04:00, 2010:09:15 14:56:42-04:00, 2010:09:15 15:00:05-04:00, 2010:09:15 15:08:17-04:00, 2010:09:15 15:08:45-04:00, 2010:09:15 15:10:06-04:00, 2010:09:15 15:10:34-04:00, 2010:09:15 15:11:37-04:00, 2010:09:15 15:15:23-04:00, 2010:09:15 15:17:17-04:00, 2010:09:15 15:50:05-04:00, 2010:09:20 11:51:09-04:00, 2010:09:20 11:55:45-04:00, 2010:09:20 11:56:29-04:00, 2010:09:20 12:08:26-04:00, 2010:09:20 12:09:42-04:00, 2010:09:20 12:12:05-04:00, 2010:09:20 12:16:07-04:00, 2010:09:20 12:17:15-04:00, 2010:09:20 12:22:17-04:00, 2010:09:20 12:24:55-04:00, 2010:09:20 12:26:48-04:00, 2010:12:03 11:41:26-05:00, 2011:02:25 10:31:25-05:00, 2011:02:25 10:31:25-05:00, 2011:02:25 10:32:14-05:00, 2011:02:25 10:34:11-05:00, 2011:02:25 10:40:55-05:00, 2011:03:10 14:52:59-05:00, 2011:03:10 14:53:31-05:00, 2011:03:10 14:54:02-05:00, 2011:03:10 14:57:20-05:00, 2011:03:10 15:12:36-05:00, 2011:03:10 15:14:28-05:00, 2011:03:11 08:06:07-05:00, 2011:03:11 08:06:57-05:00, 2011:03:11 08:06:57-05:00, 2011:03:28 16:52:28-04:00, 2011:03:28 16:53:24-04:00, 2011:04:06 10:11:25-04:00, 2011:04:06 10:11:54-04:00, 2011:04:06 10:12:10-04:00, 2011:04:06 10:13:03-04:00, 2011:04:06 10:13:11-04:00, 2011:04:06 10:13:48-04:00, 2011:04:06 10:14:03-04:00, 2011:04:06 10:14:47-04:00, 2011:04:06 10:15:24-04:00, 2011:04:06 10:16:10-04:00, 2011:04:06 10:18:12-04:00, 2011:04:06 10:18:54-04:00, 2011:04:06 10:21:14-04:00, 2011:04:06 10:23:21-04:00, 2011:04:06 10:30:11-04:00, 2011:04:06 11:56:59-04:00, 2011:04:12 09:54:23-04:00, 2011:04:12 09:59:14-04:00, 2011:04:12 10:00:51-04:00, 2011:04:12 10:03:24-04:00, 2011:04:12 10:04:10-04:00, 2011:04:14 09:11:55-04:00, 2011:10:06 11:20:49-04:00, 2011:10:06 11:55:14-04:00, 2011:10:06 12:13:44-04:00, 2011:10:06 12:15:02-04:00, 2011:10:06 12:17:49-04:00, 2011:10:06 12:18:08-04:00, 2011:10:06 12:19:50-04:00, 2011:10:18 15:34:14-04:00, 2011:10:18 15:41:28-04:00, 2011:10:18 15:46:39-04:00, 2011:10:25 14:30:40-04:00, 2011:10:25 14:34:03-04:00, 2011:10:25 14:36-04:00, 2011:10:25 14:36:40-04:00, 2011:10:25 14:38:33-04:00, 2011:10:31 13:54:15-04:00, 2011:10:31 13:55:09-04:00, 2011:10:31 13:55:33-04:00, 2011:10:31 13:58:31-04:00, 2011:10:31 13:59:07-04:00, 2011:10:31 14:01:09-04:00, 2011:10:31 14:02:38-04:00, 2011:11:01 14:19:20-04:00, 2011:11:01 14:19:49-04:00, 2011:11:01 14:25:18-04:00, 2011:11:01 14:25:18-04:00, 2011:11:04 11:03:47-04:00, 2011:11:04 11:03:47-04:00, 2011:11:04 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/;/metadata, /;/metadata, /;/metadata, /;/metadata, /;/metadata, /;/metadata, /;/metadata Derived From Instance ID : xmp.iid:4CFC314D0F2068119457FD71D21C6835 Derived From Document ID : xmp.did:49C6D4A1292068118A6D844F1E84AA8B Derived From Original Document ID: xmp.did:E6413A57272068119109A1F00570920E Derived From Rendition Class : default Doc Change Count : 6636 Format : application/pdf Title : TT-136 Pure Monomer Resins Subject : TT-136, TT136 Description : Extending hydrogenated hydrocarbon resins with pure monomer resins in SIS-based nonwoven construction pressure sensitive adhesive formulations Producer : Adobe PDF Library 9.9 Trapped : Unknown Startup Profile : Print Page Count : 8EXIF Metadata provided by EXIF.tools