NB 226SGS BOM（ROHS） 161008 ROHS REPORT
2016-04-05
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bill of material (RoHS) Model: test result（unit：PPM） Item Description Specifications Qty supplier test report No. date of issue laboratr y 1 Resistor Pb Hg Cr/VI PBB PBDE ROHS 0603 33PF/k 2 RTO7R-6593-001 (attached P1) 2007-11-16 Intertek ND ND ND ND ND ND ROHS 0603 102K 10 RTO7R-6593-001 (attached P1) 2007-11-16 Intertek ND ND ND ND ND ND ROHS 0603 103K 4 P1) 2007-11-16 Intertek ND ND ND ND ND ND SMD Capacitor 2 Cd RTO7R-6593-001(attached Yuan mao ROHS 0603 104K 1 RTO7R-6593-001 (attached P1) 2007-11-16 Intertek ND ND ND ND ND ND ROHS 0603 105Z 6 RTO7R-6593-001 (attached P1) 2007-11-16 Intertek ND ND ND ND ND ND ROHS 0603 100pF±10% 2 RTO7R-6593-001 (attached P1) 2007-11-16 Intertek ND ND ND ND ND ND ROHS 0603 6.8Ω ±0.5% 8 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND ROHS 0603 22Ω ±0.5% 4 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND ROHS 0603 100Ω±0.5% 3 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND ROHS 0603 1.5kΩ±0.5% 1 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND ROHS 0603 4.7kΩ±0.5% 2 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND ROHS 0603 10 kΩ±0.5% 2 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND ROHS 0603 1 MΩ±0.5% 5 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND ROHS 0603 3.9M ±0.5% 2 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND 1 CANEC0800932401 (attached P2) 2008-03-20 SGS ND ND ND ND ND ND CE/2008/19508 (attached P3) 2008-02-13 SGS ND ND ND ND ND ND CE/2008/21496 (attached P4) 2008-02-20 SGS ND ND ND ND ND ND CE/2008/ 21491 (attached P5) 2008-02-20 SGS ND ND ND ND ND ND CE/2008/21494 (attached P6) 2008-02-20 SGS ND ND ND ND ND ND ROHS Shi meng 0603 AVR-M1608C120MT6AB Moulding gold green Tantalum powder Tantalum wire 3 Capacitor Manganese nitrate ROHS 47UF 1210 2 Tai suo bill of material (RoHS) Model: Item Description Specifications Qty supplier date of test report No. issue test result（unit：PPM） laboratr Cd y Pb Hg Cr/VI PBB PBDE Graphite CE/2008/19551 (attached P7) 2008-02-13 SGS ND ND ND ND ND ND Silver CE/2008/21499 (attached P8) 2008-02-20 SGS ND ND ND ND ND ND Paste CE/2008/ 21498 (attached P9) 2008-02-20 SGS ND ND ND ND ND ND CE/2008/219553 (attached P10) 2008-02-13 SGS ND 6 ND ND ND ND CE/2008/19545A (attached P11) 2008-02-20 SGS ND 319 ND ND ND ND CE/2008/34047 (attached P12) 2008-03-19 SGS ND ND ND ND ND ND CANEC0800544501(attachedP13) 2008-03-05 SGS ND ND ND ND ND ND CE/2008/34047 (attached P14) 2008-03-19 SGS ND ND ND ND ND ND CE/2008/34047 (attached P14) 2008-03-19 SGS ND ND ND ND ND ND GZ0711179980A/CHEM(attachedP15) 2008-4-16 SGS ND 6 ND ND ND ND CANEC0802822801 (attached P16) 2008-6-7 SGS ND ND ND ND ND ND CANEC0801059201 (attached 2008-03-24 SGS ND 15 ND ND ND ND CANEC0700699901(attached P18) 2007-11-14 SGS ND 6 ND ND ND ND CANEC0700699901(attached P18) 2007-11-14 SGS ND 6 ND ND ND ND STD Solder paste Leadframe NILO-Sn 4 Inductance 5 Crystal oscillator ROHS 1UH±10% 1812 4 Tai suo ROHS 12MHz 30PPM 1 BO li da 11*4mm SMD ROHS 56Ω 0805 6 3 Tai suo Magnetic bead ROHS 600Ω 0603 1 ROHS Ф3 2 LAMP 7 LED Hong jin SMD LED 8 PCB 9 EVA ROHS 36*36*1.2 mm 1 ROHS Ф15*0.5mm BK 2 Hua xing P17) Jin run he ROHS 120*3.0*1.5mm 2 ROHS ABS 9 S5 KA/2008/10040 (attached P19) 2008-01-09 SGS ND ND ND ND ND ND 10 Plastic 11 Lampshade ROHS PMMA 1 S5 KA/2008/10056 (attached P20) 2008-01-09 SGS ND ND ND ND ND ND 12 Glide board ROHS POM 2 S5 CD/2008/10512 (attached P21) 2008-01-06 SGS ND ND ND ND ND ND 13 Speaker unit ROHS 1.2” 8Ω 3w 2 Yong sheng SZHH00303727(attachedP22) 2008-10-06 Intertek ND ND ND ND ND ND bill of material (RoHS) Model: test result（unit：PPM） Item Description Specifications Qty supplier test report No. date of issue laboratr y 14 Pb Hg PBB PBDE I Brassy metal GZ0707098676/CHEM(attachedP23) 2007-07-18 SGS ND 42 ND ND ND ND Color powder SH7013378/CHEM(attachedP24) 2007-02-08 SGS ND ND ND ND ND ND Plastic grains GZ0707098677/CHEM(attachedP25) 2007-07-18 SGS ND 17 ND ND ND ND Color plastic GZ0702024726/CHEM(attachedP26) 2007-03-07 SGS ND 5 ND ND ND ND GZ0707098675/CHEM(attachedP27) 2007-07-18 SGS ND ND ND ND ND ND GZ0701009563A/CHEM(attachedP28) 2007-03-06 SGS ND 7 ND ND ND ND Metal terminal GZ0705069465/CHEM(attachedP29) 2007-03-23 SGS ND 21 ND ND ND ND PVC GZ0703029657/CHEM(attachedP30) 2007-03-14 SGS ND ND ND ND ND ND Metal GZ0705068556/CHEM(attachedP31) 2007-05-22 SGS ND 4 ND ND ND ND Tin thread A07032803C2342(attachedP32) 2007-03-28 ∧OV ND 89．6 ND ND ND ND Brass GZ0712190867/CHEM(attachedP33) 2007-12-21 SGS 4 165 ND ND ND ND Lron shell GZ0712190866/CHEM(attachedP34) 2007-12-21 SGS ND ND ND ND ND ND GZ0707105752/CHEM(attachedP35) 2007-08-01 SGS ND ND ND ND ND ND Plastic GZ0707105751/CHEM(attachedP36) 2007-08-01 SGS ND ND ND ND ND ND Green liquid GZ0712199380/CHEM(attachedP37) 2008-01-04 SGS ND ND ND ND ND ND Brown liquid GZ0712199378/CHEM(attachedP38) 2008-01-04 SGS ND ND ND ND ND ND Color metal ROHS Ф2.9mm 1 USB wire Ding tai L=1.6m Metal wire Phenolic resin 15 Cr/V Cd ROHS Switch 1 Hao yu ROHS Ф 0.4*OD9.0* 16 Spring 1 Ye tong CANEC0802581702(attachedP39) 2008-05-27 SGS ND ND ND ND ND ND 1 Wei feng GZSCR0809103587/LP(attachedP40) 2008-09-10 SGS ND ND ND ND ND ND L9.0*6N ROHS 17 Navigation steel 138*13.1*1.5mm bill of material (RoHS) Model: Item Description Specifications Qty supplier date of test report No. issue test result（unit：PPM） laboratr y Cd Pb Hg Cr/VI PBB PBDE ROHS KA1.3*8.0mm Ф2.4mm W 6 CANEC0801358901 (attached P41) 2008-04-06 SGS ND ND ND ND ND ND 1 CANEC0801358901 (attached P41) 2008-04-06 SGS ND ND ND ND ND ND CANEC0801358901 (attached P41) 2008-04-06 SGS ND ND ND ND ND ND 6 CANEC0801358901 (attached P41) 2008-04-06 SGS ND ND ND ND ND ND 1 CANEC0801358901 (attached P41) 2008-04-06 SGS ND ND ND ND ND ND 2 CANEC0801358901 (attached P41) 2008-04-06 SGS ND ND ND ND ND ND 2008-09-10 SGS ND 13 ND ND ND ND 2008-02-12 SGS ND ND ND ND ND ND KA/2008/10254(attached P44) 2008-01-10 SGS ND ND ND ND ND ND KA/2008/62610A-02(attached P45) 2008-07-09 SGS ND ND ND ND ND ND KA/2008/131720A-02(attached 2008-12-04 SGS ND ND ND ND ND ND ROHS PM3.0*6.0mm Ф5.0mm W ROHS KA2.3*8.0mm Ф4.0mm W 18 2 Jin ji li Screw ROHS PA2.3*8.0mm Ф3.6mm W ROHS PWA2.3*6.0mm Ф6.0mm BK ROHS PA2.6*8.0mm Ф4.0mm W PURE TIN CE/2008/90943(attached P42) LEAD FRAME KA/2007/C2817R3(attached P43) SILVER GRAY 19 IC RASTE ROHS AD62550A EPOXY LQFP-32PIN MOLDING 1 Bing zhen COMPOUND GOLD BONDING WIRE P46) P1 P1 P1 P1 P2 P2 P2 P2 P2 P2 P3 Test Report No. : CE/2008/19508 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 5 *CE/2008/19508* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : MOULDING GOLD GREEN TANTALUM DIVISION 2008/1/31 2008/1/31 TO 2008/2/13 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321, Ed.1 111/54/CDV Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P3 Test Report No. : CE/2008/19508 Date : 2008/02/13 Page : 2 of 5 *CE/2008/19508* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. n.d. n.d. n.d. (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : YELLOWISH BROWN LUMP Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P3 Test Report No. : CE/2008/19508 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 5 *CE/2008/19508* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2O2 measure the absorbance Glass HNO 3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO 3 Plastic H2SO4, H2O2, HNO 3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P3 Test Report No. : CE/2008/19508 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 5 *CE/2008/19508* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P3 Test Report No. : CE/2008/19508 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 5 *CE/2008/19508* ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P4 Test Report No. : CE/2008/21496 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 5 *CE/2008/21496* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : TANTALUM POWDER TANTALUM DIVISION 2008/2/13 2008/2/13 TO 2008/2/20 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321/2nd CDV (111/95/CDV) Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P4 Test Report No. : CE/2008/21496 Date : 2008/02/20 Page : 2 of 5 *CE/2008/21496* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. n.d. n.d. n.d. (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : BLACK POWDER Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P4 Test Report No. : CE/2008/21496 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 5 *CE/2008/21496* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr 6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 measure the absorbance Glass HNO3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P4 Test Report No. : CE/2008/21496 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 5 *CE/2008/21496* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P4 Test Report No. : CE/2008/21496 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 5 *CE/2008/21496* ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P5 Test Report No. : CE/2008/21491 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 6 *CE/2008/21491* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : TANTALUM WIRE TANTALUM DIVISION 2008/2/13 2008/2/13 TO 2008/2/20 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321/2nd CDV (111/95/CDV) Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for metallic samples by Spot test / Colorimetric Method. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P5 Test Report No. : CE/2008/21491 Date : 2008/02/20 Page : 2 of 6 *CE/2008/21491* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by Spot test / boiling water extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. n.d. n.d. Negative 2 2 2 See Note 5 (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - MDL TEST PART DESCRIPTION: NO.1 : SILVER COLORED METAL WIRE The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P5 Test Report No. : CE/2008/21491 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 6 *CE/2008/21491* Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. Spot-test: Negative = Absence of Cr(VI) coating / surface layer, Positive = Presence of Cr(VI) coating / surface layer; (The tested sample should be further verified by boiling-water-extraction method if the spot test result cannot be confirmed.) Boiling-water-extraction: Negative = Absence of Cr(VI) coating / surface layer. Positive = Presence of Cr(VI) coating / surface layer; the detected concentration in boiling-water-extraction solution is equal or greater 2 than 0.02 mg/kg with 50 cm sample surface area. 6. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P5 Test Report No. : CE/2008/21491 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 6 *CE/2008/21491* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr 6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 measure the absorbance Glass HNO3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P5 Test Report No. : CE/2008/21491 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 6 *CE/2008/21491* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P6 Test Report No. : CE/2008/21494 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 5 *CE/2008/21494* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : MANGANESE NITRATE TANTALUM DIVISION 2008/2/13 2008/2/13 TO 2008/2/20 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321/2nd CDV (111/95/CDV) Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P6 Test Report No. : CE/2008/21494 Date : 2008/02/20 Page : 2 of 5 *CE/2008/21494* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. n.d. n.d. n.d. (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : PINK PASTE Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P6 Test Report No. : CE/2008/21494 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 5 *CE/2008/21494* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr 6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 measure the absorbance Glass HNO3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P6 Test Report No. : CE/2008/21494 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 5 *CE/2008/21494* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P6 Test Report No. : CE/2008/21494 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 5 *CE/2008/21494* ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P7 Test Report No. : CE/2008/19551 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 5 *CE/2008/19551* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : GRAPHITE STD TANTALUM DIVISION 2008/1/31 2008/1/31 TO 2008/2/13 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321, Ed.1 111/54/CDV Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P7 Test Report No. : CE/2008/19551 Date : 2008/02/13 Page : 2 of 5 *CE/2008/19551* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. n.d. n.d. n.d. (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : BLACK PASTE Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P7 Test Report No. : CE/2008/19551 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 5 *CE/2008/19551* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2O2 measure the absorbance Glass HNO 3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO 3 Plastic H2SO4, H2O2, HNO 3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P7 Test Report No. : CE/2008/19551 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 5 *CE/2008/19551* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P7 Test Report No. : CE/2008/19551 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 5 *CE/2008/19551* ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P8 Test Report No. : CE/2008/21499 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 5 *CE/2008/21499* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : SILVER I TANTALUM DIVISION 2008/2/13 2008/2/13 TO 2008/2/20 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321/2nd CDV (111/95/CDV) Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P8 Test Report No. : CE/2008/21499 Date : 2008/02/20 Page : 2 of 5 *CE/2008/21499* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. n.d. n.d. n.d. (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : SILVER-GRAY COLORED LIQUID Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P8 Test Report No. : CE/2008/21499 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 5 *CE/2008/21499* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr 6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 measure the absorbance Glass HNO3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P8 Test Report No. : CE/2008/21499 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 5 *CE/2008/21499* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P8 Test Report No. : CE/2008/21499 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 5 *CE/2008/21499* ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P9 Test Report No. : CE/2008/21498 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 5 *CE/2008/21498* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : PASTE II TANTALUM DIVISION 2008/2/13 2008/2/13 TO 2008/2/20 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321/2nd CDV (111/95/CDV) Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P9 Test Report No. : CE/2008/21498 Date : 2008/02/20 Page : 2 of 5 *CE/2008/21498* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. n.d. n.d. n.d. (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : GRAY PASTE Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P9 Test Report No. : CE/2008/21498 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 5 *CE/2008/21498* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr 6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 measure the absorbance Glass HNO3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P9 Test Report No. : CE/2008/21498 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 5 *CE/2008/21498* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P9 Test Report No. : CE/2008/21498 Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 5 *CE/2008/21498* ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P10 Test Report No. : CE/2008/19553 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 5 *CE/2008/19553* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : SOLDER PASTE SAC4-325-GM5 2008/1/31 2008/1/31 TO 2008/2/13 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321, Ed.1 111/54/CDV Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Determination of Determination of Determination of Spectrometry. Cadmium by ICP-AES. Lead by ICP-AES. Mercury by ICP-AES. Hexavalent Chromium by UV/Vis (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P10 Test Report No. : CE/2008/19553 Date : 2008/02/13 Page : 2 of 5 *CE/2008/19553* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. 6 n.d. n.d. (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : GRAY PASTE Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P10 Test Report No. : CE/2008/19553 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 5 *CE/2008/19553* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2O2 measure the absorbance Glass HNO 3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO 3 Plastic H2SO4, H2O2, HNO 3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P10 Test Report No. : CE/2008/19553 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 5 *CE/2008/19553* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P10 Test Report No. : CE/2008/19553 Date : 2008/02/13 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 5 *CE/2008/19553* ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P11 Test Report No. : CE/2008/19545A Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 1 of 7 *CE/2008/19545A* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : LEADFRAME NILO-Sn II TANTALUM DIVISION 2008/01/31 2008/01/31 TO 2008/02/13 AND 2008/02/13 TO 2008/02/20 ========================================================================================= Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321/2nd CDV (111/95/CDV) Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for metallic samples by Spot test / Colorimetric Method. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). * This reports is added testing and combined with CE/2008/19545 * The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P11 Test Report No. : CE/2008/19545A Date : 2008/02/20 Page : 2 of 7 *CE/2008/19545A* AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by Spot test / boiling water extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) (Note 4) Monobromobiphenyl ether Dibromobiphenyl ether Tribromobiphenyl ether Tetrabromobiphenyl ether Pentabromobiphenyl ether Hexabromobiphenyl ether Heptabromobiphenyl ether Octabromobiphenyl ether Nonabromobiphenyl ether Decabromobiphenyl ether Sum of PBDEs (Mono to Deca) Method (Refer to) (1) (2) (3) (4) (5) Result MDL No.1 n.d. 319 n.d. Negative No.2 n.d. n.d. n.d. Negative 2 2 2 See Note 5 n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - TEST PART DESCRIPTION: NO.1 : PLATING LAYER OF SILVER COLORED METAL (CE/2008/19545) NO.2 : BASE MATERIAL OF SILVER COLORED METAL (CE/2008/19545) The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P11 Test Report No. : CE/2008/19545A Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 3 of 7 *CE/2008/19545A* Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. According to 2005/717/EC DecaBDE is exempt. 5. Spot-test: Negative = Absence of Cr(VI) coating / surface layer, Positive = Presence of Cr(VI) coating / surface layer; (The tested sample should be further verified by boiling-water-extraction method if the spot test result cannot be confirmed.) Boiling-water-extraction: Negative = Absence of Cr(VI) coating / surface layer. Positive = Presence of Cr(VI) coating / surface layer; the detected concentration in boiling-water-extraction solution is equal or greater 2 than 0.02 mg/kg with 50 cm sample surface area. 6. "-" = Not Regulated The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P11 Test Report No. : CE/2008/19545A Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 4 of 7 *CE/2008/19545A* NO.1 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Flow Chart of Stripping method for metal analysis Preparation Sample measurement Prepare suitable acid solution Put sample into acid solution Dissolve plating layer Solution ICP-AES The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P11 Test Report No. : CE/2008/19545A Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 5 of 7 *CE/2008/19545A* NO.2 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr 6+ test method excluded） 2) Name of the person who made measurement: Troy Chang 3) Name of the person in charge of measurement: Chenyu Kung Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3/HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H2O2 measure the absorbance Glass HNO3/HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P11 Test Report No. : CE/2008/19545A Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 6 of 7 *CE/2008/19545A* PBB/PBDE analytical FLOW CHART First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P11 Test Report No. : CE/2008/19545A Date : 2008/02/20 AVX / KYOCERA HONG KONG LTD. TAIWAN BRANCH 18F-6, 77 HSIN TAI WU RD., SEC. 1, HSICHIH, 221, TAIPEI HSIEN, TAIWAN Page : 7 of 7 *CE/2008/19545A* NO.1 NO.2 ** End of Report ** The content of this PDF file is in accordance with the original issued reports for reference only. This Test Report cannot be reproduced, except in full, without prior written permission of the Company SGS TAIWAN LIMITED NO. 136-1, Wu Kung Road, WuKu Industrial Zone, Taipei county, Taiwan. t(886-2) 22993939 f(886-2) 2299-3237 www.sgs.com.tw P12 P12 P12 P12 P12 P13 P13 P13 P13 P14 P14 P14 P14 P14 P15 P15 P15 P15 P15 P15 P16 P16 P16 P16 P16 P16 P17 P17 P17 P17 P18 P18 P18 P19 P19 P19 P19 P19 P20 P20 P20 P21 P21 P21 P22 P22 P22 P22 P22 P22 P22 P22 P23 P23 P23 P24 P24 P24 P25 P25 P25 P26 P26 P26 P27 P27 P27 P28 P28 P28 P28 P28 P29 P29 P29 P30 P30 P29 P30 P30 P31 P31 P31 P32 P32 P32 P32 P33 P33 P33 P34 P34 P34 P35 P35 P35 P36 P36 P36 P37 P37 P37 P37 P38 P38 P38 P38 P39 P39 P39 P39 P40 P40 P41 P41 P41 P42 Test Report No. : CE/2008/90943 Date : 2008/09/10 Page : 1 of 6 SHENMAO TECHNOLOGY INC. NO. 12-1, GONGYE 2ND RD., GUANYIN INDUSTRIAL AREA, TAOYUAN COUNTY 328, TAIWAN *CE/2008/90943* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : PURE TIN H99.99S 2008/09/03 2008/09/03 TO 2008/09/10 =========================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : With reference to IEC 62321/2nd CDV (111/95/CDV) Procedures for the Determination of Levels of Regulated Substances in Electrotechnical Products. (1) (2) (3) (4) Determination of Cadmium by ICP-AES. Determination of Lead by ICP-AES. Determination of Mercury by ICP-AES. Determination of Hexavalent Chromium for metallic samples by Spot test / boiling water extraction Method. (5) Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). Unless otherwise stated the results shown in this test report refer only to the sample(s) tested. This test report cannot be reproduced, except in full, without prior written permission of the Company. 除非另有說明，此報告結果僅對測試之樣品負責。本報告未經本公司書面許可，不可部分複製。 This Test Report is issued by the Company under its General Conditions of Service printed overleaf or available on request and accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this Test Report is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. SGS Taiwan Ltd. 台灣檢驗科技股份有限公司 Chemical-Taipei 33 WuChyuan Road, Wuku Industrial Zone, Taipei County, Taiwan /台北縣五股工業區五權路33號 t + 886 (02)2299 3279 f + 886 (02)2299 3237 www.sgs.com Member of the SGS Group (SGS SA) P42 Test Report No. : CE/2008/90943 Date : 2008/09/10 Page : 2 of 6 SHENMAO TECHNOLOGY INC. NO. 12-1, GONGYE 2ND RD., GUANYIN INDUSTRIAL AREA, TAOYUAN COUNTY 328, TAIWAN *CE/2008/90943* Test results by chemical method (Unit: mg/kg) Test Item (s): Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by Spot test / boiling water extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether Method (Refer to) (1) (2) (3) (4) Result No.1 n.d. 13 n.d. Negative 2 2 2 See Note 4 (5) n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 MDL TEST PART DESCRIPTION: NO.1 : SILVER COLORED METAL Unless otherwise stated the results shown in this test report refer only to the sample(s) tested. This test report cannot be reproduced, except in full, without prior written permission of the Company. 除非另有說明，此報告結果僅對測試之樣品負責。本報告未經本公司書面許可，不可部分複製。 This Test Report is issued by the Company under its General Conditions of Service printed overleaf or available on request and accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this Test Report is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. SGS Taiwan Ltd. 台灣檢驗科技股份有限公司 Chemical-Taipei 33 WuChyuan Road, Wuku Industrial Zone, Taipei County, Taiwan /台北縣五股工業區五權路33號 t + 886 (02)2299 3279 f + 886 (02)2299 3237 www.sgs.com Member of the SGS Group (SGS SA) P42 Test Report No. : CE/2008/90943 Date : 2008/09/10 SHENMAO TECHNOLOGY INC. NO. 12-1, GONGYE 2ND RD., GUANYIN INDUSTRIAL AREA, TAOYUAN COUNTY 328, TAIWAN Page : 3 of 6 *CE/2008/90943* Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. Spot-test: Negative = Absence of Cr(VI) coating / surface layer, Positive = Presence of Cr(VI) coating / surface layer; (The tested sample should be further verified by boiling-water-extraction method if the spot test result cannot be confirmed.) Boiling-water-extraction: Negative = Absence of Cr(VI) coating / surface layer. Positive = Presence of Cr(VI) coating / surface layer; the detected concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50 cm2 sample surface area. 5. "-" = Not Regulated Unless otherwise stated the results shown in this test report refer only to the sample(s) tested. This test report cannot be reproduced, except in full, without prior written permission of the Company. 除非另有說明，此報告結果僅對測試之樣品負責。本報告未經本公司書面許可，不可部分複製。 This Test Report is issued by the Company under its General Conditions of Service printed overleaf or available on request and accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this Test Report is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. SGS Taiwan Ltd. 台灣檢驗科技股份有限公司 Chemical-Taipei 33 WuChyuan Road, Wuku Industrial Zone, Taipei County, Taiwan /台北縣五股工業區五權路33號 t + 886 (02)2299 3279 f + 886 (02)2299 3237 www.sgs.com Member of the SGS Group (SGS SA) P42 Test Report No. : CE/2008/90943 Date : 2008/09/10 Page : 4 of 6 SHENMAO TECHNOLOGY INC. NO. 12-1, GONGYE 2ND RD., GUANYIN INDUSTRIAL AREA, TAOYUAN COUNTY 328, TAIWAN *CE/2008/90943* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. （Cr 6+ test method excluded） 2) Name of the person who made measurement: Climbgreat Yang 3) Name of the person in charge of measurement: Troy Chang Cutting / Preparation Sample Measurement Cr6 ＋ Hg Pb、Cd Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO3 /HCl/HF Filtration Add appropriate amount of digestion reagent Heat to appropriate temperature to extract Residue Solution Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve Add diphenyl-carbazide for ICP-AES Sample Material color development Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO3 , HCl, HF, H 2O2 measure the absorbance Glass HNO3 /HF at 540 nm by UV-VIS Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2 SO4 , H2O2 , HNO 3, HCl Others Any acid to total digestion Unless otherwise stated the results shown in this test report refer only to the sample(s) tested. This test report cannot be reproduced, except in full, without prior written permission of the Company. 除非另有說明，此報告結果僅對測試之樣品負責。本報告未經本公司書面許可，不可部分複製。 This Test Report is issued by the Company under its General Conditions of Service printed overleaf or available on request and accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this Test Report is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. SGS Taiwan Ltd. 台灣檢驗科技股份有限公司 Chemical-Taipei 33 WuChyuan Road, Wuku Industrial Zone, Taipei County, Taiwan /台北縣五股工業區五權路33號 t + 886 (02)2299 3279 f + 886 (02)2299 3237 www.sgs.com Member of the SGS Group (SGS SA) P42 Test Report No. : CE/2008/90943 Date : 2008/09/10 Page : 5 of 6 SHENMAO TECHNOLOGY INC. NO. 12-1, GONGYE 2ND RD., GUANYIN INDUSTRIAL AREA, TAOYUAN COUNTY 328, TAIWAN *CE/2008/90943* PBB/PBDE analytical FLOW CHART 1) Name of the person who made measurement: Roman Wong 2) Name of the person in charge of measurement: Shinjyh Chen First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report Unless otherwise stated the results shown in this test report refer only to the sample(s) tested. This test report cannot be reproduced, except in full, without prior written permission of the Company. 除非另有說明，此報告結果僅對測試之樣品負責。本報告未經本公司書面許可，不可部分複製。 This Test Report is issued by the Company under its General Conditions of Service printed overleaf or available on request and accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this Test Report is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. SGS Taiwan Ltd. 台灣檢驗科技股份有限公司 Chemical-Taipei 33 WuChyuan Road, Wuku Industrial Zone, Taipei County, Taiwan /台北縣五股工業區五權路33號 t + 886 (02)2299 3279 f + 886 (02)2299 3237 www.sgs.com Member of the SGS Group (SGS SA) P42 Test Report No. : CE/2008/90943 Date : 2008/09/10 SHENMAO TECHNOLOGY INC. NO. 12-1, GONGYE 2ND RD., GUANYIN INDUSTRIAL AREA, TAOYUAN COUNTY 328, TAIWAN Page : 6 of 6 *CE/2008/90943* ** End of Report ** Unless otherwise stated the results shown in this test report refer only to the sample(s) tested. This test report cannot be reproduced, except in full, without prior written permission of the Company. 除非另有說明，此報告結果僅對測試之樣品負責。本報告未經本公司書面許可，不可部分複製。 This Test Report is issued by the Company under its General Conditions of Service printed overleaf or available on request and accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this Test Report is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. SGS Taiwan Ltd. 台灣檢驗科技股份有限公司 Chemical-Taipei 33 WuChyuan Road, Wuku Industrial Zone, Taipei County, Taiwan /台北縣五股工業區五權路33號 t + 886 (02)2299 3279 f + 886 (02)2299 3237 www.sgs.com Member of the SGS Group (SGS SA) P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P43 P44 P44 P44 P44 P44 P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 1 of 9 *KA-2008-62610A-02* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : EPOXY MOLDING COMPOUND EME-G700L SERIES 2008/06/24 2008/06/24 TO 2008/06/30 =============================================================================================== Test Result(s) : - Please see the next page(s) - P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 2 of 9 *KA-2008-62610A-02* Test Result(s) PART NAME NO.1 ： BLACK EPOXY MOLDING COMPOUND Hexavalent Chromium Cr(VI) by alkaline extraction mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. 2 Result No. 1 n.d. Cadmium (Cd) mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Cadmium by ICP-AES. 2 n.d. Mercury (Hg) mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Mercury by ICP-AES. 2 n.d. Lead (Pb) mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Lead by ICP-AES. 2 n.d. Antimony (Sb) mg/kg With reference to US EPA 3052. Analysis was performed by ICP-AES. 2 n.d. PERFLUOROOCTANE SULFONATES mg/kg With reference to US EPA 3540C : 1996 (PFOS) method for PFOS Content. Analysis was performed by LC/MS. 10 n.d. Halogen-Bromine (Br) (CAS NO.: 007726-95-6) mg/kg With reference to BS EN 14582 .Analysis was performed by IC method for Bromine content. 50 n.d. Halogen-Chlorine (Cl) (CAS NO.: 007782-50-5) mg/kg With reference to BS EN 14582 . Analysis was performed by IC method for Chlorine content. 50 n.d. Test Item (s) Unit Method MDL P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 3 of 9 Test Item (s) Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether Sum of PBDEs (Mono to Deca) Unit mg/kg mg/kg Method With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of PBBs and PBDEs by GC/MS. With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of PBBs and PBDEs by GC/MS. *KA-2008-62610A-02* Result MDL No. 1 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. 5 n.d. n.d. Note： 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. " - " = Not Regulated 5. This is the additional test report of KA/2008/62610 which was issued on 2008/06/30. Please refer to KA/2008/62610 for original information. P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 4 of 9 *KA-2008-62610A-02* P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 5 of 9 *KA-2008-62610A-02* P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 6 of 9 *KA-2008-62610A-02* P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 7 of 9 *KA-2008-62610A-02* P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 8 of 9 *KA-2008-62610A-02* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. 2) Name of the person who made measurement: Hungming Li 3) Name of the person in charge of measurement: Ray Chang Flow Chart of Digestion for elements analysis Cutting / Preparation Sample Measurement Acid digestion by suitable acid depended on different sample material (as below table) Filtration Residue Solution 1) Alkali Fusion 2) HCl to dissolve ICP-AES Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 Glass HNO3/HF Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion P45 Test Report SUMITOMO BAKELITE \CO., LTD. NO.1, HUASI RD., DALIAO TOWNSHIP, KAOHSIUNG COUNTY 831, TAIWAN (R.O.C.) Report No. : KA/2008/62610A-02 Date : 2008/07/09 Page : 9 of 9 *KA-2008-62610A-02* ** End of Report ** P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 1 of 29 *KA-2008-B1720A-02* The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : GOLD BONDING WIRE SGL2 2008/11/24 2008/11/24 TO 2008/12/4 =============================================================================================== Test Result(s) : - Please see the next page(s) - P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 2 of 29 *KA-2008-B1720A-02* Test Result(s) PART NAME NO.1 ： GOLD BONDING WIRE Cadmium (Cd) mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Cadmium by ICP-AES. 2 Result No. 1 n.d. Lead (Pb) mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Lead by ICPAES. 2 n.d. Mercury (Hg) mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Mercury by ICP-AES. 2 n.d. Hexavalent Chromium Cr(VI) by alkaline extraction mg/kg With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of Hexavalent Chromium for samples by UV/Vis Spectrometry. 2 n.d. 5 5 5 5 5 5 5 5 5 5 - n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. 5 5 5 5 5 5 5 5 5 5 n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. Test Item (s) Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether Unit mg/kg mg/kg Method With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of PBBs and PBDEs by GC/MS. With reference to IEC 62321/2nd CDV (111/95/CDV). Determination of PBBs and PBDEs by GC/MS. MDL P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) Beryllium (Be) Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 3 of 29 *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 3052. Analysis was 2 n.d. performed by ICP-AES. Carbon Tetrachloride mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Methyl Chloroform mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 0.01 n.d. Chlorinated Paraffin (C10~C13) (CAS NO.: 010871-26-2) % With reference to US EPA 3540C. Analysis was performed by GC/ECD. Formaldehyde (CAS NO.: 000050-00-0) mg/kg With reference to DIN 53315. Analysis was performed by HPLC/DAD. 3 n.d. PCBs (Polychlorinated Biphenyls) (CAS NO.: 001336-36-3) mg/kg With reference to US EPA 3540C. Analysis was performed by GC/ECD. 0.5 n.d. Polychlorinated Naphthalene mg/kg With reference to US EPA 3540C. Analysis was performed by GC/MS. 5 n.d. PCTs (Polychlorinated Terphenyls) mg/kg With reference to US EPA 3540C. Analysis was performed by GC/MS. 0.5 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) PERFLUOROOCTANOIC ACID (PFOA) PERFLUOROOCTANE SULFONATES (PFOS) PFOS – Acid PFOS – Metal Salt PFOS – Amide PVC (CAS NO.: 9002-86-2) Unit Method mg/kg With reference to US EPA 3540C : 1996 method for PFOA Content. Analysis was performed by LC/MS. mg/kg With reference to US EPA 3540C : 1996 method for PFOS Content. Analysis was performed by LC/MS. ** Analysis was performed by FTIR and FLAME Test. 2-(2-HYDROXY-3',5'-DI-Tmg/kg With reference to US EPA 3540C. Analysis BUTYLPHENYL)BENZOTRIAZOLE was performed by GC/MS. (CAS NO.3846-71-7) Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 4 of 29 *KA-2008-B1720A-02* Result MDL No. 1 10 n.d. 10 n.d. - Negative 10 n.d. Asbestos Anthrophyllite (CAS NO.017068-78-9) --% --As per NIOSH 9000 method. Analysis was performed by XRD. --1 --Negative Crocidolite (CAS NO.012001-28-4) % As per NIOSH 9000 method. Analysis was performed by XRD. 1 Negative Amosite (CAS NO.012172-73-5) % As per NIOSH 9000 method. Analysis was performed by XRD. 1 Negative Tremolite (CAS NO.014567-73-8) % As per NIOSH 9000 method. Analysis was performed by XRD. 1 Negative Chrysotile (CAS NO.012001-29-5) % As per NIOSH 9000 method. Analysis was performed by XRD. 1 Negative Actinolite (CAS NO.013768-00-8) % As per NIOSH 9000 method. Analysis was performed by XRD. 1 Negative CHCs (Chlorinated hydrocarbon) --- --- --- --- 1,1,1,2-Tetrachloroethane (CAS NO.: 000630-20-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,1,1-Trichloroethane (CAS NO.: 000071-55-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 5 of 29 1,1,2,2-Tetrachloroethane (CAS NO.: 000079-34-5) *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. 1,1,2-Trichloroethane (CAS NO.: 000079-00-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,1-Dichloroethene (CAS NO.: 000075-35-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,1-Dichloroethane (CAS NO.: 000075-34-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,1-Dichloropropene (CAS NO.: 000563-58-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,2,3-Trichloropropane (CAS NO.: 000096-19-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,2-Dichloroethane (CAS NO.: 000107-06-2) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,2-Dichloropropane (CAS NO.: 000078-87-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,3-Dichloropropane (CAS NO.: 000142-28-9) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 2,2-Dichloropropane (CAS NO.: 000594-20-7) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chloroethane (CAS NO.: 000075-00-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chloroform (CAS NO.: 000067-66-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chloromethane (CAS NO.: 000074-87-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Cis-1,2-Dichloroethene (CAS NO.: 000156-59-2) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Test Item (s) P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 6 of 29 Cis-1,3-Dichloropropene (CAS NO.: 010061-01-5) *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. Hexachlorobutadiene (CAS NO.: 000087-68-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Methylene Chloride (CAS NO.: 000075-09-2) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. trans-1,2-Dichloroethene (CAS NO.: 000156-60-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. trans-1,3-Dichloropropene (CAS NO.: 010061-02-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Trichloroethylene (CAS NO.: 000079-01-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. --- --- Test Item (s) Hydrofluorcarbon, fluorinated hydrocarbon, fluorohydrocarbon (HFC) --- --- HFC-23 (CHF3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-32 (CH2F2) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-41 (CH3F) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-43-10mee (C5H2F10) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-125 (C2HF5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-134 (C2H2F4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-134a (CH2FCF3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-143 (C2H3F3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) HFC-143a (C2H3F3) Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 7 of 29 *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. HFC-152a (C2H4F2) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-227ea (C3HF7) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-236cb (CH2FCF2CF3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-236fa (C3H2F6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-236ea (CHF2CHFCF3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-245ca (C3H3F5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-245fa (CHF2CH2CF3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HFC-365mfc (CF3CH2CF2CH3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. --- --- PERFLUOROCARBON(PFC) --- --- F14 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Fluorocarbon 116 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) Freon 218 Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 8 of 29 *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. Decafluorobutane mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Freon C 318 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Perfluoro-1-butene mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Perfluoroisobutene mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 1,4-Dihydrooctafluorobutane mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Nonafluoro-2(trifluoromethyl)butane mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Perfluoro-n-pentane mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. 2-Perfluoromethylpentane mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Perfluorohexane mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 9 of 29 Organic-TIN compounds Tributyl Tin(TBT) (CAS NO.: 000688-73-3) *KA-2008-B1720A-02* Result Unit Method MDL No. 1 --------mg/kg With reference to DIN 38407-13. Analysis was 0.03 n.d. performed by GC/FPD. Triphenyl Tin(TphT) (CAS NO.: 000668-34-8) mg/kg With reference to DIN 38407-13. Analysis was performed by GC/FPD. 0.03 n.d. Tributyl Tin Oxide(TBTO)*** (CAS NO.: 000056-35-9) mg/kg With reference to DIN 38407-13. Analysis was performed by GC/FPD. 0.03 n.d. --- --- Test Item (s) CFCs(Chlorofluorocarbons) & HALON --- --- Chlorofluorocarbon-11 (CAS NO.: 000075-69-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-12 (CAS NO.: 000075-71-8) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-113 (CAS NO.: 000076-13-1) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-114 (CAS NO.: 000076-14-2) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-115 (CAS NO.: 000076-15-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-13 (CAS NO.: 000075-72-9) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-111 (CAS NO.: 000354-56-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 10 of 29 Chlorofluorocarbon-112 (CAS NO.: 000076-12-0) *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. Chlorofluorocarbon-211 (CAS NO.: 135401-87-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-212 (CAS NO.: 076564-99-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-213 (CAS NO.: 060285-54-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-214 (CAS NO.: 002268-46-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-215 (CAS NO.: 000076-17-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-216 (CAS NO.: 001652-80-8) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Chlorofluorocarbon-217 (CAS NO.: 000422-86-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HALON-1211 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HALON-1301 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HALON-2402 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. --- --- Test Item (s) HCFC's (Hydrogenated chlorofluorocarbons) --- --- Hydrochlorofluorocarbon-21 (CAS NO.: 000075-43-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-22 (CAS NO.: 000075-45-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 11 of 29 Hydrochlorofluorocarbon-31 (CAS NO.: 000593-70-4) *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. Hydrochlorofluorocarbon-121 (CAS NO.: 130879-71-9) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-122 (CAS NO.: 041834-16-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-123 (CAS NO.: 034077-87-7) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-124 (CAS NO.: 063938-10-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-131 (CAS NO.: 134237-34-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-132 (CAS NO.: 025915-78-0) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-133 (CAS NO.: 001330-45-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-141 (CAS NO.: 025167-88-8) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-141b (CAS NO.: 001717-00-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-142 (CAS NO.: 025497-29-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-142b (CAS NO.: 000075-68-3) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-151 (CAS NO.: 001615-75-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-221 (CAS NO.: 134237-35-7) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-222 (CAS NO.: 134237-36-8) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Test Item (s) P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 12 of 29 Hydrochlorofluorocarbon-223 (CAS NO.: 134237-37-9) *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. Hydrochlorofluorocarbon-224 (CAS NO.: 134237-38-0) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-225 (CAS NO.: 127564-92-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-225ca (CAS NO.: 000422-56-0) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-225cb (CAS NO.: 000507-55-1) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-226 (CAS NO.: 134308-72-8) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-231 (CAS NO.: 134190-48-0) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-232 (CAS NO.: 134237-39-1) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-233 (CAS NO.: 134237-40-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-234 (CAS NO.: 127564-83-4) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-235 (CAS NO.: 134237-83-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-241 (CAS NO.: 134190-49-1) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-242 (CAS NO.: 134237-42-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-243 (CAS NO.: 134237-43-7) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Test Item (s) P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 13 of 29 Hydrochlorofluorocarbon-244 (CAS NO.: 134190-50-4) *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. Hydrochlorofluorocarbon-251 (CAS NO.: 134190-51-5) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-252 (CAS NO.: 134190-52-6) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-253 (CAS NO.: 134237-44-8) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-261 (CAS NO.: 134237-45-9) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-262 (CAS NO.: 134190-53-7) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Hydrochlorofluorocarbon-271 (CAS NO.: 134190-54-8) mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. --- --- Test Item (s) HBFC's (Hydrogenated bromofluorocarbons) --- --- HBFC-21B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-22B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-31B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-121B4 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-122B3 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-123B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-124B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) HBFC-131B3 Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 14 of 29 *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. HBFC-132B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-133B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-141B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-142B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-151B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-221B6 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-222B5 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-223B4 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-224B3 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-225B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-226B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-231B5 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-232B4 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-233B3 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) HBFC-234B2 Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 15 of 29 *KA-2008-B1720A-02* Result Unit Method MDL No. 1 mg/kg With reference to US EPA 5021. Analysis was 1 n.d. performed by GC/MS. HBFC-235B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-241B4 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-242B3 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-243B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-244B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-251B3 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-252B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-253B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-261B2 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-262B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. HBFC-271B1 mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. Bromomethane mg/kg With reference to US EPA 5021. Analysis was performed by GC/MS. 1 n.d. AZO 1):4-AMINODIPHENYL (CAS NO.92-67-1) ----mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. --3 --n.d. 2):BENZIDINE (CAS NO.92-87-5) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) Unit Method Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 16 of 29 *KA-2008-B1720A-02* Result MDL No. 1 3 n.d. 3):4-CHLORO-O-TOLUIDINE (CAS NO.95-69-2) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 4):2-NAPHTHYLAMINE (CAS NO.91-59-8) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 5):O-AMINO-AZOTOLUENE (CAS NO.97-56-3) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 6):2-AMINO-4-NITROTOLUENE (CAS NO.99-55-8) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 7):P-CHLOROANILINE (CAS NO.106-47-8) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 8):2,4-DIAMINOANISOLE (CAS NO.615-05-4) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 9):4,4DIAMINODIPHENYLMETHANE (CAS NO.101-77-9) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 10):3,3-DICHLOROBENZIDINE (CAS NO.91-94-1) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 11):3,3-DIMETHOXYBENZIDINE (CAS NO.119-90-4) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 12):3,3-DIMETHYLBENZIDINE (CAS NO.119-93-7) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 13):3,3-DIMETHYL4,4DIAMINODIPHENYLMETHA (CAS NO.838-88-0) 14):P-CRESIDINE (2-METHOXY-5METHYLANILINE) (CAS NO.120-71-8) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Test Item (s) Unit Method Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 17 of 29 *KA-2008-B1720A-02* Result MDL No. 1 3 n.d. 15):4,4-METHYLENE-BIS(2-CHLORANILINE) (CAS NO.101-14-4) 16):4,4-OXYDIANILINE (CAS NO.101-80-4) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 17):4,4-THIODIANILINE (CAS NO.139-65-1) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 18):O-TOLUIDINE (CAS NO.95-53-4) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 19):2-4-TOLUYLENDIAMINE (CAS NO.95-80-7) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 20):2,4,5-TRIMETHYLANILINE (CAS NO.137-17-7) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 21):O-ANISIDINE (CAS NO.90-04-0) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 22):P-AMINOAZOBENZENE (CAS NO.60-09-3) mg/kg With reference to LMBG 82.02-Z. Analysis was performed by GC/MS. 3 n.d. 23):2,4-XYLIDINE (CAS NO.95-68-1) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. 24):2,6-XYLIDINE (CAS NO.87-62-7) mg/kg With reference to LMBG 82.02-2. Analysis was performed by GC/MS. 3 n.d. Halogen-Chlorine (Cl) (CAS No.: 022537-15-1) mg/kg With reference to BS EN 14582 . Analysis was performed by IC method for Chlorine content. 50 n.d. Halogen-Bromine (Br) (CAS No.: 010097-32-2) mg/kg With reference to BS EN 14582 .Analysis was performed by IC method for Bromine content. 50 n.d. P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 18 of 29 *KA-2008-B1720A-02* Note： 1. mg/kg = ppm; 0.1wt% = 1000ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. The exemption of DecaBDE in polymeric application according 2005/717/EC was overruled by the European Court of Justice by its decision of 01.04.2008. Subsequently DecaBDE will be included in the sum of PBDE after 01.07.2008 5. " - " = Not Regulated 6. " --- " = Not Conducted 7. * = Results shown are of the adjusted analytical results 8. ** = Qualitative analysis (No Unit) 9. Negative = Undetectable / Positive = Detectable 10. The MDL is 5ppm for the single compound of CP 11. ***The substance is calculated by the test results of Tributyl Tin or heavy metal (Ex. Antimony、 Beryllium、Silicon 、 Zinc、Cobalt or Phosphorus respectively). The MDL is evaluated for Tributyl Tin or heavy metal (Ex. Antimony、Beryllium、Silicon 、 Zinc、Cobalt or Phosphorus respectively.) 12. Amending for the 22nd Council Directive 76/769/EEC notified under document 2005/84/EC, total concentration of three compounds DEHP, DBP and BBP shall not be greater than 0.1% and total concentration of three compounds DINP, DIDP and DNOP shall not be greater than 0.1%. 13. Brand and model of FTIR: VARIAN 3100 14. The Asbestos test was subcontracted to other SGS Laboratory. 15. Normal* : Test result is within Background (Background = 0.04~0.08 μSv/ hour) 16. This is the additional test report of KA/2008/B1720 which was issued on 2008/12/04. Please refer to KA/2008/B1720 for original information. PFOS Reference Information : 2006/122/EC (Directive 2006/122/EC) (1) May not be placed on the market or used as a substance or constituent of preparations in a concentration equal to or higher than 0,005 % by mass. (2) May not be placed on the market in semi-finished products or articles, or parts thereof, if the concentration of PFOS is equal to or higher than 0,1 % by mass calculated with reference to the mass of structurally or microstructurally distinct parts that contain PFOS or, for textiles or other coated materials, if the amount of PFOS is equal to or higher than 1µg/m2 of the coated material. 15. This report supersedes all pervious documents bearing the test report number KA/200X/XXXXX. 16. This is the additional test report of KA/200X/XXXXX which was issued on yyyy/mm/dd. Please refer to KA/200X/XXXXX for original information.P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 19 of 29 *KA-2008-B1720A-02* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart.（Cr6+ test method excluded） 2) Name of the person who made measurement: Hungming Li 3) Name of the person in charge of measurement: Ray Chang Cutting / Preparation Sample Measurement Cr6＋ Hg Pb、Cd Acid digestion by suitable acid Microwave digestion with depended on different sample HNO3/HCl/HF Add appropriate amount of digestion reagent material (as below table) Heat to appropriate temperature to extract Filtration Solution Residue Cool, filter digestate through filter 1) Alkali Fusion Add diphenyl-carbazide for 2) HCl to dissolve color development ICP-AES measure the absorbance Sample Material Digestion Acid at 540 nm by UV-VIS Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 Glass HNO3/HF Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 20 of 29 PBB/PBDE analytical FLOW CHART *KA-2008-B1720A-02* 1) Name of the person who made measurement: Anson Tsao 2) Name of the person in charge of measurement: Ray Chang First testing process Optional screen process Sample Confirmation process Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 21 of 29 *KA-2008-B1720A-02* 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. 2) Name of the person who made measurement: Hungming Li 3) Name of the person in charge of measurement: Ray Chang Flow Chart of Digestion for elements analysis Cutting / Preparation Sample Measurement Acid digestion by suitable acid depended on different sample material (as below table) Filtration Residue Solution 1) Alkali Fusion 2) HCl to dissolve ICP-AES Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2 Glass HNO3/HF Gold, platinum, palladium, ceramic Aqua regia Silver HNO3 Plastic H2SO4, H2O2, HNO3, HCl Others Any acid to total digestion P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 22 of 29 *KA-2008-B1720A-02* Analytical flow chart of halogen content 1) Name of the person who made measurement: Hungming Li 2) Name of the person in charge of measurement: Ray Chang Sample picture and report number Sample pretreatment/separation Weighting and putting sample in cell Oxygen Bomb Combustion /Absorption Dilution to fixed volume Analysis was performed by IC P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 23 of 29 *KA-2008-B1720A-02* Analytical flow chart of PFOA/PFOS content 1) Name of the person who made measurement: Anson Tsao 2) Name of the person in charge of measurement: Ray Chang Sample pretreatment Sample extraction by Soxhlet extraction (Reference method US EPA 3540) Concentrate/Dilute Extracted solution Analysis was performed by LC/MS Data P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 24 of 29 *KA-2008-B1720A-02* Chlorinated Flame retardant analytical flow chart 1) Name of the person who made measurement: Anson Tsao 2) Name of the person in charge of measurement: Ray Chang Reference method: USEPA 3540 Test Items: PCBs, CP, MCCP Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute the extracted solution Analysis was performed by GC/ECD Data P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 25 of 29 *KA-2008-B1720A-02* Chlorinated Flame retardant analytical flow chart 1) Name of the person who made measurement: Anson Tsao 2) Name of the person in charge of measurement: Ray Chang Reference method: US EPA 8270D, US EPA 3540 Test Items: PCNs, PCTs, Mirex Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute the extracted solution Analysis was performed by GC/MS Data P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 26 of 29 *KA-2008-B1720A-02* Analysis flow chart for determination of Asbestos 1) Name of the person who made measurement: Victor Kao 2) Name of the person in charge of measurement: James Lu Sampling Sample pretreatment / Separation Preparation of primary analytical sample X-ray diffraction qualitative analysis Diffraction peak of Diffraction peak of asbestos is present asbestos is absent Positive Negative P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 27 of 29 *KA-2008-B1720A-02* Analysis flow chart for determination of PVC in polymer material 1) Name of the person who made measurement: Joyce Chiu 2) Name of the person in charge of measurement: Roger Lin Sample pre-treatment Flame test Sample analyzed by FTIR Check wave-number of C-Cl bond Data P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 28 of 29 *KA-2008-B1720A-02* Analytical flow chart of benzotriazole content 1) Name of the person who made measurement: Anson Tsao 2) Name of the person in charge of measurement: Ray Chang Sample pretreatment Sample extraction by soxhlet method (Reference method US EPA 3540) Concentrate/Dilute Extracted solution Analysis was performed by GC/MS Data P46 Test Report SUMITOMO METAL MINING CO.,LTD. 11-3,SHIMBASHI 5-CHOME,MINATO-KU,TOKYO 105-8716,JAPAN. ** End of Report ** Report No. : KA/2008/B1720A-02 Date : 2008/12/04 Page : 29 of 29 *KA-2008-B1720A-02*
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