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Test Report. No. CANEC1402177407 Date: 06 Mar 2014. Page 1 of 8. HUISHENG PLASTICS (SHENZHEN) CO.,LTD.. NO.2 NINETY-NINE INDUSTRIAL AREA,MINZHU VILLAGE,SHAJING TOWN,BAOAN DISTRICT OF SHENZHEN,GUANGDONG CHINA. . The following sample(s) was/were submitted and identified on behalf of the clients as : BLACK PVC. SGS Job No. : CP14-007332 - SZ. Date of Sample Received :. 28 Feb 2014. Testing Period :. 28 Feb 2014 - 06 Mar 2014. Test Requested :. Selected test(s) as requested by client.. Test Method :. Please refer to next page(s).. Test Results :. Please refer to next page(s).. Conclusion :. Based on the performed tests on submitted samples, the results of Lead, Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB), Polybrominated diphenyl ethers (PBDE) comply with the limits as set by RoHS Directive 2011/65/EU Annex II; recasting 2002/95/EC.. Signed for and on behalf of SGS-CSTC Ltd.. Alkene_Liang. Approved Signatory. Test Report. No. CANEC1402177407 Date: 06 Mar 2014. Page 2 of 8. Test Results :. Test Part Description :. Specimen No.. SN1. SGS Sample ID. CAN14-021774.002 Description. Black plastic grains. Remarks :. (1) 1 mg/kg = 1 ppm = 0.0001%. (2) MDL = Method Detection Limit. (3) ND = Not Detected ( < MDL ). (4) "-" = Not Regulated. RoHS Directive 2011/65/EU. Test Method :. (1)With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES. (2)With reference to IEC 62321-5:2013, determination of Lead by ICP-OES. (3)With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES. (4)With reference to IEC 62321:2008, determination of Hexavalent Chromium by Colorimetric Method using UV-Vis. (5)With reference to IEC 62321:2008, determination of PBBs and PBDEs by GC-MS.. Test Item(s). Limit. Unit. MDL. 002. Cadmium (Cd). 100 mg/kg. 2 ND Lead (Pb). 1,000 mg/kg. 2 ND Mercury (Hg). 1,000 mg/kg. 2 ND Hexavalent Chromium (CrVI). 1,000 mg/kg. 2 ND Sum of PBBs. 1,000 mg/kg. - ND Monobromobiphenyl. - mg/kg. 5 ND Dibromobiphenyl. - mg/kg. 5 ND Tribromobiphenyl. - mg/kg. 5 ND Tetrabromobiphenyl. - mg/kg. 5 ND Pentabromobiphenyl. - mg/kg. 5 ND Hexabromobiphenyl. - mg/kg. 5 ND Heptabromobiphenyl. - mg/kg. 5 ND Octabromobiphenyl. - mg/kg. 5 ND Nonabromobiphenyl. - mg/kg. 5 ND Decabromobiphenyl. Sum of PBDEs. Monobromodiphenyl ether. - mg/kg. 5 ND 1,000 mg/kg. - ND - mg/kg. 5 ND Test Report. No. CANEC1402177407 Date: 06 Mar 2014. Limit. Unit. MDL. 002. Dibromodiphenyl ether. - mg/kg. 5 ND Tribromodiphenyl ether. - mg/kg. 5 ND Tetrabromodiphenyl ether. - mg/kg. 5 ND Pentabromodiphenyl ether. - mg/kg. 5 ND Hexabromodiphenyl ether. - mg/kg. 5 ND Heptabromodiphenyl ether. - mg/kg. 5 ND Octabromodiphenyl ether. - mg/kg. 5 ND Nonabromodiphenyl ether. - mg/kg. 5 ND Decabromodiphenyl ether. - mg/kg. 5 ND Test Item(s). Page 3 of 8. Notes :. (1) The maximum permissible limit is quoted from the directive 2011/65/EU, Annex II.. Hexabromocyclododecane (HBCDD). Test Method :. Determination of HBCDD by GC-MS based on IEC 62321:2008.. Test Item(s). Unit. Hexabromocyclododecane (HBCDD). mg/kg. MDL. 002. 10 ND Notes :. (1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Hexabromocyclododecane (HBCDD) is considered as a priority for risk evaluation and substance restriction.. Phthalate. Test Method :. Determination of phthalates by GC-MS based on EN 14372:2004.. CAS NO. Unit. MDL. 002. Dibutyl Phthalate (DBP). 84-74-2. %(w/w). 0.003 ND Benzylbutyl Phthalate (BBP). 85-68-7. %(w/w). 0.003 ND Bis-(2-ethylhexyl) Phthalate (DEHP). 117-81-7. %(w/w). 0.003 ND Test Item(s). Test Report. Test Item(s). Diisobutyl Phthalate (DIBP). No. CANEC1402177407 Date: 06 Mar 2014. CAS NO. Unit. MDL. 002. 84-69-5. %(w/w). 0.003 ND Page 4 of 8. Notes :. (1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Bis (2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP) and Dibutyl phthalate (DBP) are considered as a priority for risk evaluation and substance restriction.. Test Report. No. CANEC1402177407 Date: 06 Mar 2014. Page 5 of 8. ATTACHMENTS RoHS Testing Flow Chart 1) Name of the person who made testing: Michael Tso / Cutey Yu 2) Name of the person in charge of testing: Adams Yu / Yolanda Wei 3) These samples were dissolved totally by pre-conditioning method according to below flow chart (Cr6+ and PBBs/PBDEs test method excluded). Sample Preparation Sample Measurement Pb/Cd/Hg Acid digestion with microwave/ hotplate Sample solvent extraction Filtration Concentration/ Dilution of extraction solution Solution Residue Filtration 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve ICP-OES/AAS DATA Cr6+ PBBs/PBDEs GC-MS DATA Nonmetallic material Adding digestion reagent Heating to 90~95℃ for extraction Filtration and pH adjustment Adding 1,5diphenylcarbazide for color development Metallic material Positive Spot test Negative Boiling water extraction Adding 1,5diphenylcarbazide for color development UV-Vis A red color indicates the presence of Cr6+. If necessary, confirm with UV-Vis. DATA DATA Test Report. No. CANEC1402177407 ATTACHMENTS HBCDD Testing Flow Chart 1) Name of the person who made testing: Cutey Yu 2) Name of the person in charge of testing: Yolanda Wei Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 06 Mar 2014. Page 6 of 8. Test Report. No. CANEC1402177407 ATTACHMENTS Phthalates Testing Flow Chart 1) Name of the person who made testing: Liu Qiong 2) Name of the person in charge of testing: Yolanda Wei Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 06 Mar 2014. Page 7 of 8. Test Report. No. CANEC1402177407 Date: 06 Mar 2014. Sample photo:. CANEC1402177407 CAN14-021774.002. SGS authenticate the photo on original report only. *** End of Report ***. Page 8 of 8.
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