Emerson Process Management Combination Ph Orp Sensor 396P Users Manual 51 RH.qxp
2015-02-06
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Instruction Manual PN 51-396P/rev.H March 2006 Models 396P and 396PVP Combination pH/ORP Sensor MODEL 396P MODEL 396PVP with mating cable DANGER HAZARDOUS AREA INSTALLATION ESSENTIAL INSTRUCTIONS READ THIS PAGE BEFORE PROCEEDING! Rosemount Analytical designs, manufactures, and tests its products to meet many national and international standards. Because these instruments are sophisticated technical products, you must properly install, use, and maintain them to ensure they continue to operate within their normal specifications. The following instructions must be adhered to and integrated into your safety program when installing, using, and maintaining Rosemount Analytical products. Failure to follow the proper instructions may cause any one of the following situations to occur: Loss of life; personal injury; property damage; damage to this instrument; and warranty invalidation. • Read all instructions prior to installing, operating, and servicing the product. If this Instruction Manual is not the correct manual, telephone 1-800-6547768 and the requested manual will be provided. Save this Instruction Manual for future reference. • If you do not understand any of the instructions, contact your Rosemount representative for clarification. • Follow all warnings, cautions, and instructions marked on and supplied with the product. • Inform and educate your personnel in the proper installation, operation, and maintenance of the product. • Install your equipment as specified in the Installation Instructions of the appropriate Instruction Manual and per applicable local and national codes. Connect all products to the proper electrical and pressure sources. • To ensure proper performance, use qualified personnel to install, operate, update, program, and maintain the product. • When replacement parts are required, ensure that qualified people use replacement parts specified by Rosemount. Unauthorized parts and procedures can affect the product’s performance and place the safe operation of your process at risk. Look alike substitutions may result in fire, electrical hazards, or improper operation. This sensor is not Intrinsically Safe. or Explosion Proof. Installations near flammable liquids or in hazardous area locations must be carefully evaluated by qualified on site safety personnel. To secure and maintain an intrinsically safe installation, an appropriate transmitter/ safety barrier/sensor combination must be used. The installation system must be in accordance with the governing approval agency (FM, CSA or BASEEFA/CENELEC) hazardous area classification requirements. Consult your analyzer/ transmitter instruction manual for details. Proper installation, operation and servicing of this sensor in a Hazardous Area Installation is entirely the responsibility of the user. CAUTION SENSOR/PROCESS APPLICATION COMPATIBILITY The wetted sensor materials may not be compatible with process composition and operating conditions. Application compatibility is entirely the responsibility of the user. About This Document This manual contains instructions for installation and operation of the Models 396P and 396PVP TUpH Combination pH/ORP Sensors. The following list provides notes concerning all revisions of this document. Rev. Level Date 0 8/95-2/01 A 12/01 Notes This is the initial release of the product manual. The manual has been reformatted to reflect the Emerson documentation style and updated to reflect any changes in the product offering. Added wiring diagram to page 14. B 4/02 Revised drawings on pages 6, 7, and 14. C 7/02 Added 1055 wiring diagrams. D 8/03 Added Silcore information. E 5/04 Added 5081 and Xmt wiring info. Deleted obsolete model information. G 11/05 Changed Figure 4-6 drawing on page 17. Resized Figure 1-1 drawing on page 2. H 3/06 Changed PN on Fig. 2-5, page 8, and in Table 7-3, page 29. Added a note on page 11. Emerson Process Management Liquid Division 2400 Barranca Parkway Irvine, CA 92606 USA Tel: (949) 757-8500 Fax: (949) 474-7250 http://www.raihome.com © Rosemount Analytical Inc. 2006 MODEL 396P and 396PVP TABLE OF CONTENTS MODEL 396P and 396PVP COMBINATION pH/ORP SENSOR TABLE OF CONTENTS Section 1.0 1.1 1.2 1.3 Title DESCRIPTION AND SPECIFICATIONS................................................................. Features and Applications........................................................................................ Physical Specifications............................................................................................. Ordering Information ................................................................................................ Page 1 1 2 3 2.0 2.1 2.2 INSTALLATION ....................................................................................................... Unpacking and Inspection........................................................................................ Mounting .................................................................................................................. 5 5 5 3.0 WIRING MODEL 396P-01 ....................................................................................... 10 4.0 WIRING MODELS 396P-02 AND 396PVP.............................................................. 16 5.0 5.1 5.2 START UP AND CALIBRATION ............................................................................. Model 396P pH ........................................................................................................ Model 396P ORP ..................................................................................................... 24 24 24 6.0 6.1 6.2 6.3 MAINTENANCE ...................................................................................................... Automatic Temperature Compensator ..................................................................... Model 396P pH ........................................................................................................ Model 396P ORP ..................................................................................................... 25 25 25 26 7.0 7.1 27 7.2 DIAGNOSTICS AND TROUBLESHOOTING.......................................................... Diagnostics & Troubleshooting With the Models 54e, 1055, 3081, 81, 4081, 5081. and Xmt.................................................................................................................... Troubleshooting Without Advanced Diagnostics...................................................... 27 28 8.0 RETURN OF MATERIAL......................................................................................... 30 LIST OF TABLES Number 1-1 3-1 4-1 5-1 6-1 6-2 7-1 7-2 7-3 Title Recommended Accessories for First Time Installations ........................................... Wiring Matrix Guide - Model 396P ........................................................................... Wiring Matrix Guide - Model 396PVP....................................................................... ORP of Saturated Quinhydrone Solution (In Millivolts)............................................. Ro and R1 Values for Temperature Compensation Elements .................................. Temperature vs Resistance of Auto T.C. Elements .................................................. Troubleshooting With Advanced Diagnostics ........................................................... Troubleshooting Without Advanced Diagnostics ...................................................... Model 396P Replacement Parts and Accessories.................................................... i Page 4 10 16 24 25 25 27 28 29 MODEL 396P and 396PVP TABLE OF CONTENTS LIST OF FIGURES Number Title Page 1-1 Cross Section Diagram of the TUpH Patented Reference Technology ............................................................................... 2 2-1 Dimensional Drawing .......................................................................................................................................................... 6 2-2 Flow-Through Tee with Adapter (PN 915240-xx)................................................................................................................. 6 2-3 Flow-Through and Insertion Installations ........................................................................................................................... 7 2-4 Model 396P/396PVP with Insertion Mounting Adapter (PN 23242-02) ............................................................................... 7 2-5 Submersion Installations .................................................................................................................................................... 8 2-6 Low Flow Cell PN 23728-00................................................................................................................................................ 9 2-7 Jet Spray Cleaner PN 12707-00.......................................................................................................................................... 10 3-1 Wire Functions for Model 396P with & without Preamplifier................................................................................................ 10 3-2 Wiring Details Model 396P-01-50 for use with & without Junction Box (PN 22719-02) for Models 1181, 1050, & 1060 .... 12 3-3 Wiring Details Model 396P-01-54 for use with & sithout Junction Box (PN 22719-02) for Models 1054/A/B, 2054, 2081 and Extension Cable (PN 9200254).................................................................................................................................... 13 3-4 Wiring Details Model 396P-01-55 for use with Junction Box (PN 23550-00) for Models 54, 3081, 4081, 81, and 5081 ... 14 3-5 Wiring Details Model 396P-01-55 for use with Models 54, 81, 3081, 4081, and 5081........................................................ 15 3-6 Wiring Model 396P-01)-( )-55 Sensor to Model 1055-10-22-32 Analyzer ........................................................................... 15 4-1 Wire Functions for Mating Variopol Cable used with Model 396PVP .................................................................................. 17 4-2 Connector Pins and their Functions .................................................................................................................................... 17 4-3 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Model 81 ....... 17 4-4 Wiring Details for Models 396PVP or 396P-02-50 with Mating Variopol Cable (PN 23645-07) for use with Model 1181 ... 17 4-5 Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-07) for use with Model 2081 ... 17 4-6 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Models 3081, 4081, and 5081 ................................................................................................................................................................... 17 4-7 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote ........ Junction Box (PN 23555-00) to Model 81 ........................................................................................................................... 18 4-8 Wiring Details for Models 396PVP or 396P-02-50 with Mating Variopol Cable (PN 23645-07) for use with Remote ........ Junction Box (PN 23309-03) to Model 1181........................................................................................................................ 18 4-9 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Model 54 ...... 18 4-10 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote ........ Junction Box (PN 23555-00) to Model 54 ........................................................................................................................... 18 4-11 Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-06) for use with Remote ........ Junction Box (PN 23309-03) to Model 2081 ....................................................................................................................... 19 4-12 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote ........ Junction Box (PN 23555-00) to Models 3081 and 4081...................................................................................................... 19 4-13 Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-07) for use with Model 1054 ... 19 4-14 Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-07) for use with ...................... Model SCL-(P/Q) ................................................................................................................................................................. 19 4-15 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Model 1055 ... 20 4-16 Wiring Model 396P-(02)-( )-54/55-(61) Sensor to Model 1055-01-10-22-32 Analyzer ........................................................ 20 4-17 Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote ........ Junction Box (PN 23557-00) to Model 1055 ....................................................................................................................... 20 4-18 Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-06) for use with Models .......... 1054A/B and 2054............................................................................................................................................................... 21 4-19 Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-06) for use with Remote ........ Junction Box (PN 23309-04) to Models 1054A/B and 2054................................................................................................ 21 4-20 Wiring to Model 54e pH/ORP with Variopol........................................................................................................................ 21 4-21 Wiring Details Model 396P-02-50 for use with Junction Box (PN 23309-03), Remote Preamplifier, and Extension .......... Cable (PN 9200254)............................................................................................................................................................ 22 4-22 Wiring Details Model 396P-02-54 for use with Junction Box (PN 23309-04), Remote Preamplifier (PN 22698-03), and .. Extension Cable (PN 9200254)........................................................................................................................................... 22 4-23 Wiring Model 396P-01 to Model Xmt-P-HT-10 ................................................................................................................... 23 4-24 Wiring Models 396P-02 and 396PVP to Model Xmt-P-HT-10 ............................................................................................ 23 ii MODEL 396P and 396PVP SECTION 1.0 DESCRIPTIONS AND SPECIFICATIONS SECTION 1.0 DESCRIPTION AND SPECIFICATIONS 1.1 FEATURES AND APPLICATIONS The Rosemount Analytical Model 396P and 396PVP Sensors measure the pH or the ORP of aqueous solutions in pipelines, open tanks, or ponds. It is designed for harsh, dirty applications such as sourwater waste treatment and scrubbers, where a high performance, low maintenance, disposable sensor is required. The combination electrode features a patented, large area polypropylene reference junction for resistance to process coatings, generally found in dirty, high solid applications. The patented helical reference pathway provides added resistance for poisoning applications. In addition, it is available in two configurations: glass/platinum electrode completely recessed within the reference junction for added life in abrasive or rough applications and the glass/platinum electrode partially exposed for added life and accuracy in viscous and low flow applications. Both Models feature a titanium solution ground constructed in an annular design around the pH/ORP electrode. The solution ground provides glass and reference sensor diagnostics for preventative maintenance when used with the Model 54e, 1055, 5081, 3081, 4081, 81 pH/ORP, and Xmt-P transmitters. In addition Models 396P and 396PVP can be used with most nondiagnostic Rosemount Analytical and other manufacturer’s instruments. Each sensor is housed in a molded polypropylene body with EPDM seals, making it virtually indestructible and chemically resistant. Complete encapsulation eliminates leakage or high humidity problems traditionally found in other pH/ORP designs. The simplified construction, designed with user convenience in mind, does not require electrolyte (KCl) replenishment or any high maintenance troubleshooting procedures. The Model 396P is offered with or without an optional integral preamplifier to convert the high impedance pH or ORP mV signal into a stable, noise-free signal with transmission capability of up to three miles. A remote preamplifier must be used with Model 396PVP. Model 396PVP is offered with a watertight sensor-tocable connector which eliminates re-wiring and cable twisting when replacing sensors. The Variopol VP multiple pin connector is an integral part of each sensor model and uses a mating VP cable. Once the cable is installed and wired to the analyzer, sensors are easily replaced without replacing the cable, and, if the replacement sensor is the same as its predecessor, without rewiring the analyzer. Also the cable can be disconnected from the sensor before removal from the process which eliminates cable twisting. The entire line of TUpH model sensors now incorporate the new SILCORE technology contaminant barrier. This triple-seal barrier prevents moisture and material impurities from migrating to the pH sensor’s reference electrode’s metal lead wire. By preventing these contaminants from compromising the integrity of the pH measurement, sensor life is increased, especially at higher temperatures where increased migrations occur. In addition, the SILCORE technology provides added protection against sensor failure due to vibrations and shock by transferring damaging energy away from the glass-to-metal seal. The AccuGLASS pH glass formulations exceed industry standards. The AccuGlass pH glass is a result of many years of glass research resulting in a formulation which has been found to increase the life of the sensor. Unlike other pH glasses presently on the market, this glass resists cracking especially at higher temperatures and reduces sodium ion error commonly found in high pH applications. Overall, the AccuGlass formulation enhances the sensor performance to measure pH more accurately and have a longer sensor life than ever before. AccuGlass and Silcore are trademarks of Rosemount Analytical. Installation is easily achieved through the wide variety of mounting configurations. The Models 396P and 396PVP feature 1 in. (MNPT) front and rear facing connections for insertion, submersion or flow through pH and ORP applications. 1 MODEL 396P and 396PVP SECTION 1.0 DESCRIPTIONS AND SPECIFICATIONS FIGURE 1-1. Cross Section Diagram of the TUpH Patented Reference Technology All TUpH sensors are designed with a large area reference junction, helical reference pathway, and an AccuGlass pH glass bulb. This patented sensor technology ensures superior performance while only requiring minimal maintenance. 1.2 SPECIFICATIONS Measurements and Ranges Available pH ACCUGLASS Types Wetted Materials Process Connection Temperature Range Pressure Range-Hemi bulb Pressure Range-Flat bulb Minimum Conductivity Integral Cable Preamplifier Options Weight/Shipping Weight *pH: 0-14 ORP: -1500 to 1500 mv GPLR hemi or flat glass Titanium, Polypropylene, EPDM, glass; platinum (ORP only) 1 in. MNPT front and rear facing threads 0-100°C (32-212°F) 100-1135 kPa [abs] (0-150 psig) 100-790 kPa [abs] (0-100 psig) 75 μS/cm, nominal; 100 μS/cm 396P: Code 01 - 25 ft; Code 02 - 15 ft coaxial 396PVP: none - must use mating VP cable 396P: Remote or Integral 396PVP: Remote only 0.45 kg/0.9 kg (1 lb/2 lb) PERCENT LINEARITY* pH range 2 GPLR hemi bulb GPLR flat bulb 0 - 2 pH 94% — 2 - 12 pH 99% 98% 12 - 13 pH 97% 95% 13 - 14 pH 92% — MODEL 396P and 396PVP SECTION 1.0 DESCRIPTIONS AND SPECIFICATIONS 1.3 ORDERING INFORMATION The Model 396P Sensor is housed in a molded reinforced polypropylene body with 1 in. MNPT threads suitable for insertion, submersion or flow through installation. The sensor includes a general purpose pH electrode or a platinum ORP electrode, a patented reference junction and a solution ground. The Model 396P comes standard with a recessed electrode; an optional slotted tip is also available. In addition, the 396P features an optional integral hermetically sealed preamplifier and 15 ft or 25 ft cable lengths. Automatic temperature compensation, Pt 100 or 3K Balco, is standard with the Model 396P. MODEL 396P TUpH INSERTION/SUBMERSION POLYPROPYLENE pH/ORP SENSOR CODE 01 PREAMPLIFIER/CABLE (Required Selection) With integral preamplifier, 25 ft cable 02 Without integral preamplifier, 15 ft cable CODE 10 MEASURING ELECTRODE TYPE (Required Selection) GPLR hemi bulb, General Purpose Low Resistivity (0-14 pH) 12 ORP 13 GPLR flat bulb, General Purpose Low Resistivity (2 - 13 pH) CODE 50 ANALYZER/TC COMPATIBILITY (Required Selection) For Models 1181 (3K TC) 54 For Models 1054A/B, 2054, 2081 (Pt 100 RTD) 55 For Models 54e, 3081, 81, 4081, 1055, 5081, Xmt (PT-100 RTD) CODE 41 396P The Model 396P insertion/submersion sensor with integral cable is offered with or without a built-in preamplifier OPTIONAL SELECTION Slotted Tip (not available on flat bulb sensors) - 01 - 10 - 55 EXAMPLE NOTE: The Model 396P is also compatible with Model SCL-P/Q (option 02-54 only). TABLE 1-1. RECOMMENDED ACCESSORIES FOR FIRST TIME INSTALLATIONS 1. Mounting Accessories (optional) Choose one: PN 915240-03, PVC flow through tee, 3/4 in. NPT process connection PN 915240-04, PVC flow through tee, 1 in. NPT process connection PN 915240-05, PVC flow through tee, 1-1/2 in. NPT process connection PN 23728-00, acrylic low flow cell PN 2002011, 1-1/2 in. CPVC tee with 1-in. FNPT connection PN 11275-01, sensor handrail assembly 2. Junction Boxes (optional) Remote Junction Boxes (used with option -02 sensors, for sensor to analyzer distances of more than 15 ft) Choose one: PN 23555-00 includes preamplifier for Models 54, 81, 3081, 4081, 5081, Xmt PN 23309-03 and PN 22698-02 plug-in preamplifier for Model 1181Analyzer PN 23309-04 and PN 22698-03 plug-in preamplifier for Models 1054A/B series, 2054, 2081 Analyzers Choose one: PN 9120516 BNC Adapter for use with remote junction boxes PNs 23309-03, 23309-04 Remote Junction Box (used with option -01 sensors) Choose one: PN 23550-00 cable extension board 3. Extension cables (used with remote junction boxes) Choose one: PN 23646-01, 11 conductor, shielded, prepped PN 9200273, 11 conductor, shielded, unprepped 3 MODEL 396P and 396PVP SECTION 1.0 DESCRIPTIONS AND SPECIFICATIONS The Model 396PVP Sensor has similar features to the Model 396P. However, the Model 396PVP is offered with the new Variopol (VP) connector and uses a mating VP cable (purchased separately). A remote preamplifier must be used with this sensor. A Variopol cable is required for all new installations. See below for cable selection. The Model 396PVP insertion/ submersion sensor with the VP (Variopol) connector MODEL 396PVP TUpH INSERTION/SUBMERSION POLYPROPYLENE pH/ORP SENSOR CODE 10 MEASURING ELECTRODE TYPE (Required Selection) GPLR hemi bulb, General Purpose Low Resistivity (0-14 pH) 12 ORP 13 GPLR flat bulb, General Purpose Low Resistivity (2 - 13 pH) CODE 50 ANALYZER/TC COMPATIBILITY (Required Selection) For Models 1181 (3K TC) 54 For Models 1054A/B, 2054, 2081 (Pt 100 RTD) 55 For Models 54e, 3081, 81, 4081, 1055, 5081, Xmt (PT-100 RTD) CODE 41 OPTIONAL SELECTION Slotted Tip (not available on flat bulb sensors) PN 23645-06 MATING VP CONNECTOR CABLE (Required for all new installations) 15 ft. cable with mating VP connector, prepped with BNC on analyzer end 23645-07 15 ft. cable with mating VP connector, prepped without BNC on analyzer end* *For use with connections to Models 1181, 1054A/B, 2081, 54e, 81, 3081, 4081, 5081, Xmt, and remote junction box PN 23555-00. OTHER ACCESSORIES FOR MODELS 396P AND 396PVP PART 22698-00 22698-02 22698-03 22743-01 22744-01 23557-00 9210012 9210013 9210014 R508-160Z 12707-00 DESCRIPTION Preamplifier plug-in for junction box, for Model 1003, Preamplifier plug-in for junction box, for Models 1181, 1050 Preamplifier plug-in for junction box, for Models 1054A/B, 2054, 2081 Pt100 preamplifier for Model 1181 3K Preamplifier for Model 1181 Preamplifier for junction box for Models 54, 3081, 81, 4081, 5081 Buffer solution, 4.01 pH, 16 oz Buffer solution, 6.86 pH, 16 oz Buffer solution, 9.18 pH, 16oz ORP solution, 460 mv ± 10 at 20°C Jet Spray Cleaner Examples of all sensing tip offerings Shrouded Tip is standard on all hemi bulb sensors 4 Optional Slotted Tip is available on all hemi bulb sensors, ordered as option -41 Flat Tip is available with flat glass bulb sensors Variopol connector shown with mating variopol cable receptacle MODEL 396P and 396PVP SECTION 2.0 INSTALLATION SECTION 2.0 INSTALLATION 2.1 UNPACKING AND INSPECTION. Inspect the outside of the carton for any damage. If damage is detected, contact the carrier immediately. Inspect the hardware. Make sure all the items in the packing list are present and in good condition. Notify the factory if any part is missing. If the sensor appears to be in satisfactory condition, proceed to Section 2.2, Mounting. NOTE Save the original packing cartons and materials as most carriers require proof of damage due to mishandling, etc. Also, if it is necessary to return the sensor to the factory, you must pack the sensor in the same manner as it was received. Refer to Section 6.0 for return instructions. If the sensor is to be stored, the vinyl boot should be filled with pH buffer solution and replaced on sensor tip until ready to use. CAUTION Buffer solution, in the vinyl boot, may cause skin or eye irritation. 2. Do not install the sensor on the horizontal. The sensor must be 10° off the horizontal to ensure accuracy. 3. Do not install the sensor upside down. 4. Air bubbles may become trapped in the sensor end between the glass bulb and the sensor body. This problem is most commonly encountered in areas of low flow or during calibration. Shake the probe while immersed in solution to remove bubbles. This problem can be avoided by ordering the sensor with the slotted tip (option -41). In most cases, the pH sensor can simply be installed as shipped and readings with an accuracy of ± 0.6 pH may be obtained. To obtain greater accuracy or to verify proper operation, the sensor must be calibrated as a loop with its compatible analyzer or transmitter. 2.2.1 Flow Through and Insertion Mounting. Model 396P and 396PVP Sensors have a 1-inch MNPT process connection at the front of the sensor for mounting into a 1-1/2 inch tee or the process pipes. See Figure 2-1 through Figure 2-7 for installation configurations. NOTE LARGE PIPE WRENCHES MUST NOT BE USED TO TIGHTEN THE SENSOR INTO A FLANGE OR OTHER TYPE OF MOUNTING. WARNING Glass electrode must be wetted at all times (in storage and in line) to maximize sensor life. 2.2 MOUNTING. The sensor has been designed to be located in industrial process environments. Temperature and pressure limitations must not be exceeded at any time. A caution label regarding this matter is attached to the sensor. Please do not remove the label. See Figure 2-1. CAUTION Internal electrolyte fill solution may cause skin or eye irritation. Mounting Guidelines: 1. Shake the sensor in a downward motion to remove any air bubbles that may be present inside the tip of the pH glass. 2.2.2 Submersion Mounting. Model 396P and 396PVP Sensors also have a 1 inch MNPT process connection at the back of the sensor. Utilizing a standard 1 inch union, the sensor may be mounted to a 1 inch SCH 80 CPVC or PVDF standpipe (see Figure 2x). Tapered pipe threads in plastic tend to loosen after installation. It is therefore recommended that Teflon1 tape be used on the threads and that the tightness of the connection be checked frequently to assure that no loosening has occurred. To prevent rain water or condensation from running into the sensor, a weatherproof junction box is recommended (see Figure 2-x). The sensor cable must be run through a protective conduit for isolation from electrical interference or physical abuse from the process. The sensor should be installed within 80° of vertical, with the electrode facing down. The sensor’s cable should not be run with power or control wiring. 1 Teflon is a registered trademark of E.I. du Pont de Nemours & Co. 5 MODEL 396P and 396PVP SECTION 2.0 INSTALLATION SENSOR CABLE (OR VP CONNECTOR - NOT SHOWN) MILLIMETER INCH DWG. NO. 40396P01 FIGURE 2-1. Dimensional Drawing MILLIMETER INCH xx* 03 04 05 SENSOR CABLE (OR VP CONNECTOR - NOT SHOWN) Process Connection Threads 3/4 inch 1 inch 1-1/2 inch FIGURE 2-2. Flow-Through Tee with Adapter (PN 915240-xx*) 6 REV. D MODEL 396P and 396PVP SECTION 2.0 INSTALLATION WHEN INCH AND METRIC DIMS ARE GIVEN MILLIMETER INCH 1-1/2” X 1” Reducing Bushing 1-1/2” X 1” Reducing Bushing 1-1/2” Pipe Tee PN 2002011 ANGLE FLOW SHOWN FLOW STRAIGHT FLOW SHOWN 1-1/2” Pipe Tee PN 2002011 1-1/2” X 1” Reducing Bushing PIPE “Y” INSTALLATION SHOWN 1-1/2” PIPE “Y” FIGURE 2-3. Flow-Through and Insertion Installations DWG. NO. 40396P02 REV. A FIGURE 2-4. Model 396P with Insertion Mounting Adapter (PN 23242-02). Not for use with Model 396PVP. Mounting adapter allows for sensor removal without twisting or disconnecting interconnecting cable for ease of maintenance. 7 MODEL 396P and 396PVP SECTION 2.0 INSTALLATION WHEN INCH AND METRIC DIMS ARE GIVEN MILLIMETER INCH DWG. NO. 40396P03 REV. A Handrail Mounting Assembly PN 11275-01 DWG. NO. 40396P04 FIGURE 2-5. Submersion Installations 8 REV. A MODEL 396P and 396PVP MILLIMETER INCH SECTION 2.0 INSTALLATION SENSOR CABLE (OR VP CONNECTOR - NOT SHOWN) FIGURE 2-6. Low Flow Cell PN 23728-00 FIGURE 2-7. Jet Spray Cleaner PN 12707-00 9 MODEL 396P and 396PVP SECTION 3.0 WIRING - MODEL 396P SECTION 3.0 WIRING — MODEL 396P-01 Figures in this section provide the guidelines for wiring the 396P-01 sensor to various Analyzer/Transmitter instruments. 2. To determine which wiring guideline to use, locate the model number of the sensor to be installed. 1. If the cable needs to be extended, use a high quality eleven conductor double shielded instrument cable available from Rosemount Analytical. Refer to Table 3-1 for the appropriate junction box to use and the corresponding wiring details. Signal cable should be run in a dedicated conduit (preferably an earth grounded metallic conduit) and should be kept away from AC power lines. For your convenience, a wire nut kit is furnished (in a plastic bag wrapped around the cable). NOTE For maximum EMI/RFI protection when wiring from the sensor to the junction box, the outer braid of the sensor should be connected to the outer braided shield of the extension cable. The outer braid of the extension cable to the instrument must be terminated at earth ground or by using an appropriate metal cable gland fitting that provides a secure connection to the instrument cable. NOTE If the cable is too long, loop up the excess cable. If the cable has to be shortened, cut and terminate each conductor neatly and make sure that the overall (outermost) drain wire is not shorted out with either of the two inner drain wires (shields). TABLE 3-1. Wiring Matrix Guide Preamplifier Location Sensor Model Options Integral to Integral to Remote Sensor Analyzer Junction Box (PN) 396P-01-()-50 396P-01-()-50 396P-01-()-54 396P-01-()-54 396P-01-()-55 396P-01-()-55 396P-01-()-55 10 Analyzer/Transmitter Interconnect 1054A, 54e, 81, 1055 (unprepped 1054B, 2054 3081, PN) 2081 4081, 5081 Ext. box (22719-02) 9200254 Ext. box (22719-02) 9200254 Ext. box (23550-00) 9200273 9200273 or 23646-01 1181 1050 1060 1003 SCL or Refer to 1023 SoluCube Figure # 3-2 3-2 3-3 3-3 3-5 3-4 3-6 MODEL 396P and 396PVP Wiring. The Model 396P has an optional built-in preamplifier and is offered with a shielded cable. The cable should be handled carefully and kept dry and free of corrosive chemicals at all times. Extreme care should be used to prevent it from being twisted, damaged or scraped by rough, sharp edges or surfaces. Please refer to Figures 3-1 through 3-6 for wiring Model 396P-01. SECTION 3.0 WIRING - MODEL 396P DANGER DO NOT CONNECT SENSOR CABLE TO POWER LINES. SERIOUS INJURY MAY RESULT. NOTE Remove electrical tape or shrink sleeve from gray reference wire before connecting wire to terminal. Model 396P Option 01 (with preamplifier) cable Model 396P Option 02 (without preamplifier) cable FIGURE 3-1. Wire Functions for Model 396P with and without Preamplifier 11 MODEL 396P and 396PVP SECTION 3.0 WIRING - MODEL 396P WHEN INCH AND METRIC DIMS ARE GIVEN MILLIMETER INCH DWG. NO. 40396P15 FIGURE 3-2. Wiring Details Model 396P-01-50 for use with and without Junction Box (PN 22719-02) for Model 1181. 12 REV. B MODEL 396P and 396PVP SECTION 3.0 WIRING - MODEL 396P WHEN INCH AND METRIC DIMS ARE GIVEN MILLIMETER INCH DWG. NO. 40396P13 REV. D FIGURE 3-3. Wiring Details Model 396P-01-54 for use with and without Junction Box (PN 22719-02) for Models 1054A, 1054B, 2054, 2081, and Extension Cable (9200254). 13 MODEL 396P and 396PVP SECTION 3.0 WIRING - MODEL 396P WHEN INCH AND METRIC DIMS ARE GIVEN MILLIMETER INCH DWG. NO. 40396P08 FIGURE 3-4. Wiring Details Model 396P-01-55 for use with Junction Box (PN 23550-00) for Models 54e, 3081, 4081, 81, and 5081. 14 REV. B MODEL 396P and 396PVP SECTION 3.0 WIRING - MODEL 396P FIGURE 3-5. Wiring Details Model 396P-01-55 for use with Models 54e, 81, 3081, 4081, and 5081 FIGURE 3-6. Wiring Model 396P-01-( )--55 Sensor to Model 1055-10-22-32 Analyzer 15 MODEL 396P and 396PVP SECTION 4.0 WIRING - MODEL 396PVP SECTION 4.0 WIRING — MODELS 396P-02 AND 396PVP Figures 4-1 thru 4-22 provide the guidelines for wiring the sensor to various Analyzer/Transmitter instruments. To determine which wiring guideline to use, locate the model number of the sensor to be installed. 1. If the cable needs to be extended, use a high quality eleven conductor double shielded instrument cable available from Rosemount Analytical. Refer to Table 4-1 to refer to the appropriate junction box to use and the corresponding wiring details. NOTE If the cable is too long, loop up the excess cable. If the cable has to be shortened, cut and terminate each conductor neatly and make sure that the overall (outermost) drain wire is not shorted out with either of the two inner drain wires (shields). 2. Signal cable should be run in a dedicated conduit (preferably an earth grounded metallic conduit) and should be kept away from AC power lines. For your convenience, a wire nut kit is furnished (in a plastic bag wrapped around the cable). NOTE For maximum EMI/RFI protection when wiring from the sensor to the junction box, the outer braid of the sensor should be connected to the outer braided shield of the extension cable. The outer braid of the extension cable to the instrument must be terminated at earth ground or by using an appropriate metal cable gland fitting that provides a secure connection to the instrument cable. TABLE 4-1. Wiring Matrix Guide Preamplifier Location Sensor Model Options Integral to Integral to Sensor Analyzer 396P-02-()-55 396PVP-55 396P-02-()-50 396PVP-50 Remote Junction Box (PN) Analyzer/Transmitter Interconnect 1054A, 54, 81, 1055 (unprepped 1054B, 2054 3081, PN) 2081 4081, 5081 1181 1050 1060 1003 SCL or Refer to 1023 SoluCube Figure # 4-3, 4-6, 4-9 4-4 396P-02-()-50 396PVP-50 23309-03 9200254 4-22 396P-02-()-50 396PVP-50 23309-03 9200273 or 23646-01 4-8 396P-02-()-54 23309-04 9200254 4-23 396P-02-()-54 396PVP-54 23309-04 9200273 or 23646-01 4-20 4-5, 4-18 4-19 396P-02-()-54 396PVP-54 396P-02-()-55 396PVP-55 396P-02-()-54 396PVP-54 23555-00 396P-02-54 396PVP-54 396P-02-55 396PVP-55 396P-02-55 396PVP-55 16 9200273 or 23646-01 4-7, 4-10 4-12 661-898695 23309-04 9200273 or 23646-01 9200273 or 23646-01 4-14 4-11 4-21 4-15 4-16 4-17 MODEL 396P and 396PVP SECTION 4.0 WIRING - MODEL 396PVP FIGURE 4-1. Wire Functions for Mating Variopol Cable used with Model 396PVP FIGURE 4-2. Connector Pins and Their Functions FIGURE 4-3. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Model 81 FIGURE 4-4. Wiring Details for Models 396PVP or 396P-02-50 with Mating Variopol Cable (PN 23645-07) for use with Model 1181 FIGURE 4-5. Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-07) for use with Model 2081 FIGURE 4-6. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Models 3081, 4081, 5081 17 MODEL 396P and 396PVP FIGURE 4-7. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote Junction Box (PN 23555-00) to Model 81 FIGURE 4-9. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Model 54/54e 18 SECTION 4.0 WIRING - MODEL 396PVP FIGURE 4-8. Wiring Details for Models 396PVP or 396P-02-50 with Mating Variopol Cable (PN 23645-06) for use with Remote Junction Box (PN 23309-03) to Model 1181 FIGURE 4-10. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote Junction Box (PN 23555-00) to Model 54/54e MODEL 396P and 396PVP FIGURE 4-11. Wiring Details for Models 396PVP or 396P02-54 with Mating Variopol Cable (PN 23645-06) for use with Remote Junction Box (PN 23309-04) to Model 2081 FIGURE 4-13. Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-07) for use with Model 1054 SECTION 4.0 WIRING - MODEL 396PVP FIGURE 4-12. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote Junction Box (PN 23555-00) to Models 3081, 4081, & 5081 FIGURE 4-14. Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-07) for use with Model SCL-(P/Q) 19 MODEL 396P and 396PVP SECTION 4.0 WIRING - MODEL 396PVP FIGURE 4-15. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Model 1055 FIGURE 4-16. Wiring Model 396P-(02)-( )--54/55-(61) Sensor to Model 1055-01-10-22-32 Analyzer FIGURE 4-17. Wiring Details for Models 396PVP or 396P-02-55 with Mating Variopol Cable (PN 23645-07) for use with Remote Junction Box (PN 23557-00) to Model 1055 NOTE: This wiring diagram can also be used for wiring a Model 396P-01. The wire colors and functions for the extension cable (PN 9200273) are the same as the 396P-01 wire colors and functions. 20 MODEL 396P and 396PVP SECTION 4.0 WIRING - MODEL 396PVP FIGURE 4-18. Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-06) for use with Models 1054A/B & 2054 FIGURE 4-19. Wiring Details for Models 396PVP or 396P-02-54 with Mating Variopol Cable (PN 23645-06) for use with Remote Junction Box (PN 23309-04) to Models 1054A/B and 2054 FIGURE 4-20. Wiring to Model 54e pH/ORP with Variopol 21 MODEL 396P and 396PVP SECTION 4.0 WIRING - MODEL 396PVP DWG. NO. 40396P25 REV. A FIGURE 4-21. Wiring Details Model 396P-02-50 for use with Junction Box (PN 23309-03) and Remote Preamplifier, Extension Cable (PN 9200254). DWG. NO. 40396P24 FIGURE 4-22. Wiring Details Model 396P-02-54 for use with Junction Box (PN 23309-04) and Remote Preamplifier (PN 22698-03), Extension Cable (9200254). 22 REV. A MODEL 396P and 396PVP SECTION 4.0 WIRING - MODEL 396PVP FIGURE 4-23. Wiring Model 396P-01 to Model Xmt-P-HT-10 FIGURE 4-24. Wiring Models 396P-02 and 396PVP to Model Xmt-P-HT-10 23 MODEL 396P and 396PVP SECTION 5.0 START UP AND CALIBRATION SECTION 5.0 START UP AND CALIBRATION 5.1 MODELS 396P and 396PVP pH SENSORS 5.1.1 SENSOR PREPARATION. Shake down the sensor to remove any air bubbles that may be present at the tip of the pH glass bulb. In most cases, the pH sensor can simply be installed as shipped and readings with an accuracy of ± 0.6 pH may be obtained. To obtain greater accuracy or to verify proper operation, the sensor must be calibrated as a loop with its compatible analyzer or transmitter. 1. While obtaining a process solution sample (it is recommended that the sample is taken close to the sensor), record the pH value that is shown on the analyzer/transmitter display. 2. Measure and record the pH of the process solution sample with another temperature compensated, calibrated pH instrument. For best results, standardization should be performed at the process temperature. 3. Adjust the analyzer/transmitter value to the standardized value. 5.1.2 pH CALIBRATION. After a temporary connection is established between the sensor and the instrument, a buffer calibration may be performed. Consult appropriate pH/ORP analyzer or transmitter instruction manual for specific calibration and standardization procedures, or see below for recommended two-point buffer calibration procedure. Recommended two-point buffer calibration procedure: Select two stable buffer solutions, preferably pH 4.0 and 10.0 (pH buffers other than pH 4.0 and pH 10.0 can be used as long as the pH values are at least two pH units apart). NOTE A pH 7.0 buffer solution reads a mV value of approximately zero, and pH buffers read approximately 59.1 mV for each pH unit above or below pH 7.0. Check the pH buffer manufacturer specifications for millivolt values at various temperatures since it may affect the actual value of the buffer solution mV/pH value. 1. Immerse sensor in the first buffer solution. Allow sensor to adjust to the buffer temperature (to avoid errors due to temperature differences between the buffer solution and sensor temperature) and wait for reading to stabilize. Value of buffer can now be acknowledged by analyzer/transmitter. 2. Once the first buffer has been acknowledged by the analyzer/transmitter, rinse the buffer solution off of the sensor with distilled or deionized water. 3. Repeat steps 1 and 2 using the second buffer solution. 4. Once the analyzer/transmitter has acknowledged both buffer solutions, a sensor slope (mV/pH) is established (the slope value can be found within the analyzer/ transmitter). 5. The slope value should read about 59.1 mV/pH for a new sensor and will decrease over time to approximately 4749 mV/pH. Once the slope reads below the 47-49 mV/pH range, a new sensor should be installed to maintain accurate readings. 5.2 MODEL 396P and 396PVP ORP SENSORS 5.2.1 SENSOR PREPARATION. Most industrial applications have a number of ORP reactions occurring in sequence or simultaneously. There can be several components that are oxidized or reduced by the reagents that are used. Theoretically, the ORP potential is absolute because it is the result of the oxidation-reduction equilibrium. However, the actual measured potential is dependent on many factors, including the condition of the surface of the ORP platinum electrode. Therefore, the sensor should be allowed 1-2 hours to become “conditioned” to the stream when first set-up or after being cleaned. 5.2.2 ORP CALIBRATION 1. Make a temporary electrical connection between the sensor and the instrument. 2. Obtain an ORP standard solution, or a standard solution can also be made quite simply by adding a few crystals of quinhydrone to either pH 4 or pH 7 buffer. Quinhydrone is only slightly soluble therefore a few crystals will be required. (Refer to Section 4.3. for an alternate ORP standard solution). 3. Immerse the sensor in the standard solution. Allow 1-2 minutes for the ORP sensor to stabilize. 4. Adjust the standardize control of the instrument to the solution value shown in Table 5-1 (below) or on the label of the standard solution. The resulting potentials, measured with a clean platinum electrode and saturated KCl/AgCl reference electrode, should be within ±20 millivolts of the value. Solution temperature must be noted to ensure accurate interpretation of results. The ORP value of saturated quinhydrone solution is not stable over long periods of time. Therefore, these standards should be made up fresh each time they are used. 5. Remove the sensor from the buffer, rinse and install in the process. TABLE 5-1. ORP of Saturated Quinhydrone Solution (In Millivolts) Recommended pH Sensor Standardization: For maximum accuracy, the sensor can be standardized online or with a process grab sample after a buffer calibration has been performed and the sensor has been conditioned to the process. Standardization accounts for the sensor junction potential and other interferences. Standardization will not change the sensor’s slope but will simply adjust the analyzer’s reading to match that of the known process pH. 24 Temp °C Millivolt Potential pH 4 Solution 20 25 30 268 264 260 pH 7 Solution 20 25 30 94 87 80 MODEL 396P and 396PVP SECTION 6.0 MAINTENANCE SECTION 6.0 MAINTENANCE The Model 396P and 396PVP Sensors require minimum maintenance. The sensor should be kept clean and free of debris and sediment at all times. The frequency of cleaning by wiping or brushing with a soft cloth or brush is determined by the nature of the solution being measured. The sensor should be removed from the process periodically and checked in buffer solutions. WARNING BEFORE REMOVING THE SENSOR, be absolutely certain that the process pressure is reduced to 0 psig and the process temperature is lowered to a safe level! If the sensor will not calibrate, refer to your analyzer/ transmitter instruction manual for proper test procedures. If it is determined that the sensor has failed, it should be discarded and replaced. 6.1 AUTOMATIC TEMPERATURE COMPENSATOR. The temperature compensator element is temperature sensitive and can be checked with an ohmmeter. Resistance increases with temperature. The 3K element will read 3000 ohms ± 1% at 25°C (77°F) and a Pt100 will read 110 ohms. Resistance varies with temperature for a 3K and Pt100 element and can be determined according to Table 6-2 or the following formula: RT=Ro [l+R1 (T-20)] Where RT = Resistance T = Temperature in °C Refer to Table 6-1 for Ro and R1 values 6.2 MODEL 396P & 396PVP pH SENSORS 4.2.1 ELECTRODE CLEANING. If the electrode is coated or dirty, clean as follows: 1. Remove the sensor from process. 2. Wipe the glass bulb with a soft, clean, lint free cloth or tissue. If this does not remove the dirt or coating, go to Step 3. (Detergents clean oil and grease; acids remove scale.) 3. Wash the glass bulb in a mild detergent solution and rinse it in clean water. If this does not clean the glass bulb, go to Step 4. CAUTION The solution used during the following check is an acid and should be handled with care. Follow the directions of the acid manufacturer. Wear the proper protective equipment. Do not let the solution come in contact with skin or clothing. If contact with skin is made, immediately rinse with clean water. 4. Wash the glass bulb in a dilute 5% hydrochloric acid solution and rinse with clean water. Soaking the sensor overnight in the acid solution can improve cleaning action. NOTE Erroneous pH results may result immediately after acid soak, due to reference junction potential build-up. Replace the sensor if cleaning does not restore sensor operation. TABLE 6-1 Ro and R1 VALUES FOR TEMPERATURE COMPENSATION ELEMENTS Temperature Compensation Element 3K Pt100 Ro R1 2934 107.7 .0045 .00385 TABLE 6-2 TEMPERATURE vs RESISTANCE OF AUTO T.C. ELEMENTS Temperature °C 0 10 20 25 30 40 50 60 70 80 90 100 Resistance (Ohms) ±1% 3K Pt100 2670 100.0 2802 103.8 2934 107.7 3000 109.6 3066 111.5 3198 115.4 3330 119.2 3462 123.1 3594 126.9 3726 130.8 3858 134.6 3990 138.5 25 MODEL 396P and 396PVP 6.3 MODEL 396P and 396PVP ORP 4.3.1 Platinum Electrode Check. The platinum electrode may be checked as follows: There are two types of standard solutions which may be used to check the ORP electrode/transmitter system. Type 1: One type of commonly used ORP standard solution is the saturated quinhydrone solution. Refer to Section 5.2. CAUTION The solution used during the following check is an acid and should be handled with care. Follow the directions of the acid manufacturer. Wear the proper protective equipment. If contact with skin of clothing is made, immediately rinse with plenty of clean water. Type 2: A second ORP standard solution is the FerricFerrous Ammonium Sulfate Solution (PN R508-16OZ), and it can be ordered as a spare part; otherwise, it can be prepared from the following recipe: Dissolve 39.2 grams of reagent grade ferrous ammonium sulfate, Fe(NH4)2 (SO4)2 • 6H2O and 48.2 grams of reagent grade ferric ammonium sulfate, FeNH4(SO4)2 • 12H2O, in approximately 700 milliliters of water (distilled water is preferred, but tap water is acceptable). Slowly and carefully add 56.2 milliliters of concentrated sulfuric acid. Add sufficient water to bring the total solution volume up to 1000 ml. This standard ORP solution, although not as simple to prepare as the quinhydrone recipe, is much more stable, and will maintain its millivolt value for approximately one year when stored in glass containers. This solution (ferric/ferrous ammonium sulfate) will produce a nominal ORP of 476 +20 mV at 25°C when used with a saturated KCl/AgCl reference electrode and platinum measuring electrode. Some tolerance in mV values is to be expected due to the rather large liquid reference junction potentials which can arise when measuring this strongly acidic and concentrated solution. However, if the measuring electrodes are kept clean and in good operating condition, consistently repeatable calibrations can be carried out using this standard solution. 26 SECTION 6.0 MAINTENANCE 6.3.2 Cleaning Platinum Electrode. The electrode can be restored to normal operation by simply cleaning the platinum electrode with baking soda. Polish it by rubbing it with a damp paper towel and baking soda until a bright, shiny appearance is attained. MODEL 396P and 396PVP SECTION 7.0 DIAGNOSTICS AND TROUBLESHOOTING SECTION 7.0 DIAGNOSTICS AND TROUBLESHOOTING 7.1 MODEL 54e/81/3081/4081/5081/Xmt DIAGNOSTICS AND TROUBLESHOOTING The Model 54 Analyzer and Models 81 and 3081 Transmitters automatically search for fault conditions that would cause an error in the measured pH value, as does the Model 1054B pH/ORP Analyzer to a lesser degree. Refer to the applicable Instruction Manual for a complete description of the analyzer’s fault conditions. Table 7-1, below, lists the Model 54’s, 4081’s, 3081’s, and 81’s diagnostic messages that indicate a possible sensor problem. A more complete description of the problem and a suggested remedy corresponding to each message is also listed. TABLE 7-1. Troubleshooting with Advanced Diagnostics DIAGNOSTIC MESSAGE 54 3081/81/4081 “Calibration Warning” /-[5ES-U1 “Cracked glass failure” ([-<
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