Toshiba 62372311 Density Meter User Manual LQ300A00
Toshiba Corporation Density Meter LQ300A00
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User Manual
6 F 8 A 0 7 8 7 Operation Manual For The Insertion Type Density Meter Type LQ300A00****** © TOSHIBA Corporation 2002 All Rights Reserved. 6 F 8 A 0 7 8 7 ■ Notice 1. Do not copy or transcribe this manual in part or entirety without written permission from Toshiba. 2. The manual is subject to change without notice. 3. Although we tried hard to make this manual error free, if you find any errors or unclear passages, kindly let us know. 1 6 F 8 A 0 7 8 7 INTRODUCTION Thank you very much for your purchase of the LQ300A00****** Density Meter. This manual is prepared for people in charge of installation, operation or maintenance. The manual describes the precautions in using the meter, and explains about installing, adjusting, calibrating and maintaining the LQ300A00****** meter. Carefully read this manual before using the meter for efficient and safe operation. Always keep the manual in a place where you can easily access. ◆ About Safety Precautions Carefully read the Safety Precautions that appear in the following pages before using the Meter. The safety signs used in the Safety Precautions will appear again in the following sections for your safety. 2 6 F 8 A 0 7 8 7 Safety Precautions Important information is shown on the product itself and in the operation manual to protect users from bodily injuries and property damages, and to enable them to use the product safely and correctly. Please be sure to thoroughly understand the meanings of the following signs and symbols before reading the sections that follow, and observe the instructions given herein. Keep the manual in a place you can easily access to whenever you need it. [ Explanation of Signs] Sign Description Red WARNING Indicates a potentially hazardous situation which could result in death or serious injury, if you do not follow the instructions in this manual. Indicates a potentially hazardous situation which may result in minor or moderate injury, and/or equipment-only-damage, if you do not follow the instruction in this manual. Note 1: Serious injury refers to cases of loss of eyesight, wounds, burns (high or low temperature), electric shock, broken bones, poisoning, etc., which leave after-effects or which require hospitalization or a long period of outpatient treatment of cure. Yellow CAUTION Note 2: Minor or moderate injury refers to cases of burns, electric shock, etc., which do not require hospitalization or a long period of outpatient treatment for cure; equipment damage refers to cases of extensive damage involving damage to property or equipment. [ Explanation of the Symbols] Symbol Description This sign indicates PROHIBITION (Do not). The content of prohibition is shown by a picture or words beside the symbol. This sign indicates MANDATORY ACTION (You are required to do). The content of action is shown by a picture or words beside the symbol. Red Yellow This shape or symbol indicates WARNING. The content of WARNING is shown by a picture or words beside the symbol. ◆Color back : red, flame, picture and words : black This shape or symbol indicates CAUTION. The content of CAUTION is shown by a picture or words beside the symbol. ◆Color back : yellow, flame, picture and words : black 3 6 F 8 A 0 7 8 7 Safety Precautions (Continued) For a safe use of the LQ300A00****** Density Meter, take precautions described in this manual and observe ordinances in making the installation and operation. Toshiba is not responsible for any accident arising from the use that does not conform to above. INSTALLATION PRECAUTIONS Red DO WARNING ■ Electrical and mechanical constructions are necessary for the meter. Please consult your vender or Toshiba sales representative. ■ The meter is heavy. To move them or relocate them may need a qualified operator for handling a crane, a hoist or a truck for safe operation. DO ■ When hoisting this unit, use the hoisting bands. In addition, when hoisting the unit with hoisting bands, tighten the bands so that the bands will not be loosened or slipped off. DO ■ Do not operate where there is a possibility of leakage of flammable or explosive gas. Overturning or dropping can cause injuries or equipment failure. DON’T Yellow A fire or explosion can occur. CAUTION ■ Avoid installing the meter in any of the following places: DO Inadequate construction can cause electric shock and fire. l Dusty place l Place where corrosive gases (SO2, H2S) or flammable gases may be generated. l Place exposed to vibration or shock that exceeds permissible level. l Place exposed to condensation due to abrupt change in temperature. l Place too cold or hot for installation l Place too humid for installation l Near an apparatus that generates strong radio waves or strong magnetic field. Otherwise, a fire or equipment breakdown or failure can occur. 4 ■ Install the meter in a place that is good for operation, maintenance and inspection. DO A stumble or an overturn can cause injuries. 6 F 8 A 0 7 8 7 Safety Precautions (Continued) WIRING PRECAUTIONS Yellow WARNING ■Be sure to install a fuse and a switch to disconnect the equipment from the power source. DO DO Failure to observe this can cause electric shock or equipment failure. Without grounding, electric shock, malfunction, or equipment failure can be caused by electric leakage. ■Make sure that the main power line is off before wiring or cabling. DO Wiring or cabling without switching off the main power line can cause electric shock. ■Use crimp terminals with insulation sleeves for power line and grounding wire terminals. DO Wrong wiring or cabling can cause malfunctions, overheating, sparking, or electric shock. A disconnected cable or wire from the terminal or a loose terminal can cause electric shock or generate heat and cause a fire or equipment failure. Do not wire or cable with wet hands. ■Wiring and cabling should be done as shown in the wiring and connection diagrams. DO ■Be sure to ground the equipment using a grounding wire separate from those used for power tools. (With 100 Ohms or less ground resistance) A wet hand can cause electric shock. DON’T Yellow The label shown left appears near a terminal block on the equipment to which power is supplied. Take precautions to avoid electric shock. Yellow 5 6 F 8 A 0 7 8 7 Safety Precautions (Continued) PRECAUTIONS REGARDING MAINTENANCE, INSPECTION, AND PARTS REPLACEMENT Yellow DO WARNING ■ Be sure to set the power switch on the equipment to the OFF position before doing maintenance or inspection inside the equipment or replacing its parts. ■ Be sure to set the power switch on the equipment to the OFF position before replacing the fuse. DO Failure to observe this can cause electric shock. Failure to observe this can cause electric shock or equipment failure. DON’T ■ Do not touch the terminal block during maintenance or inspection. If it is necessary to touch the terminal block, set the power switch on the equipment to the OFF position in advance. ■ Do not attempt disassemble or modify the equipment. DON’T Failure to observe this can cause electric shock or equipment failure. Failure to observe this can cause electric shock. ■ Do not touch the detector main body during measuring fluid density. DON’T The label shown at left is placed near each terminal block on the equipment to which power is supplied. Be careful of electric shock. The temperature of the detector main body rises with fluid temperature. Touching the detector main body causes burns. 6 6 F 8 A 0 7 8 7 Safety Precautions (Continued) Limited Applications of the product This product is not designed or manufactured for the purpose of applying to the systems, such as shown below, which require the level of safety that directly concerns with human life. When your use includes potential applications in those systems, contact Toshiba for consultation. • Main control system for atomic power generating plant/Safety protection system for nuclear facilities/Other critical safety systems/medical control system for sustaining life • This product is manufactured under strict quality control but components might fail and if this product is likely to be applied to a system that concerns with human life or it is likely to be applied to a facility that may have serious effects, please consider special efforts to make the system safe regarding the operation, maintenance and management of the system. Liability Exemptions Toshiba assumes liability exemptions from the following examples. • • Damages caused by fire, earthquake, actions by third party, other accidents, abuse or faulty use whether accidental or intentional by the user, or by other uses of abnormal conditions. Damages or losses that are incidental to the use of or disuse of the product (loss of business profit, interruption of business operation, etc.) 7 6 F 8 A 0 7 8 7 [NOTE] Sign In addition to the signs and symbols for safety precautions shown in the first several pages of the manual, the following sign is also used. ♦ [NOTE] Sign When an explanation is made in the text regarding the Safety Precautions, the [NOTE] sign shown below appears in the left margin of a page. The [NOTE] gives you directions to follow in the following instances. • • • • To use product correctly and effectively. To prevent abnormal or degrading performance of the product. To prevent faulty actions. To store the product when you do not use the product for a long time. [Note] 8 6 F 8 A 0 7 8 7 Important Notes on Use of The Insertion Type Density Meter LQ300A00****** Be sure to observe following instructions in order to maintain the original performance of the insertion type density meter LQ300A00****** and safely use it over a long period of time. ♦ Toshiba is not held responsible for any fault or result caused by not observing the precautions described in this manual or by not observing the laws or regulations in installing or using the product. [NOTE] Do not install or store the product in the following places. Otherwise, meter performance can deteriorate and malfunction, fault, or breakage can occur. Place exposed to direct sunlight Hot, humid place Place exposed to severe vibration and shock Place to be submerged under water except the liquid contacting area of the detector Place of corrosive atmosphere [NOTE] Use a separate wire for grounding the meter. Do not share the same grounding wire with other devices. Otherwise, malfunction, fault, or breakage can occur. [NOTE] Lay the output signal cable through their own conduit away from the AC power cable and other sources of noise. Noise can interrupt correct measurement. [NOTE] Perform periodic maintenance and inspection. A long period of reliable measurement requires periodic span calibration. (e.g. once every 3 months) Avoid using the density meter where fluid substances accumulate or entangle in the density meter detector. [NOTE] Be careful not to let water or moisture into the applicator mount of the detector, converter, or cable ends. Water or moisture can adversely affect performance and shorten parts service life. Close the covers and doors securely, and make the cable outlets airtight. [NOTE] Turn on the density meter only when the density meter is installed in a metal piping system. Make sure to turn off the power when installing or removing the density meter. Leakage of radio waves may cause interference to other equipment. [NOTE] Do not step on any part of the density meter (temperature detector mount, applicator (antenna) mount, converter for example) when you do piping work. Do not place any heavy object on it. Otherwise, deformation or fault can occur. 9 6 F 8 A 0 7 8 7 Important Notes on Use of The Insertion Type Density Meter LQ300A00****** [NOTE] Do not use a transceiver, handy telephone, or other wireless device nearby. Such a device can adversely affect correct measurement. In the event one must be used, observe the following precautions. (1) When using a transceiver, make sure that its output power is 5W or less. (2) When using a transceiver or a handy telephone, keep the converter and signal cable at least 50cm away from the antenna. (3) Do not use a transceiver or a portable telephone nearby while the density meter is in online operation. This is important to protect if from being affected by a sudden output power change. (4) Do not install the fixed antenna of a wireless device in the area around the converter and signal cable. [NOTE] Use a fuse of the specified rating. A fuse other than that specified can cause density meter malfunction or breakage. [NOTE] Do not modify or disassemble the density meter unnecessarily. Do not use parts other than specified. Failure can cause malfunction and density meter fault. [NOTE] When moving the meter elsewhere for installation, be careful not to drop, hit, or subject to strong shock. Otherwise, the density meter may be broken, resulting in malfunction or fault. [NOTE] Before returning your density meter to Toshiba for repair, etc., make sure to inform us about the measured matter remaining in the density meter pipe, including whether it is dangerous or not to touch the material and then clean the meter so that no measured matter remains in its pipe. Disposal [NOTE] When disposing of this density meter, obey the rules and regulations of the local government. [FCC notice] This equipment has been tested and found to comply with the limits for a field disturbance sensor, pursuant to Part 15 of the FCC rules. These limits are designed to provide reasonable protection against harmful interference in a residential installation. This equipment generates, uses and can radiate radio frequency energy and, if not installed and used in accordance with the instructions, it may cause harmful interference to radio communications. However, there is no guarantee that interference will not occur in a particular installation. If this equipment does cause harmful interference to radio or television reception, which can be determined by turning the equipment off and on, the user is encouraged to try to correct the interference by one or more of the following measures. • Reorient the receiving antenna. • Increase the separation between the equipment and receiver. • Connect the equipment into an outlet on a circuit different fr6m' that to which the receiver is connected. • Consult the dealer or an experienced radio,'1'V technician for help. WARNING: This equipment has been certified to comply with the limits for a field disturbance sensor, pursuant to Subpart C of part 15 FCC rules. Except AC power cable, shielded cables must be used between the external devices and the terminals of the converter of the equipment. Changes or modifications made to this equipment, not expressly approved by Toshiba or parties authorized by Toshiba could void the user's authority to operate the equipment. 10 6 F 8 A 0 7 8 7 Contents Safety Precautions ................................................................................................................................................................................3 [NOTE] Sign ...........................................................................................................................................................................................8 Important Notes on Use of The Insertion Type Density Meter LQ300A00****** ..............................................................................9 1 OVERVIEW .....................................................................................................................................................................................14 1.1 Principle of Measurement ....................................................................................................................................................14 1.2 Features...............................................................................................................................................................................15 2 UNPACKING...................................................................................................................................................................................16 2.1 Standard Components .........................................................................................................................................................16 2.2 Standard Accessories ..........................................................................................................................................................16 3 INSTALLATION ..............................................................................................................................................................................17 3.1 Precautions for Installation...................................................................................................................................................17 3.2 Installation Location .............................................................................................................................................................19 3.3 Installation and Piping ..........................................................................................................................................................21 3.4 Precautions for Wiring..........................................................................................................................................................25 3.5 Wiring...................................................................................................................................................................................26 4. Part Names and Functions ...........................................................................................................................................................28 4.1 Detector................................................................................................................................................................................28 4.2 Conveter...............................................................................................................................................................................29 5. Operation Procedure.....................................................................................................................................................................31 5.1 Parameters and Set Values .................................................................................................................................................31 5.2 Menus and operations..........................................................................................................................................................33 5.2.1 main menu...................................................................................................................................................................33 5.2.2 Setting keys.................................................................................................................................................................34 5.2.3 Menu display ...............................................................................................................................................................35 5.2.4 Monitoring menu display and operating procedures ...................................................................................................38 5.2.5 Setting menu display and operating procedures ....................................................................................................39 5.2.6 Measuring mode display and operating procedures ...................................................................................................40 5.2.7 Reading of parameters display and operating procedures..........................................................................................40 5.2.8 Measured values display and operating procedures...................................................................................................44 5.2.9 Self-diagnosis data display operating procedures.......................................................................................................44 5.2.10 Parameter setting display and operating procedures..................................................................................................46 5.2.11 Zero calibration display and operating procedures .....................................................................................................49 5.2.12 Span calibration display and operating procedures ....................................................................................................49 5.2.13 Phase angle rotation correction display and operating procedures ............................................................................50 5.2.14 Linearize/conductity correction display and operating procedures..............................................................................51 5.2.15 Additives correction display and operating procedures...............................................................................................53 5.2.16 Other menus display and operating procedures .........................................................................................................56 6. Operations .....................................................................................................................................................................................57 6.1 Procedures for Preparing and Running................................................................................................................................57 6.2 Preparations before Turning on Power ................................................................................................................................58 6.3 Power on and Preparations for Measuring...........................................................................................................................58 6.3.1 Turning power on ........................................................................................................................................................58 11 6 F 8 A 0 7 8 7 6.3.2 Verifying and setting measurement conditions............................................................................................................59 6.4 Zero Calibration....................................................................................................................................................................60 6.5 Span Calibration...................................................................................................................................................................62 6.6 Operation .............................................................................................................................................................................64 6.7 External Synchronized Operation ........................................................................................................................................65 6.7.1 Movement of the external synchronized operation......................................................................................................65 6.7.2 Setting the external synchronized operation ...............................................................................................................66 6.8 Functions Related to Operation ...........................................................................................................................................67 7 MAINTENANCE ..............................................................................................................................................................................68 7.1 Precautions for Maintenance, Inspection, and Parts Replacement .....................................................................................68 7.2 Maintenance and Inspection Items ......................................................................................................................................69 8 TROUBLESHOOTING ....................................................................................................................................................................70 8.1 Troubleshooting ...................................................................................................................................................................70 8.2 Error Indications and Recovery Operations .........................................................................................................................72 9 CORRECTIONS IN DENSITY CALCULATION ..............................................................................................................................74 9.1 Density Calculation ..............................................................................................................................................................74 9.2 Various Kinds of Corrections................................................................................................................................................75 9.2.1 Phase angle rotation correction...................................................................................................................................75 9.2.2 Liquid temperature correction......................................................................................................................................75 9.2.3 RF correction...............................................................................................................................................................76 9.2.4 Atmospheric temperature correction ...........................................................................................................................76 9.3 Phase Angle Rotation Correction (Details) ..........................................................................................................................77 9.3.1 Care point concerning phase angle rotation................................................................................................................77 9.3.2 Phase angle rotation in external synchronized operation............................................................................................77 9.3.3 Outline of automatic adjustment function of phase angle rotations.............................................................................77 9.3.4 Judgement conditions and adjustments for automatic adjustment of phase angle rotations ......................................77 9.3.5 Restrictions and invalidation in applying the automatic adjustment of phase angle rotations.....................................78 9.3.6 Invalidation by setting the automatic adjustment of phase angle rotations .................................................................78 9.3.7 Actions after invalidating the automatic adjustment of phase angle rotations.............................................................79 9.3.8 Return to the normal through manual input of the phase angle rotations ...................................................................80 10 VARIOUS FUNCTIONS ..................................................................................................................................................................81 10.1 Various Functions and their Outlines ...................................................................................................................................81 10.2 Moving Average ...................................................................................................................................................................82 10.2.1 Function of moving average........................................................................................................................................82 10.2.2 Setting of the moving average times ...........................................................................................................................82 10.2.3 Cautions in using the moving average function...........................................................................................................82 10.3 Change-rata limit..................................................................................................................................................................83 10.3.1 Outline of change-rate limit function............................................................................................................................83 10.3.2 Examples of operating the change-rate limit function .................................................................................................83 10.3.3 Cautions in using the change-rate limit factor .............................................................................................................84 10.3.4 Setting the change-rate limit........................................................................................................................................85 10.4 Electric Conductivity Correction ...........................................................................................................................................86 10.4.1 Standard conductivity correction factor .......................................................................................................................86 10.4.2 How to obtain and set a correction factor....................................................................................................................87 10.5 Additives Correction Factor..................................................................................................................................................90 10.5.1 Additive Correction Function .......................................................................................................................................90 10.5.2 Density calculation ......................................................................................................................................................91 10.5.3 Procedures for using the additives correction function................................................................................................92 10.5.4 How to set the additives correction function................................................................................................................93 10.5.5 Simplified Correction on Additives...............................................................................................................................94 12 6 F 8 A 0 7 8 7 10.6 LINEARIZER SETTING........................................................................................................................................................95 10.6.1 Linearizer function.......................................................................................................................................................95 10.6.2 Linearizer setting.........................................................................................................................................................97 10.7 Density Multiplier Switching by External Signals..................................................................................................................98 10.7.1 Density multiplier switching function by external signals.............................................................................................98 10.7.2 Setting the density multiplier switching by external signals.........................................................................................99 11. Specifications ..............................................................................................................................................................................100 11.1 General Specifications .......................................................................................................................................................100 11.2 Detector Specifications ......................................................................................................................................................101 11.3 Converter Specifications ....................................................................................................................................................102 11.4 Model Number Table..........................................................................................................................................................105 Appendix ............................................................................................................................................................................................107 Attached Figure 1............................................................................................................................................................................107 13 6 F 8 A 0 7 8 7 1 OVERVIEW The LQ300A00****** Density Meter measures the density of a substance that flows in a tank and through a pipe by means of a phase difference method using microwaves. This method is little affected by the presence of contamination. It uses no moving mechanical parts or mechanism that is often used in other measuring methods for cleaning, sampling, or defoaming. It permits continuous measurement. The density meter, which outputs measured density in electric current, is suitable for an application in a process for monitoring and controlling. 1.1 Principle of Measurement This insertion type density meter LQ300A00****** has adopted a new measuring method called “Phase difference method by microwaves.” When microwaves go through a substance and comes out of it, by measuring the phase lag of the waves, we get a certain physical property of the substance that is proportional to the density. The theory of density measurement based on the phase difference method is shown in Figure 1.1 The difference between the phase lagθ1 of the microwave received through water (density 0%) and the phase lagθ2 of the microwave received through the object substance, that is, Δθ = θ2 − θ1 is determined, and since the differenceΔθis in direct proportion to the density, the density of the object substance is measured. Water Received microwaves Transmitted microwaves with phase lag θ1 Substance measured Phase lag θ2 Phase difference △θ=θ2−θ1 Fig. 1.1 Principle of phase angle difference 14 6 F 8 A 0 7 8 7 1.2 Features The Insertion Type Density Meter has the following features compared to the flow-through type density meter: (1) Applicable to the larger size piping or tank of more than 300 mm in meter size In this system the transmission and reception applicators (antenna) are installed at a fixed distance in a pipe and then the pipe itself is inserted into a larger pipe or a tank thus the installation of this density meter is not dependent on pipe size. The density meter can measure the fluid density in a pipe or tank exceeding 300 mm in diameter. (2) Fluid materials with its conductivity up to 15mS/cm can be measured New applicators are developed so that the radiation power of microwaves are concentrated on the area between the transmission and reception applicators (antenna) and its reception applicator can prevent unwanted electromagnetic waves from outside and this made the density meter applicable to higher conductivity fluid materials of up to 15 mS/cm. In the case of 250 mm or 300 mm pipe size, the flow-through type density meter may be difficult to measure fluid materials due to conductivity problems but with this insertion type density meter the measurement may be possible. (3) Fluid materials with its density up to 50% TS can be measured (4) Conformed to low-level radio-wave equipment The output of microwaves is as low as 1 mW that this density meter is categorized as low-level radio-wave equipment. Therefore the user is free to use this density meter without applying for permission, registration, and licenses and so on to use this density meter. Compared with the conventional method, this phase difference measurement method using microwaves, in principle, has the following features. (1) Not easily affected by contamination and bubbles. This method is measuring the variation of the transmission time but not for measuring the attenuation of the wave motion strength that has been transmitted into the measured matter. Therefore, it is unnecessary for the window part for sending/receiving microwaves to be transparent as the optical type. (2) High liability and simple maintenance. This reliability of this density meter is high because it has no moving parts like the rotary pulp density meter does. In addition, it has no consumable parts such as bearings or pulleys and thus its maintenance is easy. (3) Not easily affected by the pulp material type or freeness. Taking density measurements captivating the dielectric change following the density change in the measured matter, the new method has the feature of not easily affected by the pulp material type or freeness, etc. (4) Capable of continuous measurement. (5) Can easily change the measurement range. (6) The operation is simple because complex processings such as density calculation and correction, etc. are performed automatically by micro computers. (7) Remote control is made possible by using the hand-held terminal AF100LQ3 type (optional), which is a specialized terminal for communication.Density meter LQ300A00****** is equipped with the display/operation consoles as standard. Therefore, if the meter is installed on a location easy for maintenance, the hand-held terminal is not always needed. 15 6 F 8 A 0 7 8 7 2 UNPACKING Check items by the following list and table at unpacking. 2.1 Standard Components (1) Density Meter (2) Standard accessories : 1 unit : 1 unit In the event of performing remote control through communications, you are required to have the handheld terminal AF100 type (type code: AF100LQ3AAA3), which is a specialized terminal for communications. Therefore, please purchase one separately. 2.2 Standard Accessories Table.2.1 Standard accessories Accessory Fuse Operation manual Specifications 1A(M),250V cartridge, glass tubular fuse, 5.2mm outer dia. x 20mm long (The document you are reading.) 16 Qty 6 F 8 A 0 7 8 7 3 INSTALLATION 3.1 Precautions for Installation Red DO WARNING ■ Do not operate where there is a possibility of leakage of flammable or explosive gas. ■ The meter is heavy. To move it for relocation or installation, an qualified operator qualified for safety should handle it by using equipment such as a crane or a sling. DON’T A fire or explosion can occur. Overturning or dropping can cause human injuries or equipment failure. Yellow CAUTION ■ Avoid installing the meter in any of the following places. A fire or explosion can occur. DO • • • • • • • • ■ Install the meter in a place where it is easy to operate, maintain, and inspect. Dusty place Place where corrosive gases (SO2, H2S, etc.) or flammable gases may be generated. Place exposed to vibration or shock above permissible levels Place exposed to condensation due to abrupt change in temperature. Place too cold or hot for installation Place too humid for installation Near an apparatus that generates strong radio waves or a strong magnetic field. Otherwise, a fire, equipment breakdown or failure can occur. DO 17 A stumble or a fall when working can cause human injuries. 6 F 8 A 0 7 8 7 Hoisting the Density Meter Before Installation Make sure to hoist the density meter using the hoisting bands. Hoisting it with incomplete position or condition can cause a fall or damage to the density meter. [NOTE] When you move or install the Insertion Type Density Meter, make sure to hoist the density meter using the hoisting bands. In addition, care should be taken to put the cushioning material between the hoisting band and the converter case. If the hoisting band touches the converter case directly it may cause a scratch on the converter front panel. Main unit mass: approx. 20 kg Recommended hoisting bands: made of cloth, applicable band size 25 mm Note: This unit is heavy. To move the unit or relocate it needs a qualified operator for handling a hand truck, crane, hoist or other. In addition, when hoisting the unit with hoisting bands, tighten the bands so that the bands will not be loosened or slipped off. 重心位置 Center of gravity position 吊りposition ベルト装着位置 Hoisting with band Hoisting 吊り direction 上げ方向 Hoisting direction 吊り上げ方向 吊りベルト装着位置 Hoisting position with band Center of gravity position 重心位置 Fig. 3.1.1 Hoisting with Hoisting Bands (1) Fig. 3.1.1 Hoisting with Hoisting Bands (2) 18 6 F 8 A 0 7 8 7 3.2 Installation Location [NOTE] ◆ Determine an indoor installation place in accordance with the following instructions. (1) Choose a place that is free of vibrations and corrosive gasses, and has ample space for maintenance. (2) Secure maintenance space in front, rear and above the density meter. (Refer to fig. 3.2.1) (3) In the case of outdoor installation, provide covering against sun. (4) Do not install the meter in a place where there is a possibility of leakage of flammable or explosive gas. (5) Use a strength pipe, connected at both upstream and downstream sides, to securely install the detector main body, or provide a supporting structure for the detector main body. (Weight of this unit is shown in the external dimension list as attached.) (6) When the density meter is used in an application where the process fluid contains plenty of fur or fiber, these substances may accumulate or entangle in the density meter and thus perform the maintenance operation periodically (clean the insertion probe area). (7) The tank or pipe where this density meter is installed should be metal. (8) Install the density meter in a place where the density distribution is even. If the density distribution is not even, manual analysis data and the indication value of the density meter may not be the same. (9) Install this density meter in a piping system where bubbles are not found, and fluid does not empty itself, and also sedimentation and accumulation of materials does not occur. 19 M8M8ネジ締め付けト screw tightening torque: ルク: 10.0 1 to0 13.5 N•m .0∼1 3.5N・m (Tighten the screws evenly.) ( 片締めと ならないこ と) 231(*1) 600 6 F 8 A 0 7 8 7 L(*2) 600 Flow direction 変換器 Converter shows flow direction 流れ方向を表示 流 れ 600 方 向 Metal pipe or metal tank 金属製配管 Fluid to be measured 測定対象流体 Length (mm) 347 346 345 金属製配管 Metal pipe or metal tank 測定対象流体 Fluid to be measured 600 Mounting flange surface Internal wall of tank or pipe 600 Diameter (mm) 300 350 400 600 Notes *1 The length when Toshiba recommendation flange is used. (Refer to 3H8A6579 and 3H8A6580 for details.) *2 The length when *1 above and Sch40 standard stainless steel pipe is used. 120mm or less Figure 3.2.1 Maintenance Space 20 6 F 8 A 0 7 8 7 3.3 Installation and Piping Installing the density meter is illustrated in Fig. 3.3.1 and Fig. 3.3.2, Fig.3.3.3, Fig.3.3.4. [NOTE] (1) Install the density meter in a place where the distribution of density is even. (2) Install the density meter in a location where the measured fluid flows in a tank or pipe in full and bubbles do not stay. Insufficient fluid flowing or bubbles staying in the tube will cause measuring errors or indicated-value fluctuations. (3) Avoid installing the density meter where the material to be measured precipitates and accumulates at the bottom of the tank or pipe. (4) Avoid installing the density meter in a tank or pipe where bubbles are mixed in the fluid to be measured. (5) The front side of the density meter's converter section is equipped with an LED density display section. When installing the meter, choose a location and direction in which this density display section will be easily visible. However, if it is difficult to look straight at the density value display area as a result of installation layout, we recommend you order an optional external display unit. (6) In the event that the tank or piping system (where the density meter is installed) may no longer be full of the fluid while the pump is shut down or the density distribution in the density meter may become uneven, make sure to take measurements only while the pump is operating by using the external interlock function. (7) Take necessary measures to prevent vibrations of the pump, etc. from travelling through the density meter. (8) Select the type and material of the gasket to use in the tank or pipe in accordance with the connection method and the fluid material to measure. (9) Make sure that the surface for the O-ring face and O-ring itself are clean without dirt or dust before starting the installation work. (10) We recommend the following tightening torque for bolts and nuts when mounting the flange for the density meter. Tightening torque: 10.0 to 13.5 N•m for M8 bolts and nuts (11) Perform the periodical inspection to make sure that the thin and long materials such as fur, fiber or strings are not entangled in the applicators (antenna), or there are no scratches or cracks. (12) Make sure that the applicator (antenna) is positioned more inside than the internal wall of the tank or pipe. The distance from the mounting flange face of the insertion probe area to the internal wall should be 120 mm or less. (13) We recommend the installation should be made to a vertical piping system. The density meter can operate the same performance even in a horizontal installation but only a vertical installation is allowed for item (14). (14) The installation should be made to a vertical piping system in the following cases: a) Bubbles may remain in the piping. b) The distribution of density in the piping may become uneven because the material to be measured precipitates or floats unusually due to slow flow rate etc. c) When main piping is enlarged and the density meter is installed to a larger piping system than the main piping. (15) We recommend that the converter section stay at the top when the density meter is installed to a horizontal piping system because the maintenance is easy and its performance is assured. (16) We recommend that the density meter should be installed at a point as far away as possible from a port open to atmosphere and the water pressure is required a little to prevent bubbles from entering in the fluid to be measured. 21 6 F 8 A 0 7 8 7 (17) On both the upstream and downstream sides of the density meter, install shutoff valves. Furthermore, between these valves and the density meter, install the sampling port, the zero water supply port, the air release port, the drain port with a shutoff valve attached respectively. In the event that the flow of the pipe line cannot be stopped, provide a bypass pipe halfway with a shutoff valve attached. When performing zero point calibration, these are needed to discharge the measured matter out of the density meter through its drain port and fill up the meter with fresh water of zero density. (See Figures 3.3.2 and 3.3.3.) (18) As to insertion orientation, install the density meter so that a pair of antennas face toward upstream. (19) In a tank, install the density meter so that the applicators (antenna) are submerged 150 mm or more under water from the surface. If the depth of water is less than 150 mm or the applicators surface stays above the water level in cases like a pump operation, use the external synch signal and measure the density only when the applicators surface remains more than 150 mm under water (see Figure 3.3.1.) (20) Install the density meter far from such places as near the agitator in a tank where bubble are generated and density disturbances occur and this affects the density measurement. [NOTE] ♦ Sampling valve: Used to extract fluids for manual analysis. Install this valve to the side of the pipe in the case of horizontal installation. It is recommended that a 1-inch ball valve be installed to the side of the pipe. ♦ Zero point water valve: Used to supply drinking water (density or consistency 0%) to the detector pipe for zero point adjustment. Install this valve at the top of the pipe in the case of horizontal installation. It is recommended that a 1-inch ball valve be installed in the top of the pipe and zero point water is supplied through this inlet using a vinyl hose etc. If valve water pipe is connected to this valve, air cannot be extracted. Therefore, another valve (vent valve) is needed to extract air. ♦ Vent valve: Used to vent process fluids to open air when performing zero adjustment. This helps the drinking water (density or consistency 0%) enter the detector pipe easily. Install this valve in the top of the pipe in the case of horizontal installation. ♦ Drain valve: Used to drain the fluids before supplying drinking water (density or consistency 0%) to the detector pipe for zero adjustment. Install this valve at the lowest point of the pipe. It is recommended that a 1-inch ball valve be installed at the lowest point of the pipe. Water surface Metal tank 1500mm or more Fluid to be measured 120mm or less Figure 3.3.1 Precautions when installing the density meter in a tank 22 6 F 8 A 0 7 8 7 Shutoff valve Shutoff valve Vent valve Zero point water valve Zero point water piping Density meter Bypass piping Drain valve Drain piping Shutoff valve Direction of flow upward Fig. 3.3.2 Meter mounted vertically Vent valve Shutoff valve Sampling valve Shutoff valve Zero point water valve Density meter Shutoff valve Drain valve Bypass piping Fig. 3.3.3 Meter mounted Horizontally (looking from above) [NOTE] (1) Make sure that the surface for the O-ring face and O-ring itself are clean without dirt or dust before starting the installation work. (2) We recommend the following tightening torque for bolts and nuts when mounting the flange for the density meter. Tightening torque: 10.0 to 13.5 N•m for M8 bolts and nuts 23 6 F 8 A 0 7 8 7 [NOTE] (1) When you install the density meter, see 3.3.4 Precautions When Installing the Density Meter. (2) Install the density meter in a metal piping system. M8 screw tightening torque: 10.0 to 13.5N•m (Tighten the screws evenly.) When installing or removing the density meter, insert or remove the applicator mount section with its backside along the mounting flange. Extra care should be taken not to let the applicators (antenna) hit against the flange or the internal wall. shows flow direction 231 589 Flow direction Make sure to mount the density meter so that the applicators (antenna) face upstream and in parallel with the direction of the flow. Section A Converter Make sure that the O-ring groove and Oring itself are clean without dirt, dust or cracks before installing the density meter. Fluid to be measured Metal pipe or metal tank Section A expanded JIS10K 100mm Sch20 Refer to 3H8A6579 and 3H8A6580 for details. Density value display Flange standard: Diameter Deviation of flange hole positions with respect to the piping axial direction: ±2° or less 3.2 Deviation from piping system in perpendicular direction: ±1.5° or less Surface roughness: Ra3.2 minimum (56.6) 1.5 Fig 3.3.4 Installation Precaution 24 6 F 8 A 0 7 8 7 3.4 Precautions for Wiring Yellow WARNING ■Be sure to install a fuse and a switch to disconnect the equipment from the power source. DO DO Failure to observe this can cause electric shock or equipment failure. Without grounding, electric shock, malfunction, or equipment failure can be caused by electric leakage. ■Make sure that the main power line is off before wiring or cabling. DO Wiring or cabling without switching off the main power line can cause electric shock. ■Use crimp terminals with insulation sleeves for power line and grounding wire terminals. DO Wrong wiring or cabling can cause malfunctions, overheating, sparking, or electric shock. Yellow A disconnected cable or wire from the terminal or a loose terminal can cause electric shock or generate heat and cause a fire or equipment failure. Do not wire or cable with wet hands. ■Wiring and cabling should be done as shown in the wiring and connection diagrams. DO ■Be sure to ground the equipment using a grounding wire separate from those used for power tools. (With 100 Ohms or less ground resistance) A wet hand can cause electric shock. DON’T The label shown left appears near a terminal block on the equipment to which power is supplied. Take precautions to avoid electric shock. Yellow 25 6 F 8 A 0 7 8 7 3.5 Wiring Figure 3.5.1 on the next page shows connections to the density meter and the external units. Figure 3.5.2 shows wiring assignment to a converter terminal. Refer to these figures for correct wiring. [IMPORTANT] (1) Provide a switch and a fuse to separate this unit from the mains power for ease of maintenance. Power requirement of this unit is 50VA. (2) Ground the LQ300A00****** with 100 Ohms or less ground resistance. Do not use a common ground shared by other power equipment. The demands of the meter are 50VAs. (3) Use a sheathed cable (CVV) with 2mm2 cross-sectional area for AC power cable and make sure the voltage drop across the cable is less than 2 V. And use a M4 sized solderless contact for connection cable with terminal. (4) The cables should be free from vibration or sway. The cables should be placed in thick-walled steel conduits. (5) Wire the LQ300A00****** output in conduit separated from those of AC power cable, control signals, alarm signal or other cables which could become the source of noise. (6) Use a 2-wire shielded sheathed cable (CVVS) to wire the LQ300A00****** output (4 - 20mAdc). And ground the shielded cable on the receiving instrument side. For performing the conductivity compensation, use a 2-wire shielded sheathed cable (CVVS) to wire the LQ300A00****** conductivity signal input (4-20mA). And ground the shielded cable on the receiving instrument side. (7) As the cable port is made air-tight using a packing, tighten the cable gland securely when all the wiring is completed. If the diameter of the cable is smaller than the inside diameter of the packing, enlarge the cable diameter to the same size as the packing by wrapping valves around the cable. Its suitable diameter is 11mm. (8) Tighten the terminal screws securely. Appropriated torque to tighten the screws is 1.2 N・m . (9) Do not turn on the power of the density meter when the applicators (antenna) are taken out of the piping system. Leakage of radio waves may cause interference to external equipment. 26 6 F 8 A 0 7 8 7 CW L1 AC Power 100 to 240V 50/60Hz (50VA) L2 Ground (R<100 ohms) (PE terminal) CW COM External sync. contact input (24VDC, 1A) DI COM1 Density meter error or “in-maintenance”, contact output (125Vac, 0.1A) DO1 Measured Density Output (420mADC,R<750ohms insulated output) Voltage input for selection of "density multiplier" (H:20 to 30VDC,L:2VDC or less,Input resistance: Approx. 3k ohms) COM2 DI2 DI3 The ground connection of the shielded wire of CVVS should be made on the side of the receiving instrument. CWS A1 + A2 − Conductivity signal input (4-20mA) CVVS Reserved A3 to A8 Ground resistance: 100 ohms or less Ground terminal (M6) Note: Either the FG terminal of the terminal block inside the converter or the ground terminal of the converter case should be grounded. (PE terminal) Converter Terminal block A7 A5 A8 No use (for future) A3 A6 AI (Conductivity signal input A1,A2) Cable inlet (PE terminal) A1 A7 A4 DI A2 DO1 DI2 COM COM1 COM2 DI (Extemal sync.contat input DI, COM) DO + DI3 L1 − DI AO(+,-) (Density meter error or “in- (Factor-select 4 to 20mA DI2, DI3, (HART) maintenance”, contact COM2) output: O1,COM1) Cable inlet 2 27 L2 Cable inlet 3 AC power (L1,L2,PE) Cable inlet 4 6 F 8 A 0 7 8 7 4. Part Names and Functions The detector is integrated with the converter in the Insertion Type Density Meter LQ300A00******. 4.1 Detector (4) Density value display (5) Converter cover Detector (1) Temperature detector (2) Applicators (antenna) (3) Converter Fig. 4.1 Insertion Type Density Meter LQ400A00 (1) Temperature detector This is a temperature detector (RTD) to correct the temperature difference. This detector measures the temperature of the fluid to be measured (fluid temperature) flowing in the pipe where the density meter is installed. (2) Applicators The applicators (antenna) for transmitting and receiving microwaves are built inside. The applicator on the left in Fig.4.1 is for transmitting and the right is for receiving. Always keep the lids closed and the screws of the lids secured. (3) Converter See Section 4.2 28 6 F 8 A 0 7 8 7 4.2 Conveter Figure 4.2 shows the converter cover (5 in Fig. 4.1) with its door open. (10) Density indicator (4 in Fig 4.1) (6) LCD display (7) Setting keys (4) [MEASURE] indicator (3) [POWER] indicator (5) [ALARM] indicator (11) Terminals for communication (2) FUSE 1A(M) 250V (1) [POWER] switch (12) Ground terminal (8) Terminal block (9) Cable glands Fig 4.2 Converter 29 6 F 8 A 0 7 8 7 (1) [POWER] switch The power switch for the density meter. (2) Fuse 1A(M), 250V glass tube fuse is inside. (3) [POWER] Indicator (Green LED) Green LED lights when AC power turns on by the power switch. (4) [MEASURE] Indicator (Green LED) The indicator lights when measuring, and turns off when setting and when measuring stops at externally synchronized operation. (5) [ALARM] Indicator (Red LED) Lights on error signal from the meter. (6) LCD indicator Displays measured values, set values and self-diagnosis data, etc. Being an indicator of 20 characters by 4 lines, it displays numerical values, alphanumeric characters and symbols in accordance with needs. (7) Setting keys These keys are used for switching between display contents of the LCD indicator or setting various set values. They include the [ESC] key, the [→] key, the [UP] key, [DN] key and the [SET] key. (8) Terminal block Refers to the terminal block connecting cables for external connection. (9) Cable glands Four cable glands are available for introducing cables for external connection, such as power supplies and output signals. (10) Density (%TS) indicator (Red LED seven segments) Indicates the density of the measured matter in terms of %TS. (11) Terminals for communication Remote control is made possible by connecting the leads of the hand-held terminal AF100 to these terminals. (12) Ground terminal Make sure to ground this terminal to earth ground. 30 6 F 8 A 0 7 8 7 5. Operation Procedure 5.1 Parameters and Set Values The set values and setting ranges by parameter at the time of factory shipment are listed in Table 5.1.1 below. Table 5.1.1 Parameters and Set Values (No.1) Measurement Condition Parameter Density multiplier (C) Upper density measurement range (UR) Lower density measurement range (LR) Density line slope (a) Density intercept (b) Density test output during setting mode (ot) Unit ― %TS %TS %TS per degree %TS %TS Ex-factory Set Value 1.000 (Standard value) Value specified in your order Value specified in your order 0.084 0.00 (Standard value) 50% density of FS (Provisional value) Setting Range 0.00 to 9.99 1.0 to 99.9 0.0 to 99.5 - 0.2000 to 0.2000 - 99.99 to 99.99 0.0 to 99.9 Delayed time in external synchronized operation (dt) Minute 0.5 (Provisional value) Zero-point phase θ1 (zp) Degree Value at the time of factory adjustment 0.00 to 359.99 °C Value at the time of factory adjustment 0.00 to 100.00 RF correction factor (cG) Zero-point RF data (zG) Moving average times (ma) Permissible width of change-rate limit (dx) Limit times of change-rate limit (HL) Upper angle of angle rotation correction (UH) − − Time %TS − Degree Value at the time of factory adjustment Value at the time of factory adjustment 1 (Without moving averaging) 0.00 (NONE) 0 (Without change-rate limit ) 260 -9.99 to 9.99 0.00 to 100.00 1 to 99 0.00 to 9.99 0 to 99 240 to 360 Upper angle of angle rotation correction (SH) Degree 100 Zero-point liguid temperature T0 (zT) Linearizer density A (LA) Linearizer density B (LB) Linearizer inclination (K1) Linearizer inclination (K2) Linearizer inclination (K3) Electric conductivity correction factor γ (r) Zero-point electric conductivity Eo (zE) Measured object electric conductivity (EC) %TS %TS − − − mS / cm 0.60 (Provisional value) 1.00 (Provisional value) 1.00 (Without linearization) 1.00 (Without linearization) 1.00 (Without linearization) 00 (Without electric conductivity correction) 0.00 mS / cm 0.00 Degree (per mS/cm) 31 0.1 to 99.9 0 to 120 0.00 to 99.99 0.00 to 99.99 0.00 to 9.99 0.00 to 9.99 0.00 to 9.99 0.00 to 99.99 0.00 to 10.00 0.00 to 10.00 6 F 8 A 0 7 8 7 Table 5.1.1 Parameters and Set Values (No.2) Measurement Condition Parameter Availability of additives correction (AF) Display density type of additives correction (Ad) Output density type of additives correction (Ac) Parameter set No. of additives correction (Ap) Main-object sensitivity (sO) Additives sensitivity (s1) Additives sensitivity (s2) Additives sensitivity (s3) Additives sensitivity (s4) Additives sensitivity (s5) Loading additive ratio (R1) Loading additive ratio (R2) Loading additive ratio (R3) Loading additive ratio (R4) Loading additive ratio (R5) Output at contact OFF in external synchronized operation (ho) Availability of density multiplier switching (D1) Density multiplier at DI (C2) Density multiplier at DI (C3) Density multiplier at DI (C4) Availability of automatic adjustment of angle rotation (NA) Switching between continuous operation and external synchronized operation (OP) Note : Unit Ex-factory Set Values No (Without loading material correction) Setting Range − Total TOTAL / MAIN − Total TOTAL / MAIN − 1∼10 − − − − − − − − − − − 1.00 0.00 0.00 0.00 0.00 0.00 0.000 0.000 0.000 0.000 0.000 − 4mA −9.99 to 9.99 −9.99 to 9.99 −9.99 to 9.99 −9.99 to 9.99 −9.99 to 9.99 −9.99 to 9.99 0.000 to 1.999 0.000 to 1.999 0.000 to 1.999 0.000 to 1.999 0.000 to 1.999 Value immediately before 4mA ; simulated output in setting mode − OFF(NONE) ON / OFF − − − 1.000 1.000 1.000 0.000 to 9.999 0.000 to 9.999 0.000 to 9.999 − ON ON / OFF − CONT CONT (Continuous) / EXT(External) − OFF / ON The expression "without ..." has been used in several places in Table 5.1.1 to mean that the respective numeric values in the table above are set to invalidate their functions. 32 6 F 8 A 0 7 8 7 5.2 Menus and operations Operations should be done with five keys for setting, in combination with the LCD display. This section shows menus and operations. 5.2.1 main menu Main menu is composed of three basic menus shown below. Table 5.2.1 shows the functions of each menu and performances when selected. 1 : MONITORING MENU 2 : SETTING MENU 3 : MEASURING MODE Table 5.2.1. Functions and performances of main menu 1 : MONITORING MENU 2 : SETTING MENU 3 : MEASURING MODE Functions Reading of each measuring conditions (parameters), measured values, and selfdiagnosis data Changing of each measuring conditions (parameters), zero calibration and span calibration Mode selection from among two measuring modes (operation modes) of the normal continuous operation and the externally synchronized operation Measured density output(4 to 20mA) Measured density continuous output Density Test output Measured density continuous output Density display Measured density value Density Test output Measured density valve [Measure] indicator On Off On Note: In the Setting menu, when “Zero calibration” or “Span calibration” is executed, LED density display indicates the Measured Density value and not the preset Density Test output because this makes it easy to quickly compare the density measured output before and after the zero or span calibration. On the other hand, the Measured Density Current output continuous to output the Density Test output in every Setting menu including Zero calibration and Span calibration. 33 6 F 8 A 0 7 8 7 5.2.2 Setting keys Five setting keys are available. The basic methods for using them are described in Table 5.2.2. For specification information, please refer to their respective operating procedures. Table 5.2.2 Basic Methods for Using Operation Keys Setting Key Notation in Operation Manual ESC [ESC] Basic Use Returns to the menu screen that is one level higher. [→] On the set value change screen, use this key to clear the setup change before returning to the previous screen. On the menu list screen, use this key to move the cursor under the menu number to the location of the next number. In the state of setting numerical values, press this key each time the cursor has to be shifted rightwards by a digit's worth. If the cursor is located rightmost, the cursor is shifted to the leftmost digit. In the event of entering the setting menu, press the [SET] key to display the message saying that the output will be switched to the simulated value. After making sure that no problem is present, press the [→] key to enter the setting menu. This procedure is taken for the purpose of preventing the output from being switched to the simulated value as a result of mistakenly pressing the [SET] key twice in a row. On the menu screen, use this key to switch to the next menu screen. UP [UP] In the state of setting numerical values, use this key to move up the numeric value of the digit where the cursor is located. Each time the key is pressed, the numeric value changes incrementally, as following; "0", "1", "2", ・・・・, "9", "-"(minus symbol), "."(decimal point), "0", "1", "2", ・・・・. Note: If the numerical value does not belong to the leftmost digit, "-" (minus symbol) will not appear after 9. In the event of selecting an item from multiple items (such as ON/OFF), the cursor (of the selected item) is switched each time this key is pressed. On the menu screen, use this key to switch to the previous menu screen. DN [DN] In the state of setting numerical values, use this key to move down the numerical value of the digit where the cursor is located. Each time the key is pressed, the numerical value changes detrimentally , as following; "0", "."(decimal point), "-"(minus symbol), "9", "8", ・・・・ "1", "0". Note: If the numerical value does not belong to the leftmost digit, "-" (minus symbol) will not appear after "."(decimal point). In the event of selecting an item from multiple items (such as ON/OFF), the cursor (of the selected item) is switched each time this key is pressed. SET [SET] Use this key to select the menu number where the cursor is located or confirm the set value. 34 6 F 8 A 0 7 8 7 5.2.3 Menu display The menu display of the converter LCD display section has a hierarchical structure as shown in Table 5.2.3. Note: Occasionally using some abbreviated terms as well, actual LCD displays differ from Table 5.2.3. For details, refer to Section 5.2.4. The symbols in parentheses in Table 5.2.3 correspond to those displayed on the upper left corner of their respective LCD screens. Table 5.2.3 Menu Display (1) Menu 1 Menu 2 Menu 3 Density multiplier (C) Upper density measurement range (UR) Lower density measurement range (LR) Density line slope (a) Density intercept (b) Density test output (ot) Delayed time in external synchronized Read operation (dt) parameters Zero-point phase θ1 (zp) Zero-point liquid temperature T0 (zT) RF correction factor (cG) Zero-point RF data (zG) Monitoring menu Moving average times (ma) Permissible width of change-rate limit (dx) Limit times of change-rate limit (HL) Measured Phase θ2(p), liquid temperature (T), value atmospheric temperature (A), density (X) Operation status (ST) Microwave signal level (SL) Micro wave factor (F) Self-diagnosis RF data(G) data +5V power supply voltage(J) Reference phase error (pd) Memory check (Mc) 35 Menu 4 6 F 8 A 0 7 8 7 Table 5.2.3 Menu Display (2) Menu 1 Setting menu Menu 2 Menu 3 Upper density measurement range (UR) Lower density measurement range (LR) Density line slope (a) Density intercept (b) Density test output (ot) Delayed time in external synchronized operation (dt) Parameter setting Zero-point phase θ1 (zp) Zero-point liquid temperature T0 (zT) RF correction factor (cG) Zero-point RF data (zG) Moving average times (ma) Permissible width of change-rate limit (dx) Limit times of change-rate limit (HL) Zero calibration Zero calibration Span calibration Density multiplier (C1) Upper angle (UH) Angle rotation Lower angle (SH) correction Angle rotation (N) Linearizer density A (LA) Linearizer density B (LB) Linearizer line slope (K1) Linearizer line slope (K2) Linearizer / electric Linearizer line slope (K3) conductivity Electric conductivity correction factor γ correction (r) Zero-point electric conductivity E0 (zE) Measured object electric conductivity (EC) 36 Menu 4 Setting the upper density measurement range (UR) Setting the lower density measurement range (LR) Setting the density line slope (a) Setting the density intercept (b) Setting the density test output (ot) Setting the delayed time in external synchronized operation (dt) Setting the zero-point phase θ1 (zp) Setting the zero-point liquid temperature T0 (zT) Setting the RF correction factor (cG) Setting the zero-point RF data(zG) Setting the Moving average times (ma) Setting the permissible width of change-rate limit (dx) Setting the permissible times of change-rate limit (HL) Zero calibration implementation verification Setting the density multiplier (C1) Setting the upper angle (UH) Setting the lower angle (SH) Setting the angle rotation (N) Setting the linearizer density A (LA) Setting the linearizer density B (LB) Setting the linearizer line slope (K1) Setting the linearizer line slope (K2) Setting the linearizer line slope (K3) Setting the electric conductivity correction factor γ (r) Setting the zero-point electric conductivity E0 (zE) Setting the measured object electric conductivity (EC) 6 F 8 A 0 7 8 7 Table 5.2.3 Menu Display (3) Menu 1 Menu 2 Additives correction Setting menu Others Measuring mode Continuous operation and external synchronized operation (OP) Menu 3 Availability of additives correction (AF) Display density type (Ad) Output density type (Ac) Parameter set No. (Ap) Main-object sensitivity (sO) Additives sensitivity (s1) Additives sensitivity (s2) Additives sensitivity (s3) Additives sensitivity (s4) Additives sensitivity (s5) Loading additive ratio (R1) Loading additive ratio (R2) Loading additive ratio (R3) Loading additive ratio (R4) Loading additive ratio (R5) Output at contact OFF in external synchronized operation(ho) Availability of density multiplier switching (D1) Density multiplier at DI (C2) Density multiplier at DI (C3) Density multiplier at DI (C4) Availability of automatic adjustment of angle rotation (NA) Switching between continuous operation and external synchronized operation (OP) 37 Menu 4 Selecting the availability of additives correction (AF) Selecting the display density type (Ad) Displaying the output density type (Ac) Setting parameter set No. (Ap) Setting the main-object sensitivity (sO) Setting the additives sensitivity (s1) Setting the additives sensitivity (s2) Setting the additives sensitivity (s3) Setting the additives sensitivity (s4) Setting the additives sensitivity (s5) Setting the loading additive ratio (R1) Setting the loading additive ratio (R2) Setting the loading additive ratio (R3) Setting the loading additive ratio (R4) Setting the loading additive ratio (R5) Selecting the output at contact OFF in external synchronized operation (ho) Selecting the availability of density multiplier switching (D1) Setting the density multiplier at DI (C2) Setting the density multiplier at DI (C3) Setting the density multiplier at DI (C4) Selecting the availability of automatic adjustment of angle rotation (NA) 6 F 8 A 0 7 8 7 5.2.4 Monitoring menu display and operating procedures 1 :MONITORING MENU 2 :SETTING MENU 3 :MEASURING MODE [ESC] (Previous Menu) Move the cursor to "1" with [→] key, and press [SET] key. 1 :READ PARAMETERS 2 :MEASURED VALUES 3 :SELF-DIAGNOSIS Note: In actual display, the cursor is blinking. Move the cursor to the menu number with [→] key, and press [SET] key. Menus of [1 : READ PARAMETERS] [ESC] (Previous Menu) Data display of [2 : MEASURED VALUES] Data display of [3 : SELF-DIAGNOSIS] 38 6 F 8 A 0 7 8 7 Setting menu display and operating procedures 5.2.5 1 :MONITORING MENU 2 : SETTING MENU 3 : MEASURING MODE Move the cursor to "2" with [→] key, and press [SET] key. Test output will be [ESC] (Previous Menu) valid. [→] : CONTINUE [ESC]: CANCEL When [2: SETTING MENU] is selected, the density output signal and the density display are hold in the simulated values that have been set. This warning screen will appear once before getting into [2: SETTING MENU]. After making sure that there is no problem, press the [→] key to get into [2: SETTING MENU]. Press the [→] key to get into [2: SETTING MENU]. Input password [ESC] (Previous Menu) PASSWORD :0000 [SET]SET,[ESC]CANCEL To get into [2: SETTING MENU], it is necessary to further enter the password "8000". In the initial condition, the cursor is on the forth digit. Therefore, press [DN] key 4 times to set to "8" and press the [SET] key to get into [2: SETTING MENU]. An incorrect password will cause the following message to appear. Return to the screen at left by pressing any key and then enter the correct password once again. PASSWORD ERROR PUSH ANY KEY. 5:SET PARAMETERS [ESC] (Previous Menu) 6:ZERO CALIBRATION 7:SPAN CALIBRATION 8:ANGLE ROTATION Move the cursor to the menu number with [→] key, and press [SET] key. [UP] [DN] 9:LINEARIZ/CNDUCTVTY [ESC] (Previous Menu) 10:ADDITIVES CORRECT 11:OTHERS [UP] [DN] 1 :READ PARAMETERS [ESC] (Previous Menu) 2 :MEASURED VALUES 3 :SELF-DIAGNOSIS 39 6 F 8 A 0 7 8 7 5.2.6 Measuring mode display and operating procedures 1 :MONITORING MENU 2 :SETTING MENU 3 :MEASURING MODE [ESC] (Previous Menu) Move the cursor to "3" with [→] key, and press [SET] key. OP:MEASURING MODE DATA:CONT [SET] CHANGE [ESC] RETURN Press the SET key to set. Press the SET key to confirm. Press the ESC key to cancel. OP:MEASURING MODE RANGE :CONT/EXT DATA :CONT [SET] SET,[ESC]CANCEL Each time the [UP] or [DN] key is pressed, CONT/EXT are mutually alternated thus making it possible to select an operation mode. Select "CONT" for normal continuous operations; select "EXT" for external synchronized operations. For details on the external synchronized operation, refer to Section 6.7. 5.2.7 Reading of parameters display and operating procedures 1 :READ PARAMETERS 2 :MEASURED VALUES 3 :SELF-DIAGNOSIS Move the cursor to "1" with [→] key, and press [SET] key, and select [1 : READ PARAMETERS] C:DENSITY MULTIPLIER DATA:1.000(C1) [ESC] [ESC] RETURN (Previous Menu) [UP] [DN] The set value of the density multiplier C, which is used for density calculation, can be verified. If C2, C3 or C4 is displayed in the parentheses, it indicates that the density multiplier switched to by the external voltage signal (DI) is selected. UR:UPPER RANGE DATA:3.0 [ESC] (Previous Menu) The set value of the upper density measurement range (the density whose current output is 20mA) can be verified. [ESC] RETURN [UP] [DN] LR:LOWER RANGE DATA:0.0 [ESC] (Previous Menu) The set value of the lower density measurement range (the density whose current output is 4mA) can be verified. [ESC] RETURN [UP] 40 6 F 8 A 0 7 8 7 [DN] a:DENSITY LINE SLOPE [ESC] (Previous Menu) DATA:0.0840 [ESC] RETURN The set value of "density line slope" of the arithmetic expression for calculating the density from the phase measurement data, etc. can be verified. Normally “0.084” is displayed here. [UP] [DN] b:DENSITY INTERCEPT DATA:0.0 [ESC] (Previous Menu) [ESC] RETURN The set value of "density intercept" of the arithmetic expression for calculating the density from the phase measurement data, etc. can be verified. Normally, this is set to zero. [UP] [DN] ot:DENSTY TEST OUT DATA:1.5 [ESC] (Previous [ESC] RETURN Menu) Upon getting into [2: SETTING MENU], the current output and the LED density display are switched to simulated values. In this screen, the set value of the simulated value (unit: %TS) can be verified. [UP] [DN] dt:DELAYED SYNC.TIME DATA:0.5 [ESC] (Previous [ESC] RETURN Menu) In external synchronized operations, the set value of the delayed time (unit: minute) from when the external contact input is turned ON until the measurement starts can be verified. For details, refer to Section 6.7. [UP] [DN] zp:ZERO POINT PHASE DATA:80.00 [ESC] (Previous Menu) [ESC] RETURN The phase at the time of zero calibration can be verified. [UP] Note : The item which is enclosed dot line is not displayed for Density meters with its ROM version 1.07 or later. 41 6 F 8 A 0 7 8 7 [DN] zT:ZERO LIQUID TEMP. DATA:25.00 [ESC] (Previous Menu) The liquid temperature at the time of zero calibration can be verified. [ESC] RETURN [UP] [DN] cG:RF COEF. DATA:0.00 [ESC] (Previous [ESC] RETURN Menu) [UP] [DN] zG:ZERO RF DATA The set value of the RF correction factor used for density calculation can be verified. Before shipment, this value is already set in accordance with the product's characteristics in the shipping test. If you change this value, it will affect the performance; therefore, normally, do not change it. The RF data at the time of zero calibration can be verified. DATA:50.00 [ESC] (Previous [ESC] RETURN Menu) [UP] [DN] ma:AVERAGING TIMES DATA:1 [ESC] (Previous [ESC] RETURN Menu) [UP] [DN] dx: CHANGE-RATE LIMIT DATA:0.00 [ESC] (Previous [ESC] RETURN Menu) [UP] The variation width (%TS) permitted in the change-rate limit function can be verified. [DN] HL:LIMIT TIMES [ESC] (Previous Menu) The set value of the moving average times can be verified. DATA:0 The times permitted in the change-rate limit function can be verified. [ESC] RETURN [UP] 42 6 F 8 A 0 7 8 7 [DN] C:DENSITY MULTIPLIER DATA:1.000 [ESC] (Previous Menu) [ESC] RETURN 43 6 F 8 A 0 7 8 7 5.2.8 Measured values display and operating procedures 1 :READ PARAMETERS 2 :MEASURED VALUES 3 :SELF-DIAGNOSIS [ESC] (Previous Menu) Move the cursor to "2" with [→] key, and press [SET] key to select [ 2:MEASURED VALUES] It is possible to verify the measured phase value (and the angle rotation N), the measured liquid temperature value, the measured atmospheric temperature value, as well as the density calculated based on them. [*] at the left end of the bottom line will blink synchronously with the data updating thus making it possible to verify that the data updating is definitely taking place. p PHASE: 123.56 N=0 T LIQ_TMP: 30.00 ℃ A AT_TMP : 30.00 ℃ *X DENSITY: 2.34 %TS: 5.2.9 Self-diagnosis data display operating procedures 1 :READ PARAMETERS 2 :MEASURED VALUES 3 :SELF-DIAGNOSIS Move the cursor to "3" with [→] key, and press [SET] key to select [3:SELF-DIAGNOSIS] ST:STATUS :GOOD [ESC] (Previous Menu) Whether the phase measurement operation is normally functioning or not can be verified. [ESC] RETURN [UP] [DN] SL:MICROWAVE SIG.LVL DATA :−53 The micro wave receive signal level can be verified. Normally, the level is -45 to -75. [ESC] (Previous [ESC] RETURN Menu) [UP] [DN] F:MICROWAVE COEF. The micro wave signal constant can be verified. Normally, the value is 1825 to 1975. DATA : 1910 [ESC] (Previous Menu) [ESC] RETURN [UP] 44 6 F 8 A 0 7 8 7 [DN] The converter's RF data (concerning the micro wave phase measurement) can be verified. Normally, the value is 10 to 70. G:RF DATA. DATA : 40.00 [ESC] [ESC] RETURN (Previous [UP] Menu) [DN] The voltage of the 5-volt power supply can be checked. J:+5V POWER SUPPLY DATA :5.00 [ESC] [ESC] RETURN (Previous Menu) [UP] [DN] The soundness of the phase measurement unit can be verified. pd:REF PHASE DATA:0.0 [ESC] (Previous Menu) [ESC] RETURN [UP] [DN] The soundness of various memory units can be verified. Mc:MEMORY CHECK:GOOD EPROM :GOOD RAM :GOOD EEPROM :GOOD [ESC] (Previous Menu) [UP] [DN] ST:STATUS :GOOD [ESC] (Previous Menu) [ESC] : RETURN 45 6 F 8 A 0 7 8 7 5.2.10 Parameter setting display and operating procedures 5:SET PARAMETERS 6:ZERO CALIBRATION 7:SPAN CALIBRATION 8:ANGLE ROTATION Move the cursor to "5" with [→] key, and press [SET] key to select[ 5:SET PARAMETERS] [ESC] (Previous Menu) UR:UPPER RANGE [SET](Set) UR:UPPER RANGE DATA:3.0 [SET] CHANGE [ESC] RETURN. [SET](Fix) RANGE :1.0-99.9 %TS DATA : [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] The upper density measurement range (whose current output is 20mA) is set. [DN] [ESC] (Previous Menu) LR:LOWER RANGE [SET](Set) LR:LOWER RANGE DATA:0.0 [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :0.0-99.5 %TS DATA : [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] The lower density measurement range (whose current output is 4mA) is set. [DN] a:DENSITY LINE SLOPE [SET](Set) a:DENSITY LINE SLOPE DATA:0.0840 [SET] CHANGE [ESC] RETURN RANGE :−0.2000−0.2000 DATA : [SET] SET,[ESC] CANCEL [SET](Fix) [ESC] (Previous Menu) [UP] [ESC](Cancel) The "density line slope" of the arithmetic expression for calculating the density from the phase measurement data, etc. is set. However, normally do not change settings here. [DN] b:DENSITY INTERCEPT [ESC] (Previous Menu) DATA:0.00 [SET] CHANGE [ESC] RETURN [UP] [DN] ot:DENSTY TEST OUT. [ESC] (Previous Menu) DATA:3.0 [SET] CHANGE [ESC] RETURN [UP] [DN] [SET](Set) [SET](Fix) [ESC](Cancel) b:DENSITY INTERCEPT RANGE :−99.99−99.99 DATA : [SET] SET,[ESC] CANCEL The "density intercept" of the arithmetic expression for calculating the density from the phase measurement data, etc. is set. In the event that the zero point is out of position, it is corrected through zero calibration; it is also possible to shift the zero point by changing this coefficient. Normally, set the value to zero. [SET](Set) [SET](Fix) [ESC](Cancel) ot:DENSTY TEST OUT. RANGE :0.0-99.9 %TS DATA : [SET] SET,[ESC] CANCEL When [2: SETTING MENU] is selected, the density output signal and the density display are hold in the simulated values that have been set. In this screen, the simulated values are set in terms of "%TS". 46 6 F 8 A 0 7 8 7 [DN] [ESC] (Previous Menu) dt:DELAYED SYNC.TIME [SET](Set) dt:DELAYED SYNC.TIME DATA:0.5 [SET] CHANGE [ESC] RETURN RANGE :0.1-99.9 min DATA : [SET] SET,[ESC] CANCEL [UP] [DN] [SET](Fix) [ESC](Cancel) In external synchronized operations, the delayed time from when the external contact input is turned ON until the measurement starts is set. For details, refer to Section 6.7. zp:ZERO POINT PHASE zp:ZERO POINT PHASE [SET](Set) [ESC] (Previous Menu) DATA:80.00 [SET] CHANGE [ESC] RETURN [SET](Fix) [ESC](Cancel) The zero-point phase can be set in this menu through manual input. Normally, the zero-point phase is automatically set when implementing the zero calibration. [UP] [DN] [ESC] (Previous Menu) zT:ZERO LIQUID TEMP. [SET](Set) zT:ZERO LIQUID TEMP. DATA:25.00 [SET] CHANGE [ESC] RETURN RANGE :0.00-100.00 ゚C DATA : [SET] SET,[ESC] CANCEL [SET](Fix) [ESC](Cancel) [UP] The zero-point liquid temperature can be set in this menu through manual input. Normally, the zero-point liquid temperature is automatically set when implementing the zero calibration. [DN] cG:RF COEF. [ESC] (Previous Menu) RANGE :0.00-359.99 DATA : [SET] SET,[ESC] CANCEL DATA: 0.00 [SET] CHANGE [ESC] RETURN [SET](Set) [SET](Fix) [ESC](Cancel) [UP] cG:RF COEF. RANGE : -9.99-9.99 DATA: [SET] SET,[ESC] CANCEL The RF correction factor used for density calculation is set. Before shipment, this value is already set in accordance with the product's characteristics in the shipping test. If you change this value, it will affect the performance; therefore, normally, do not change it. 47 6 F 8 A 0 7 8 7 [DN] [ESC] (Previous Menu) zG:ZERO RF DATA [SET](Set) DATA: 50.00 [SET] CHANGE [ESC] RETURN [SET](Fix) [ESC](Cancel) [UP] RANGE :0.00-100.00 ゚C DATA: [SET] SET,[ESC] CANCEL The zero-point RF data can be set in this menu through manual input. Normally, the zero-point RF constant is automatically set when implementing the zero calibration. [DN] [ESC] (Previous Menu) zG:ZERO RF DATA ma:AVERAGING TIMES [SET](Set) DATA:1 [SET] CHANGE [ESC] RETURN [SET](Fix) [ESC](Cancel) ma:AVERAGING TIMES RANGE : 1-99 DATA : [SET] SET,[ESC] CANCEL The moving average times are set. If the output averaged for density control, etc. is needed, the value from 5 to about 10 is set. [UP] [DN] [ESC] (Previous Menu) dx:CHANGE RATE LIMIT [SET](Set) DATA:0.00 [SET] CHANGE [ESC] RETURN [SET](Fix) [ESC](Cancel) [UP] If there is a signal of sharp variation, the change-rate limit function excludes this signal to restrict a sudden output variation. In this menu, the permissible variation width is set in terms of "%TS". [DN] HL:LIMIT TIMES [ESC] (Previous Menu) DATA: 0 [SET] CHANGE [ESC] RETURN [UP] [DN] dx:CHANGE RATE LIMIT RANGE :0.00-9.99 DATA: [SET] SET,[ESC] CANCEL [SET](Set) [SET](Fix) [ESC](Cancel) HL:LIMIT TIMES RANGE :0-99 DATA: [SET] SET,[ESC] CANCEL The limit times in the change-rate limit function are set. If the variation width exceeds dx(%TS) that was set in the previous menu, the signal is excluded for up to the HL times that are set in this menu. At HL=0, the change-rate limit function does not work. UR:UPPER RANGE [ESC] (Previous Menu) [NOTE]: DATA:3.0 [SET] CHANGE [ESC] RETURN For all menus, when data outside the allowed range is input, the error message is displayed, and the wrong data is refused. Press any key to return, and input adequate data. 48 VALUE OUT OF RANGE UR:UPPER RANGE PRESS ANY KEY TO RETURN 6 F 8 A 0 7 8 7 5.2.11 Zero calibration display and operating procedures 5:SET PARAMETERS 6:ZERO CALIBRATION 7:SPAN CALIBRATION 8:ANGLE ROTATION Move the cursor to "6" with [→] key, and press [SET] key to select [6:ZERO CALIBRATION] zp PHASE :81.23 ゜ N=0 [ESC] (Previous Menu) ZERO POINT zT TEMP. :26.55 °C zA TEMP. :26.55 °C *X DENSITY : 0.05 %TS [SET](Set) New data displayed CALIBRATION HAS BEEN COMPLETED Press the [SET] key for zero calibration. In zero calibration, the phase, the liquid temperature, the atmospheric temperature, and RF data of zero point will be replaced with the present measured values. And also, angle rotation "N" will be set to zero. Note:The display will return to the left display automatically after approximately one second. 5.2.12 Span calibration display and operating procedures 5:SET PARAMETERS 6:ZERO CALIBRATION 7:SPAN CALIBRATION 8:ANGLE ROTATION Move the cursor to "7" with [→] key, and press [SET] key to select [7:SPAN CALIBRATION] C1:DensityMultiplier [ESC] (Previous Menu) DATA:1.000 [SET] CHANGE [ESC] RETURN [SET](Set) C1:DensityMultiplier [SET](Fix) RANGE :0.000-9.999 DATA : [SET] SET,[ESC]CANCEL [ESC](Cancel) The density multiplier C1 should be set to the suitable value so that the measured density value is corresponding to the manual analysis value. For details, refer to Section 6.5. 49 6 F 8 A 0 7 8 7 5.2.13 Phase angle rotation correction display and operating procedures 5:SET PARAMETERS 6:ZERO CALIBRATION 7:SPAN CALIBRATION 8:ANGLE ROTATION Move the cursor to "8" with [→] key, and press [SET] key to select [8:ANGLE ROTATION] UH:UPPER ANGLE [ESC] (Previous Menu) DATA : 20 [SET] CHANGE [ESC] RETURN [SET](Set) UH:UPPER ANGLE [SET](Fix) RANGE :240-360 ゚ DATA : [SET] SET,[ESC] CANCEL [ESC](Cancel) Before shipping, this value is set to 260 degrees. Changing the setting may result in damaging the otherwise normal operation. Therefore, normally, do not change the setting. [UP] [DN] [ESC] (Previous Menu) SH:LOWER ANGLE [SET](Set) SH:LOWER ANGLE DATA :100 [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :0-120 ゚ DATA : [SET] SET,[ESC] CANCEL [ESC](Cancel) Before shipping, this value is set to 100 degrees. Changing the setting may result in damaging the otherwise normal operation. Therefore, normally, do not change the setting. [UP] [DN] [ESC] (Previous Menu) N:ROTATION [SET](Set) N:ROTATION DATA:0 [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :−10 - 10 DATA : [SET] SET,[ESC] CANCEL [ESC](Cancel) Normally, the angle rotation N is automatically computed; therefore, it is unnecessary to change the setting through manual input. However, there are some cases of high density measurements which require settings through manual input. [UP] [DN] UH:UPPER ANGLE [ESC] (Previous Menu) DATA :260 [SET] CHANGE [ESC] RETURN 50 6 F 8 A 0 7 8 7 5.2.14 Linearize/conductity correction display and operating procedures 9:LINEARIZ/CNDUCTVTY 10:ADDITIVES CORRECT 11:OTHERS Move the cursor to "9" with [→] key, and press [SET] key to select [ 9:LINEARIZ/CNDUCTVTY] LA:DENSITY A DATA :0.60 [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) [SET](Fix) [ESC](Cancel) [DN] DATA:1.00 [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) [SET](Fix) [ESC](Cancel) [ESC] (Previous Menu) RANGE :0.00-99.99 DATA : [SET] SET,[ESC] CANCEL In the event of three straight lines which closely analogous each other, the density of the crossover point B of the 2nd and 3rd lines is set. [DN] DATA:1.00 [SET] CHANGE [ESC] RETURN LB:DENSITY B [SET](Set) [UP] K1:COEF. RANGE :0.00-99.99 DATA : [SET] SET,[ESC] CANCEL In the event of three straight lines which closely analogous each other, the density of the crossover point A of the 2nd and 3rd lines is set. [UP] LB:DENSITY B LA:DENSITY A [SET](Set) [SET](Set) K1:COEF. [SET](Fix) RANGE:0.00-9.99 DATA : [SET] SET,[ESC] CANCEL [ESC](Cancel) In the event of three straight lines which closely analogous each other, the inclination K1 of the 1st line is set. [UP] [DN] K2:COEF. DATA:1.00 [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) [SET](Fix) [ESC](Cancel) [UP] K3:COEF. [SET](Set) DATA:1.00 [SET] CHANGE [ESC] RETURN [SET](Fix) [UP] RANGE:0.00-9.99 DATA : [SET] SET,[ESC] CANCEL In the event of three straight lines which closely analogous each other, the inclination K2 of the 2nd line is set. [DN] [ESC] (Previous Menu) K2:COEF. [SET](Set) K3:COEF. [ESC](Cancel) RANGE :0.00-9.99 DATA : [SET] SET,[ESC] CANCEL In the event of three straight lines which closely analogous each other, the inclination K2 of the 3rd line is set. 51 6 F 8 A 0 7 8 7 [DN] [ESC] (Previous Menu) r:CNDUCTVTY. COEF. [SET](Set) r:CNDUCTVTY. COEF. RANGE :10.00 [SET] DATA [ESC] RETURN [SET](Fix) RANGE :0.00-99.99 DATA : [SET] SET,[ESC] CANCEL [UP] [DN] [ESC] (Previous Menu) [ESC](Cancel) In the event of performing electric conductivity correction, the correction factor γ is set. At γ= 0.00, electric conductivity correction does not work. zE:CNDUCTVTY. /ZERO [SET](Set) DATA:3.00 [SET]( Fix in "LINE mode") [SET] CHANGE [ESC] RETURN MANU/LINE SELECTION RANGE :MANU/LINE DATA :(LINE) [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] and [DN] is used to switch between MANU/LINE to select the method for setting the zero-point electric conductivity. By selecting "LINE" and pressing [SET] in the zero-point state (see the screen above), the electric conductivity signal of the zero point is read to be automatically set as the zero-point electric conductivity. [UP] MANU/LINE SELECTION RANGE :MANU/LINE DATA:(MANU) [SET] SET,[ESC] CANCEL [ESC] [DN] (Cancel) zE:CNDUCTVTY. /ZERO RANGE :0.00-10.00 DATA : [SET] SET,[ESC] CANCEL EC:CONDUCTIVITY [SET](Set) MANU/LINE SELECTION DATA:1.23(LINE) [SET] CHANGE [ESC] RETURN [SET](Fix in "LINE mode") RANGE :MANU/LINE DATA:(LINE) [SET] SET,[ESC] CANCEL [ESC](Cancel) Selecting MANU/LINE with [UP] or [DN], the setting [ESC] (Previous Menu) [UP] method of electric conductivity correction can be chosen. or [DN] When “LINE” is selected (above screen), and then pressing [SET], the density measurement with continuous conductivity correction will be made using the conductivity signal from the object to be measured. MANU/LINE SELECTION RANGE :MANU/LINE DATA:(MANU) [SET] SET,[ESC] CANCEL [DN] [ESC] (Cancel) EC:CONDUCTIVITY LA:DENSITY A [ESC] (Previous Menu) DATA :0.60 [SET] CHANGE [ESC] RETURN By selecting "MANU" (see the screen above) and then pressing [SET], the electric conductivity of the measured object is made settable as the fixed value through manual input. After the zero-point electric conductivity is entered, [SET] is used to confirm the setting in MANU mode. 52 RANGE :0.00-10.00 DATA: [SET] SET,[ESC] CANCEL 6 F 8 A 0 7 8 7 5.2.15 Additives correction display and operating procedures 9:LINEARIZ/CNDUCTVTY 10:ADDITIVES CORRECT 11:OTHERS Move the cursor to "10" with [→] key, and press [SET] key to select [10:ADDITIVES CORRECT ] [SET](Set) AF:ADDITIVES COMP. [ESC] (Previous Menu) DATA :ON [SET] CHANGE [ESC] RETURN AF:ADDITIVES COMP. [SET](Fix) [ESC](Cancel) Each time the [UP] or [DN] key is pressed, OFF/ON are mutually alternated thus making it possible to select the availability of the additives correction function. If OFF is selected, the following screen will not appear. [UP] [DN] Ad:DISPLAY DENSITY [ESC] (Previous Menu) DATA:TOTAL [SET] CHANGE [ESC] RETURN [UP] RANGE :OFF/ON DATA:ON [SET] SET,[ESC] CANCEL [SET](Set) Ad:DISPLAY DENSITY [SET](Fix) [ESC](Cancel) RANGE :TOTAL/MAIN DATA:TOTAL [SET] SET,[ESC] CANCEL Each time the [UP] or [DN] key is pressed, TOTAL/MAIN are mutually alternated thus making it possible to switch between density calculations to be displayed. If TOTAL is selected, the density of the entirety in which the pulp and the additives are combined will be displayed. If MAIN is selected, the density of only the pulp, which is the main object, will be displayed. [DN] [ESC] (Previous Menu) Ac:OUTPUT DENSITY [SET](Set) Ac:OUTPUT DENSITY DATA:TOTAL [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :TOTAL/MAIN DATA:TOTAL [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] Each time the [UP] or [DN] key is pressed, TOTAL/MAIN are mutually alternated thus making it possible to switch between density calculations to be output. If TOTAL is selected, the density of the entirety in which the pulp and the additives are combined will be output. If MAIN is selected, the density of only the pulp, which is the main object, will be output. 53 6 F 8 A 0 7 8 7 [DN] Ap:PARAMETER SET NO. DATA:01 [ESC] [SET] CHANGE (Previous [ESC] RETURN [SET](Set) [SET](Fix) [ESC](Cancel) Menu) [UP] [DN] [ESC] (Previous Menu) Ap:PARAMETER SET NO. RANGE:1 - 10 DATA:01 [SET] SET,[ESC] CANCEL Ten parameter sets (tables for each brands) can be registered for additives correction. This is used for selecting the parameter set number appropriate to the brand in the event of making measurements with additives correction, or for selecting the parameter set number in the event of newly registering or changing an individual parameter. s0:MAIN OBJ. SENS. [SET](Set) s0:MAIN OBJ. SENS. DATA:1.00 [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :−9.99 - 9.99 DATA:1.00 [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] The sensitivity of component 0 (pulp) is set. [DN] [ESC] (Previous Menu) s1:ADDITIVE SENS. [SET](Set) s1:ADDITIVE SENS. DATA:1.00 [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :−9.99 - 9.99 DATA:1.00 [SET] SET,[ESC] CANCEL [ESC](Cancel) The sensitivity of additive 1 is set. In the same manner, the sensitivities of the following additives 2 to 5 are set. [UP] [DN] [ESC] (Previous Menu) s2:ADDITIVE SENS. [SET](Set) s2:ADDITIVE SENS. DATA:1.00 [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :−9.99 - 9.99 DATA:1.00 [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] [DN] [ESC] (Previous Menu) s3:ADDITIVE SENS. [SET](Set) s3:ADDITIVE SENS. DATA:1.00 [SET] CHANGE [ESC] RETURN [SET](Fix) [ESC](Cancel) RANGE :−9.99 - 9.99 DATA:1.00 [SET] SET,[ESC] CANCEL s4:ADDITIVE SENS. [SET](Set) s4:ADDITIVE SENS. DATA:1.00 [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :−9.99 - 9.99 DATA:1.00 [SET] SET,[ESC] CANCEL [UP] [DN] [ESC] (Previous Menu) [ESC](Cancel) [UP] 54 6 F 8 A 0 7 8 7 [DN] s5:ADDITIVE SENS. DATA:1.00 [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) [SET](Set) s5:ADDITIVE SENS. [SET](Fix) [ESC](Cancel) RANGE :−9.99 - 9.99 DATA:1.00 [SET] SET,[ESC] CANCEL [UP] [DN] R1:ADDITIVE RATIO DATA:0.000 [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) R1:ADDITIVE RATIO [SET](Set) RANGE :0.000 - 1.999 DATA:0.100 [SET] SET,[ESC] CANCEL [SET](Fix) [ESC](Cancel) [UP] The additive ratio of additive 1 (the mass ratio with regard to component 0) is set. In the same manner, the sensitivities of the following additives 2 to 5 are set. [DN] R2:ADDITIVE RATIO DATA:0.000 [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) [SET](Set) [SET](Fix) R2:ADDITIVE RATIO RANGE :0.000 - 1.999 DATA:0.100 [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] [DN] R3:ADDITIVE RATIO DATA:0.000 [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) [SET](Set) [SET](Fix) R3:ADDITIVE RATIO RANGE :0.000 - 1.999 DATA:0.100 [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] [DN] R4:ADDITIVE RATIO [ESC] (Previous Menu) DATA:0.000 [SET] CHANGE [ESC] RETURN [SET](Set) [SET](Fix) R4:ADDITIVE RATIO RANGE :0.000 - 1.999 DATA:0.100 [SET] SET,[ESC] CANCEL [ESC](Cancel) [UP] [DN] R5:ADDITIVE RATIO [ESC] (Previous Menu) DATA:0.000 [SET] CHANGE [ESC] RETURN [SET](Set) [SET](Fix) [ESC](Cancel) [UP] [DN] AF:ADDITIVES COMP. [ESC] (Previous Menu) DATA :ON [SET] CHANGE [ESC] RETURN 55 R5:ADDITIVE RATIO RANGE :0.000 - 1.999 DATA:0.100 [SET] SET,[ESC] CANCEL 6 F 8 A 0 7 8 7 5.2.16 Other menus display and operating procedures 9:LINEARIZ/CNDUCTVTY 10:ADDITIVES CORRECT 11:OTHERS Move the cursor to "11" with [→] key, and press [SET] key to select [ 11:OTHERS] ho:4-20mA IN [EXT] [SET](Set) ho:4-20mA IN [EXT] DATA :4mA [SET] CHANGE [ESC] RETURN [SET](Fix) RANGE :LAST/4mA/TEST DATA: [SET] SET,[ESC] CANCEL [ESC] (Previous [UP] Menu) [DN] [ESC](Cancel) The simulated output at contact OFF in the event of external synchronized operation can be selected. Each time the[UP] or [DN] key is pressed, the mode display is switched around among LAST VALUE (immediately preceding value), 4mA and TEST OUTPUT (simulated output 0.0 to 99.9%TS when in setting mode). [SET] is pressed with the mode display to select. DI:C CHANGE. ON/OFF DATA :ON/OFF [SET] CHANGE [ESC] RETURN [ESC] (Previous Menu) [UP] [DN] [SET](Fix) [ESC](Cancel) [DN] [ESC] (Previous Menu) RANGE :ON/OFF DATA: [SET] SET,[ESC] CANCEL [SET](Set) C2:DensityMultiplier [SET](Fix) RANGE :0.000-9.999 DATA: [SET] SET,[ESC] CANCEL [ESC](Cancel) In the event of performing the density multiplier switching by means of the external voltage signal (DI) of two points, the second density multiplier is set. In the same manner, the following 3rd and 4th density multipliers are set. The first density multiplier is performed with the menu for span calibration. C3:DensityMultiplier [SET](Set) C3:DensityMultiplier DATA:1.000 [SET] CHANGE [ESC] RETURN [SET](Fix) [ESC](Cancel) RANGE :0.000-9.999 DATA: [SET] SET,[ESC] CANCEL C4:DensityMultiplier [SET](Set) C4:DensityMultiplier DATA:1.000 [SET] CHANGE [ESC] RETURN [SET](Fix) [ESC](Cancel) RANGE :0.000-9.999 DATA: [SET] SET,[ESC] CANCEL [UP] [ESC] (Previous Menu) [UP] [DN] [DN] NA:N AUTO ADJUSTMENT [SET](Set) NA:N AUTO ADJUSTMENT DATA:ON [SET](Fix) [ESC](Cancel) RANGE :ON/OFF DATA: [SET] SET,[ESC]CANCEL [ESC] [SET] : CHANGE (Previous [ESC] : RETURN Menu) [UP] [DN] ho:4-20mA IN [EXT] [ESC] (Previous Menu) DI:C CHANGE. ON/OFF Up to four density multipliers can be switched around by the external voltage signal (DI) of two points. This is used for switching the brand, etc. On this menu, whether to perform the density multipliers switching (ON) or not (OFF) is selected. Each time the [UP] or [DN] key is pressed, ON/OFF are mutually alternated. C2:DensityMultiplier DATA:1.000 [SET] CHANGE [ESC] RETURN [UP] [SET](Set) DATA :4mA [SET] CHANGE [ESC] RETURN Although, in the event of high density measurement, the software is installed in such a manner that the automatic adjustment function of the phase angle rotation is automatically canceled (OFF) by the setting full-scale (the upper density measurement range), the function can also be canceled by force through manual input. However, normally, set it to "ON". Each time the [UP] or [DN] key is pressed, ON/OFF are mutually alternated. 56 6 F 8 A 0 7 8 7 6. Operations 6.1 Procedures for Preparing and Running Make preparations and perform operations, that is, density measurements, in accordance with the following procedure. Verifying the piping See 6.2 (1) Verifying the valve closure See 6.2 (2) Verifying the cable connection See 6.2 (3) Verifying the converter power-ON & display See 6.3.1 (1) Warm-up See 6.3.1 (2) Verifying and setting measurement conditions See 6.3.2 (1) and (2) Filling up the piping system (in which the density meter is installed) with fresh water (density 0%) See 6.4 (2) to (10) Normally omitted. Zero calibration See 6.4 (11) to (15) Pour the fluid to be measured Span calibration See 6.5 Startup See 6.6 57 6 F 8 A 0 7 8 7 6.2 Preparations before Turning on Power (1) Check piping Check piping and ensure that there are no loose nuts and bolts, or missing gaskets. Make sure that the density meter is properly connected in the pipeline. See the section 3.3, “Precautions when installing the density meter in a tank”. (2) Close the valves Make sure that the drain valve, sampling valve, and zero water valve, which are installed in the pipeline, are all closed. (3) Verifying the cable connection It is verified that cables are correctly connected to their respective terminal blocks. It is verified that the ground (grounding resister: less than 100 Ω) is reliably connected to this density meter. In the event of performing an external synchronized operation, the external contact input signal connected with ON/OFF of the pump is required; therefore, make sure that the external contact input signal cable is reliably connected. 6.3 Power on and Preparations for Measuring 6.3.1 Turning power on (1) Turn the power switch on Turn on the power switch of the converter and see that the power indicator(「POWER」), the density indicator, and the LCD display are lit. (2) Warming-up Please warm up for 30 minutes or more to achieve a steady measurement after turning power on. 58 6 F 8 A 0 7 8 7 6.3.2 Verifying and setting measurement conditions (1) Verifications and settings for initial powering-ON In the event of starting the operation after turning on the power for the first time since installing this density meter, it is necessary to first set the measurement conditions of the converter. Various measurement conditions (parameters) are verified and set by means of the setting key while viewing each menu screen of the LCD indicator. Major measurement conditions are as follows. 1) 2) 3) 4) 5) [NOTE] Verifying and setting the measurement range. Unless otherwise specified in your order, the value here is set to 0 to 3%TS, which is the provisional set value at the time of factory shipment. Reset the value in accordance with the operation condition of your plant. If the measurement range is specified in your order, verify that the value is set as specified. If the value is different, reset it. Verifying and setting the operation mode At the time of factory shipment, this is set to "CONT" (the normal continuous operation mode). In the event of the density meter being made empty due to pump shutdown or valve closure, etc. or of using such a method that stops the flow for some time, it is recommended that "EXT" (the external synchronized operation of switching between ON/OFF of measurement by means of ON/OFF of the external contact input signal connected with the pump ON/OFF) be selected. In the event that the external synchronized operation is selected, the values of “delayed time (dt)” and “output at contact OFF(ho)” are the provisional set values at the factory shipment. If the those values are meet to the operation conditions of the plant rest it to an appropriate value in accordance with the operation conditions of the plant. Verifying and setting the simulated output in setting mode. Normal measurements are suspended while this density meter is in the setting mode (see “2 SETTING MENU”); thus, both the density display and the density output are given the simulated values ( density test output (ot)) that are set beforehand. Although, at the time of factory shipment, the value is provisionally set to "1.5%TS" (50% of the specified full-scale density if the measurement range is specified), reset it to an appropriate value in accordance with the operation conditions of the plant. Verifying and setting the moving average times At the time of factory shipment, the "moving average times" is set to 1 (without the moving average). If the averaged output is required to be used for density control, etc., set it to about 10. The more the moving average times, the worse the responsiveness becomes with regard to density variation. Therefore, set it to an appropriate value in accordance with the plant conditions, including the right balance with the responsiveness. For other measurement conditions, the standard values are set. Therefore, it is normally unnecessary to change these settings. "10 VARIOUS FUNCTION" describes various functions of the Density Meter LQ300A00******. If necessary, make additional settings for using these functions appropriately. (2) Verifications at the time of normal power-ON In the event that measurement conditions of the converter are already set with the operation not being the first one since installation, verify the set value while referring to (1). 59 6 F 8 A 0 7 8 7 6.4 Zero Calibration All the density meters are calibrated for zero point [zero point phase ( θ1 ) zero point liquid temperature (T0), and atmospheric temperature (A0) ] at the time of shipment and parameters are set correctly. You do not need to calibrate the meter for zero point before using it at site. In the case of the density readings are found to be way off from the result by manual analysis, or when you need to read just the zero point for a particular reason, follow the procedures below in calibrating the zero. For information on the converter operation and the LCD display regarding zero-point calibration, please refer to Subsection 5.2.11. (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid." Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Stop the flow in or out from the tank and in the piping system. If it is possible to stop the flow in or out from the tank and in the piping system where the density meter is installed, do so by, for example, turning off the pump. ● If it is not allowed to stop the fluid flow through the pipeline: When it is not permitted to stop the flow of the line, bypass the flow by opening the valve on the bypass pipe. ◆ It is recommended that the bypass piping be installed for adjustment/maintenance purposes such as zero calibration in the event that the flow in the pipe line cannot be stopped. (3) Close the upstream valve and downstream valve Close the shutoff valves on both sides of the detector tightly. Note: Be sure to close the upstream valve first. ◆ In the event that the density meter is installed on the discharge side of the pump, make sure to shut the valves starting from the upstream one to prevent the fluid pressure in the density meter from rising. (4) Drain the detector pipe Open the drain valve on the pipeline to discharge the fluid from the main pipe of the detector. (5) Open the zero water feed port Open the valve or remove the cap to feed zero water. ◆ Make sure that the pressure of the fluid in the detector gets low enough to let the valve open without causing blow out of the fluid. Any remaining pressure will cause the measured matter to be spurted out. Be careful about this. (6) Close the drain valve 60 6 F 8 A 0 7 8 7 (7) Supplying zero water Put zero water (such as tap water) in the density meter pipe through the zero water supply port by using a vinyl hose. (8) Clean the tank or the piping system where the density meter is installed. When the detector main pipe is filled with water, open the drain valve to let out the water from the main pipe. Wash inside of the tank or the piping system where the density meter is installed by repeating steps (7) and (8) until the water density can be said to be zero against the density of the object fluid. (It is not necessary to make the water clean and transparent.) (9) Fill the tank or the piping system where the density meter is installed. When cleaning is finished, close the drain valve and fill the tank or the piping system with zero water. Keep adding water while releasing air until water overflows the supply port. (10) Wait Leave the detector and water in this state for about 5 minutes. ◆ In the event that the flow of the measured matter can be switched to that of the zero water by switching over to another valve, etc., it is all right to replace the work activities (2) to (10) with the relevant method and implement the following zero calibration while allowing the zero water to keep flowing. Even when switching the flow to that of zero water, wait for about 15 minutes before implementing the zero calibration. (11) Selecting the zero calibration menu (see Subsection 5.2.5) After verifying that the converter is in the setting mode ("2 SETTING MENU") through the operation of (1), use the [→] key to move the cursor of the LCD indicator to the menu number "6" of [6 ZERO CALIBRATION] and then press the [SET] key. (12) Check zero water density reading (see Subsection 5.2.11) The measured density of zero water is displayed on the density indicator. If the indicator shows [-0.00], it means that the zero point is off toward the negative. ◆ In the Setting menu, LED density display indicates the preset Density Test output, but in the Zero calibration menu, the LED density display indicates the density value measured at the same time the calibration is executed so that it is possible to check the zero point before and after the calibration. (13) Zero calibration (see Subsection 5.2.11) If the zero point is found to be off, press the [SET] key. The data (θ1, T 0, A0, zG) of the zero point is replaced by the current data, thus rendering the angle rotation to N=0 and automatically the density display to zero. The data (θ1, T0, A0, zG) of the zero point is stored in the memory of the density meter until the zero calibration is implemented once again, thus making it possible to verify it on the constant monitoring menu. However, for the purpose of history management, keep a note of the data. ◆ Unless the zero point is out of place, the zero calibration is suspended by pressing the [ESC] key. (14) End zero calibration This completes the zero calibration. Close the zero water valve, ensure that the sampling valve and drain valve are closed, then open the shutoff valves on both ends of the detector pipe, downstream first and upstream next. Lastly, close the shutoff valve on the bypass pipe to restore the flow of the fluid as before the calibration. 61 6 F 8 A 0 7 8 7 (15) Restoring to the measuring mode Press the [ESC] key of the converter twice to return the menu of the LCD indicator to the initial menu display to return to the usual measuring mode from the setting mode. Thus, the measurement starts. ◆ In the event that the external synchronized operation is selected, the external contact input signal is changed to ON, thus starting the density measurement after the specified delayed time has elapsed. 6.5 Span Calibration Span calibration is for adjusting the readings of the density meter to the values determined by manual (off-line) analysis. For information on the converter operation and the LCD display regarding span calibration, please refer to Subsection 5.2.12. (1) Preparations for manual analysis Prepare following items for manual analysis; a moisture meter (for example, an infrared moisture [NOTE] meter, with the accuracy or percentage reading down to 0. 1 %), plastic bottles of about l liter with a wide opening, and plastic beakers of about l00 ml for manual analysis. (2) Sample fluid for manual analysis Slightly open the sampling valve on the pipeline and let out the fluid a while before filling a 1liter bottle to half. Read and record the density value of the current fluid. ◆ Make sure to carry out the sampling when the density of the measured matter is in a stable state with the measured matter flowing. (3) Manual analysis Put a part of the sample fluid into a 100-ml plastic beaker, and measure the density of it using drying and weighing method of analysis. (4) Calculation of density multiplier Use the result of analysis to calculate a density multiplier using the following equation after the manual analysis conducted: Density multiplier C = A/(M/C’ ) where M is the density by the density meter (as read and recorded); A is the result of the manual analysis C’ is the density multiplier before span calibration (Initially, C’ is equal to 1.000 which is the value set in the factory before shipping) For example, if M = 4.0 z%TS, A = 4.8 %TS and C’ =1.000 C = 4.8 / (4.0/1) = 4.8/4.0 = 1.2 ◆ In the case that span calibration has been done already, and density multiplier C is not 1.000, the new density multiplier C can be calculated in the following way. For example, if M = 4.8 %TS, A = 4.2 %TS and C0=1.2 C = 4.2 / (4.8/1.2) = 4.2/4 = 1.05 62 6 F 8 A 0 7 8 7 (5) Setting the density multiplier (5-1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status). Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Tset output will be vaild." Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (5-2) Selecting the converter constant setting menu (see Subsection 5.25) The menu list of menu numbers 5 to 8 is displayed. Use the [→] key to move the LCD indicator cursor to the menu number "7" of "7: SPAN CALIBRATION" and then press the [SET] key to select the menu of "7: SPAN CALIBRATION." ◆ In the Setting menu, LED density display indicates the preset Density Test output, but in the Span calibration menu, the LED density display indicates the density value measured at the same time the calibration is executed so that it is possible to check the density measured value before and after the calibration. (5-3) Verifying and recording the density multiplier before span calibration For example, the set value of the current density multiplier as is displayed as in "DATA: 1.000" is displayed. Record this value. (5-4) Setting the density multiplier Press the [SET] key to switch over to the setting menu of the density multiplier and enter the density multiplier found in (4). Use the [→] key to move from one digit to another. Use the [UP] and [DN] keys to switch around the number of the relevant digit. When the input is completed, press the [SET] key to confirm it. Then, the display will be returned to the immediately preceding menu screen. Verify that the resetting has been done correctly. [NOTE] (5-5) Restoring to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode, thus restarting the usual measurement. Verify that the density display has been changed appropriately in accordance with the setting of the density multiplier. ◆ In the event that the external synchronized operation is selected, the external contact input signal is changed to ON, thus starting the density measurement after the specified delayed time has elapsed. (6) Completing the span calibration Thus, the span calibration is completed. The above describes the method for finding the density multiplier as an example in the comparison with onetime manual analysis. However, to exclude errors caused by sampling, it is recommended that as many comparative data as possible be collected to find the density multiplier from their mean value. 63 6 F 8 A 0 7 8 7 6.6 Operation (1) Startup (see Subsection 5.2.5) When the power is turned ON, the menu setup is automatically changed to the measuring mode (the state of "1: MONITORING MENU"), thus starting the density measurement. If the meter is in setting mode (the state of "2:SETTING MENU"), the density measurement operation is started by pressing the [ESC] key several times (varying between one to three times depending on the operation status) and thus pulling the menu setup out of the setting mode. ◆ In the event that the external synchronized operation is selected, the menu setup is changed to the measuring mode and the external contact input signal is turned ON, thus starting the density measurement after the specified delayed time has elapsed.. (2) Executing the measurement Executes the density measurement while updating the output values (density current output value; LED density display; LCD density display on the monitor menu) approximately every second. (3) Suspending the measurement (see Subsection 5.2.5) When stopping the measurement, select "2: SETTING MENU" from the initial menu list to get into the setting mode. Once in the setting mode, the density measurement will be suspended and the output will be switched to the simulated value that was set beforehand. ◆ In the event that the external synchronized operation is selected, the density measurement is suspended if the external contact input signal is turned OFF even in the measuring mode. For details including the output when the density measurement is suspended, refer to Section 6.7. [NOTE] ◆ In the event that the measured matter does not flow continuously or the interior of the detector is temporarily left empty due to the intermittent operation of the shifting pump to the tank or the piping system on which the tank or the piping system (where the density meter is installed) is installed, perform the external synchronized operation described in Section 6.7. ◆ When the flow in the pipe has stopped, solid matters may subside or float causing the density in the pipe to lose its uniformity, which in turn may cause the density measured value to gradually rise or fall. In addition, if some fluid escapes from the pipe and thus the tank or the piping system (where the density meter is installed) is not completely full of the measured matter, the density measured value turns out to be erroneous (such as full-scale excess; shift to the minus side; major marginal error). However, this does not mean that the density meter has failed. Even to avoid such a phenomenon, it is necessary to perform the external synchronized operation. 64 6 F 8 A 0 7 8 7 6.7 External Synchronized Operation This operation mode is used in the event that the measured matter does not flow continuously or the interior of the detector is temporarily left empty due to the intermittent operation of the shifting pump to the pipe line on which the density meter is installed. This mode is used to take measurements only when operating the shifting pump. To use this operation mode, it is necessary to connect the shifting pump operation and the contact signal (no-voltage) to the external synchronized input signal pins beforehand. 6.7.1 Movement of the external synchronized operation Time Pump operating status (External contact) Pump shutdown (OFF) Pump operation (ON) Pump shutdown (OFF) Time Density measuring status(Output) Suspension of density measurement (Simulated output) Execution of density measurement (Measured value output) Suspension of density measurement (Simulated output) Delayed time Fig.6.7.1 External synchronized Operation The external synchronized operation, as shown in Fig. 6.7.1, is so designed that the density measurement is executed only while the pump is being operated; and the density measurement is suspended while the pump is shut down and the simulated output is issued during this time. The external synchronized operation is effective in preventing the following inadequate phenomena. (1) The pump shutdown causes solid matters to subside or float thus making it impossible to take density measurements correctly. (2) The pump shutdown may cause the fluid to escape from the tank or the piping system (where the density meter is installed) thus either leaving it completely empty or insufficiently filled with fluid. In such a situation, the measured value of the density meter falls into error such as full-scale excess, shift to the minus side, or occurrence of fluctuation within major marginal error. It takes time for the tank or the piping system (where the density meter is installed) to be filled sufficiently with the measured matter after the pump is operated. Here, it is so arranged that the measurement start after the "delayed time" that is set beforehand has elapsed since receiving the contact signal linked with the pump operation. Make sure that the delayed time that is set is sufficient for the whole process of the pipe length and flow, etc. from the pump to the density meter. As the simulated value when the density measurement is suspended, it is possible to select from among three options: "4mA", "density measured value immediately preceding the pump shutdown" and "simulated output in setting mode". The default value is 4mA. However, make sure to select a simulated output suitable to your system. 65 6 F 8 A 0 7 8 7 6.7.2 Setting the external synchronized operation (1) Setting the delayed time (see Subsection 5.2.10) (1-1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid." Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (1-2) Selecting the parameter setting menu (see Subsection 5.25) The menu list of menu numbers 5 to 8 is displayed. Use the [→] key to move the LCD indicator cursor to the menu number "5" of "5: SET PARAMETERS" and then press the [SET] key to select the menu of "5: SET PARAMETERS." (1-3) Setting the delayed time at the time of external synchronized(see Subsection 5.2.10) Press the [UP] key five times to select the setting menu of the delayed time at the time of external synchronized(dt: DELAYED SYNC. TIME). Press the [SET] key to get into the set value input screen and then enter an appropriate value (the time sufficient for the measured matter to flow up to the density meter and fill up the pipe after the shifting pump operation is started). Use the [→] key to move from one digit to another. Use the [UP] and [DN] keys to switch around the number of the relevant digit. When the input is completed, press the [SET] key to confirm it. Then, the display will be returned to the immediately preceding menu screen. Verify that the resetting has been done correctly. (2) Setting the simulated output at measurement suspension (at external contact OFF) (see Subsection 5.2.16) As the simulated output when the measurement is suspended (at external contact OFF), it is possible to select from among three options as shown in Table 6.7.1. Make sure to select a simulated output suitable to your system. Table 6.7.1 Density Display and Output at Measurement Suspension in External Synchronized Operation Mode "LAST" "4mA" (Standard) Density Indicator Display Holds the density measured value immediately before OFF Held in 0%TS "TEST" same as the simulated output value in setting mode "LAST" Holds the density measured value immediately before OFF 66 Output (4 - 20mA) Holds the density measured value correspondence output immediately before OFF Output held in 4mA Same as the simulated output value correspondence output in setting mode Holds the density measured value correspondence output immediately before OFF 6 F 8 A 0 7 8 7 (2-1) Selecting the "OTHERS" setting menu (see Subsection 5.2.5) Continuing on from (1), press the [ESC] key to return to the display of menus 5 to 8 in setting mode. Press the [UP] key to switch to the display of the next menus 9 to 11. Use the [→] key to move the cursor of the LCD indicator to the menu number "11" of "11: OTHERS" and press the [SET] key to select the "11: OTHERS" menu. (2-2) Setting the output mode at contact OFF in external synchronized operation (see 5.2.16) The current output mode at contact OFF in external synchronized operation is displayed in the initial menu "ho: 4-20mA IN [EXT]" of "11: OTHERS". To make changes, it is necessary to press the [SET] key and place the software in the setup state. Each time the [UP] or [DN] key is pressed, the mode display is switched around from "LAST" (immediately preceding value), through "4mA" to "TEST" (the simulated output value in setting mode). Press the [SET] key on the display in the selected mode to confirm. The screen is returned to that of the immediately preceding menu screen. Make sure that the resetting is done correctly. (2-3) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu and return from the setting mode to the measuring mode to resume the normal measurement. (3) Setting the operation mode (3-1) Selecting the operation mode change menu (see Subsection 5.2.6) In the initial menu, use the [→] key to move the cursor of the LCD indicator to the menu number "3" of "3: MEASURING MODE" and then press the [SET] key to get into the operation mode menu. (3-2) Verifying and setting the operation mode The current operation mode is displayed at "DATA" of the LCD indicator . "CONT" refers to the mode of taking measures continuously without relying on the status of the external contact signal, whereas "EXT" refers to the external synchronized operation mode. If the current setting is "CONT," press the [SET] key to get into the setup screen of operation mode; press the [UP] or [DN] key to switch the set value of the operation mode to "EXT"; and press the [SET] key to confirm. The screen is returned to the immediately preceding menu screen. Make sure that the resetting has been done correctly. (4) Starting the external synchronized operation With the settings above, measurement ON/OFF are proceeded with as shown in Fig.6.7.1 in accordance with external synchronized contact signal ON/OFF. 6.8 Functions Related to Operation To enable you to use the Insertion Type Density Meter LQ300A00****** more appropriately in various processes and situations, the device is equipped with various functions including the moving average, the change-rate limit, the electric conductivity correction, the additive correction, the linearizer and the density multiplier switching by external signals. Make settings necessary for using these functions appropriately where necessary. For details, please refer to Chapter 10. 67 6 F 8 A 0 7 8 7 7 MAINTENANCE 7.1 Precautions for Maintenance, Inspection, and Parts Replacement Yellow DO WARNING ■ Be sure to turn the power switch on the equipment to OFF before doing maintenance or inspection inside the equipment or replacing its parts. ■ Be sure to set the power switch on the equipment to OFF before replacing fuse. DO Failure to observe this can cause electric shock. Failure to observe this can cause electric shock or equipment failure. DO ■ Avoid touching the terminal block during maintenance or inspection. If it is necessary to touch the terminal block, turn the power switch on the equipment to OFF in advance. ■ Do not attempt to disassemble or modify the equipment DON’T Failure to observe this can cause electric shock or equipment failure. Failure to observe this can cause electric shock. Yellow The sticker shown left is pasted near a terminal block on the equipment to which power is supplied. Take care to avoid electric shock Yellow 68 6 F 8 A 0 7 8 7 7.2 Maintenance and Inspection Items Periodic maintenance and inspection is necessary for reliable measurement over a long period of time. Since the density meter has no mechanically moving parts, however, it does not require replacement of mechanism elements in a normal operating environment. Compare the density measured value and the manually analyzed value in the cycle shown in Table 7.1. If necessary, implement the span calibration after implementing the zero calibration. The spare parts that must be kept on hand are the fuses in Table 7.2. Table 7.1 Maintenance and Inspection Items Item Cycle Comparison of density meter measured value When necessary with manually analyzed value Materials accumulated or entangled, or When necessary physical damage [NOTE] Remarks At least three samples are desirable. ◆ If the density meter measured value deviates from the manually analyzed value to the extent of causing obstacles, implement the span calibration (changing the density multiplier C) while referring to Section 6.5. ◆ If the density meter measured value greatly deviates from the manually analyzed value by less than half or more than twice, implement the span calibration after implementing the zero calibration while referring to Section 6.4 and 6.5. ◆ When the density meter is used in an application where the process fluid contains plenty of fur or fiber, these substances may accumulate or entangle in the insertion probe area and thus perform the maintenance and inspection operation, and cleaning periodically. ◆ Take extra care not let the applicators (antenna) hit the hard object. Table 7.2 Spare Parts Name Fuse [NOTE] Specifications 1A(M),250V cartridge, glass tubular fuse, 5.2mm outer dia. x 20mm long Qty ◆ Fuses are parts with expected life span. Therefore, replace them periodically. (Recommended replacement cycle: about 3 years) ◆ In general, the service life of an electronic part becomes shorter at higher ambient temperature. Electrolytic capacitors are used in the converter and their service life is about 10 years at the ambient temperature of 20°C or about 3 years at 50°C. For stable use of the meter for many years, it is desirable to replace these parts in time. When replacing the capacitors, please contact Toshiba's Service Dept. ◆ In the event that the characters on the LCD display becomes weak in contrast or edge, it is considered that the LCD display unit has reached the end of its life. Although such unsatisfactory visibility may not affect the performance of the density measurement, the display unit should be replaced if it interferes with the operation. When replacing the display unit, contact Toshiba's Service Dept. 69 6 F 8 A 0 7 8 7 8 TROUBLESHOOTING 8.1 Troubleshooting If any trouble has developed, make a careful check and take appropriate steps. Table 8.1 shows possible troubles, their causes, and remedies. If anything wrong occurs, refer to the table below and take the necessary steps. If that does not remedy the trouble, send information on the trouble, in as much detail as possible, and self-diagnosis data to our Service Department. Table 8.1 Troubleshooting (1) No. Trouble Converter power cannot be switched on. Cause AC power is not supplied. Check terminals [L1] and [L2] on terminal block with voltage tester. If AC voltage is not supplied, supply AC power in accordance with specifications. Fuse (1A) is blown. Replace fuse. In accordance with Section 8.2, perform self-diagnosis data check and restoration operations. If ALARM indicator lights again, send self-diagnosis data to our Service Department. ALARM indicator lights; density meter error contact output.. Fault in the density meter While the flow is stagnant, the indicator is in error. The fluid drained out in the piping system where the density meter is installed. While the flow is stagnant, the measured density value slowly increases or decreases. Remedy Use the externally synchronized Density becomes uneven because the operation. measurement object fluid in the fluid in See Section 6.7. (Density meter is not faulty.) the pipe starts to sinks or floats, thus causing the density in the center portion of measured fluid to increase or decrease. 70 6 F 8 A 0 7 8 7 Table 8.1 Troubleshooting (2) No. Trouble Cause Inappropriate density correction factor setting. Very slow flow can be the cause. Make the flow faster by using smaller bore detector to prevent air or substance from remaining in the detector. If this does not solve the problem, resort to vertical piping. Large quantity of bubbles are contained in the fluid. Find out where the air is brought in, and make necessary adjustments. Keep mixer vanes under water. Position the pump inlet low enough. Keep fluid pressure high (0.1MPa or more is recommended). Large quantity of bubbles are contained in the fluid. Measured density varies widely and does not agree with manual analysis value. Suitable location varies depending on density. Output is either unstable or unsuitable. Calibrate span as described in section 6.5. Air accumulates and keep staying inside the detector. Or substance being measured is sediment. Too much difference between measured density and manual analysis value Remedy The tank or the piping system (where the density meter is installed) is not flowing filled with substance to be measured. Or bubbles stay in the tank or the piping system (where the density meter is installed). Remedy the locations containing air bubbles. An example is to position the blade of the agitator in the tank below the fluid level. Another example is to position the inlet port of the pump sufficiently below the fluid level. Take necessary steps to make the fluid pressure high (0.1MPa or more is recommended). It is desirable to install the meter on the discharge port of the pump. At the same time, make sure that the meter is placed as far as possible (closer to the pump) from the pipe outlet for air release. Keep the tube always filled up with fluid by closing the downstream valve slightly or add a relief valve. Installing the density meter on the outlet side of the pump can help eliminate the cause of those troubles. Vertical piping is recommended for filling the pipe. Zero point is off. Calibrate zero point as described in Section 6. 4, then calibrate span described in Section 6.5 The electric conductivity of the measured matter is too high. Check if the electric conductivity is within the specified range. If the electric conductivity is beyond the range, send its measurement results and selfdiagnosis data to our Service Department. Converter failure Send self-diagnosis data to our Service Department. 71 6 F 8 A 0 7 8 7 8.2 Error Indications and Recovery Operations If an error occurs to the density meter, the error indicator [ALARM] will light up and a contact signal (OFF) will be output. Check the self-diagnosis data for any faulty values in accordance with the following steps. (1) Monitor menu display (see Subsection 5.2.4) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "1" of "1: MONITORING MENU" and then press the [SET] key. (The cursor of the initial state is located on "1".) (2) Switching to the self-diagnosis menu (see Subsection 5.2.7) In the monitoring menu, use the [→] key to move the cursor of the LCD indicator to the menu number "3" of "3: SELF-DIAGNOSIS" and then press the [SET] key. (3) Checking the self-diagnosis data (see Subsection 5.2.9) Press the [UP] key to move from one self-diagnosis data to another to check for any error. ◆ To detect which numerical range is an error value, please refer to Table 8.2. (4) Terminating the self-diagnosis After checking, press the [ESC] key twice to return to the initial menu display. If an error value is found, turn off all the power switches of the converter and then turn them back on. The self-diagnosis is executed all over again by the powering-ON. If an error is displayed again as a result of the self-diagnosis, send the relevant item to our Service Department. 72 6 F 8 A 0 7 8 7 Table 8.2 Self-diagnosis data Data Item Data Status Symbol Item name Data (Numeric value range; normal data range, status) ST Status [STATUS] Normal [GOOD] Warning [WARNING.] Whether the phase measurement operation is normally functioning or not can be verified. SL Microwave received signal level [MICROWAVE SIG. LVL] Without error judgment based on data numeric Usual range: -90 to -40 (dBm) Microwave coef. [MICROWAVE COEF.] Without error judgment based on data numeric • Normal range: 1825 to 1975 Data concerning microwave phase measurement [RF DATA] Without error judgment based on data numeric • Normal range + 10.0 to + 80.0 +5 V voltage [+5V POWER SUPPLY] Without error judgment based on data numeric • Normal range 4.5 to 5.5 (V) pd Reference phase error [REF PHASE] Without error judgment based on data numeric • Normal range - 9.9 to + 9.9 (degrees) Memory check [MEMORY CHECK] • Norma1 • Abnormal EPROM, RAM, EEPROM are checked [GOOD] [N.G.] 73 6 F 8 A 0 7 8 7 9 CORRECTIONS IN DENSITY CALCULATION This density meter, which operates on the basis of phase difference measurement by microwaves makes automatic corrections to the measured phase angel for the fluid temperature and phase angel rotation before making the density calculations for the measured substance. This chapter describes the methods for corrections and the density calculations. 9.1 Density Calculation This density meter measures the phase lag θ1 in the density zero water (zero water), which is the basis, and the phase lag θ 2 in the measured matter, the difference △θ(= θ 2 - θ 1) of which being proportional to the density is used to obtain the density. The density (X) of the measured matter is calculated in accordance with the following equation. X = C ×( a × △θ )+ b where : Measured density value (%TS) △θ : Phase difference. △θ = θ2−θ1 (degrees) : Density line slope; : Density intercept; : Density multiplier (Density correction factor.) 74 6 F 8 A 0 7 8 7 9.2 Various Kinds of Corrections 9.2.1 Phase angle rotation correction The phase is available only from 0 degree to 360 degrees. If the phase incrementally reaches 360 degrees, it returns to 0 degree, from which it keeps incrementing again. If the phase decreasingly reaches 0 degrees, it returns to 360 degrees, from which it keeps decreasing again. Accordingly, the concept of phase angle rotation is incorporated into this density meter and some corrections have been made so to allow the phase to change to an unlimited extent. In such a manner, this density meter has overcome the limit that the phase is available only from 0 to 360 degrees, thus realizing high density measurement. Phase angle rotation correction refers to obtaining the real phase angle θ2 by judging the number of rotations the dummy angle θ2' belongs to based on the measured values coming before and after. θ2 = θ2' + N x 360 (degrees) N: Number of rotations Set N=0 at the time of zero calibration, making the number of rotations to zero for the phase angle θ1 at zero point. If the θ2' exceeds 360 degrees to enter into the next rotation, set N=1. If it again exceeds 360 degrees to enter into the rotation after the next rotation, set N=2. (N will move up to 2 only if the meter is of large diameter and the density is high.) On the other hand, if θ2' goes below zero (0) degree to enter into the previous rotation, decrease N by one (1). In other words, when it goes into the -1st rotation from the 0th one, set N=−1; and when into the 0th rotation from the 1st one, set N=0. Note: The description above is the basics regarding the phase angle rotation correction. Normally, it is all right to use the density meter without being aware of this correction. However, in the event of measuring high density, etc., special setups and actions may be needed. For details, refer to Section 9.3. 9.2.2 Liquid temperature correction The phase tends to change in a straight line with regard to the liquid temperature. In this connection, liquid temperature correction is performed on θ2 as follows to obtain the phase difference △θ △θ={θ2−α(Τ−Τ0)}− θ1 △θ : Phase difference [degrees] θ2 : Actual phase angle of measurement object liquid [degrees] θ1 : Phase during zero water measurement (degrees) (Measured during zero calibration, and set in advance as a constant) α : Liquid temperature correction factor (degrees/°C) : Temperature of measurement object liquid (°C) T0 : Liquid temperature during zero calibration (°C) (Measured during zero calibration, and set in advance as a constant) 75 6 F 8 A 0 7 8 7 9.2.3 RF correction In addition to the liquid temperature correction, the density meter is equipped with the RF correction function in accordance with the features of the converter. The correction is performed on θ2 as follows to obtain the phase difference △θ. △θ={θ2−α(Τ−Τ0)−δ(G−G0)}−θ1 △θ : Phase difference [degrees] θ2 : Actual phase angle of measurement object liquid [degrees] θ1 : Phase during zero water measurement (degrees) (Measured during zero point calibration, and set in advance as a constant) α : Liquid temperature correction factor (degrees/°C) : Temperature of measurement object liquid (°C) T0 : Liquid temperature during zero calibration (°C) (Measured during zero calibration, and set in advance as a constant) δ : RF correction factor G : RF data during measurement G0 : Zero point RF data (Measured during zero point calibration, and set in advance as a constant) 9.2.4 Atmospheric temperature correction In addition to the liquid temperature correction and the RF correction, the density meter is equipped with the atmospheric temperature correction function in accordance with the features of the converter. The correction is performed on θ2 as follows to obtain the phase difference △θ. Atmospheric temperature correction function is an option item, therefore, make sure to set the atmospheric temperature correction factor β to “0.00”. △θ={θ2−α(Τ−Τ0)−δ(G−G0)−β(A−A0)}−θ1 △θ : Phase difference [degrees] θ2 : Actual phase angle of measurement object liquid [degrees] θ1 : Phase during zero water measurement (degrees) (Measured during zero point calibration, and set in advance as a constant) α : Liquid correction factor (degrees/°C) Τ : Temperature of measurement object liquid (°C) Τ0 : Liquid temperature during zero adjustment (°C) (Measured during zero point calibration, and set in advance as a constant) δ : RF correction factor G : RF data during measurement G0 : Zero point RF data (Measured during zero point calibration, and set in advance as a constant) β : Atmospheric temperature correction factor (degrees/°C) : Atmospheric temperature of measurement object liquid (°C) A0 : Atmospheric temperature during zero adjustment (°C) (Measured during zero point calibration, and set in advance as a constant) 76 6 F 8 A 0 7 8 7 9.3 Phase Angle Rotation Correction (Details) This section describes the special setups and actions required for cases of measuring high density. In normal measurement, it is unnecessary to be aware of the phase angle rotation correction, which is performed automatically. 9.3.1 Care point concerning phase angle rotation As described in 9.2.1, the number of phase angle rotations N is incremented or decreased judging from the values before and after the measured value. Such a processing requires the condition that the measured phase value varies continuously in accordance with the density of the measured matter. If the tank or the piping system (where the density meter is installed) is empty, however, the continuity of measured phase values is damaged thus making a normal phase angle rotation correction impossible, which in turn may cause the number of phase angle rotations to jump to a faulty value. If the number of phase angle rotations N is inappropriate, the density calculation result will also turn out to be erroneous. Once such a trouble occurs, it is necessary to reset the number of phase angle rotations N to an appropriate value through manual input. 9.3.2 Phase angle rotation in external synchronized operation The trouble previously described will be solved by performing the "external synchronized operation" incorporated into this density meter. In the external synchronized operation, if the contact signal is switched OFF synchronized with the pump shutdown, not only the output is switched to the simulated one but also the immediately preceding value is kept as the number of phase angle rotations N. 9.3.3 Outline of automatic adjustment function of phase angle rotations Furthermore, this density meter is equipped with the function of "automatic adjustment of phase angle rotations." This function judges whether the measured density calculated with the number of phase angle rotations N is proper or not in terms of the set density measurement range, etc. and then adjusts the number of phase angle rotations either incrementally or decreasingly if necessary. Even when the tank or the piping system (where the density meter is installed) is temporarily made empty thus causing the number of phase angle rotations N to jump to an inappropriate value, this function is also used to fill up the density meter detector once again with the matter to be measured and automatically adjust the number of phase angle rotations N to an appropriate value, which in turn will render an appropriate value for the measured density. While the tank or the piping system (where the density meter is installed) is left empty, the measured phase value itself comes to have an indefinite value, which in turn will render the measured density indefinite. Therefore, if the tank or the piping system (where the density meter is installed) could be made empty, it is desirable to perform the external synchronized operation. 9.3.4 Judgment conditions and adjustments for automatic adjustment of phase angle rotations The judgment conditions and adjustments regarding the automatic adjustment of phase angle rotations and the measured density are listed in Table 9.3.1. 77 6 F 8 A 0 7 8 7 Table 9.3.1 Judgement Conditions and Adjustments for Automatic Adjustment of Phase Angle Rotations Measured Density Automatic Adjustment of Phase Angle Rotations N Xmin = Less than - 4(%TS) Incremented (N = N+1) - 4∼C×a×360(%TS) Unadjusted Xmax = More than C x a x 360 (%TS) Decreased (N = N-1) In Table 9.3.1 above, C: Density multiplier (Varies with the character of the measured matter.) a: Density slope (A constant determined by the meter size) Table 9.3.2 is shown when C = 1, 0.7 and 1.8 as examples of the value Xmax in which N is judged to be too large. To obtain the value, multiplied the value when C = 1 in Table 9.3.2 by C. Table 9.3.2 Xmax Value (%TS) 0.7 1.0 1.8 9.3.5 XMAX 21.17 30.24 54.43 Restrictions and invalidation in applying the automatic adjustment of phase angle rotations This function of automatic adjustment of phase angle rotations involves some application restrictions. For example, it cannot be applied to the case of measuring high density as follows. Upper density measurement range: 20%TS; and density multiplier: 0.7 As shown in Table 9.3.2, Xmax=21.17(%TS). Therefore, when the measured density exceeds 21.17(%TS), the adjustment of decreasing the number of phase angle rotations applies as shown in Table 9.3.1, thus making it impossible to measure the density in excess of 21.17(%TS). To solve the problems as shown in the example above, measurement is taken so that the function of automatic adjustment of phase angle rotations is automatically invalidated if the upper measured density range exceeds Xmax. Check the operating conditions to see if the function of automatic adjustment of phase angle rotations is applicable or not. [NOTE] In the cases where the automatic adjustment of phase angle rotations is not applicable, after the tank or the piping system (where the density meter is installed) is temporarily made empty, it is necessary to reset the phase angle rotation to an appropriate value through manual input. In the cases, it is more desirable to perform the external synchronized operation. 9.3.6 Invalidation by setting the automatic adjustment of phase angle rotations As mentioned in the previous subsection, the density meter is equipped with the function of automatically invalidating the function of automatic adjustment of phase angle rotations, based on the conditions for setting the upper density measurement range and the density multiplier. However, in the state of starting the operation, the upper density measurement range is determined but the density multiplier is not determined yet (determined in the span calibration described in Section 6.5), thus the operation is started with a provisional value (initial value: 1). Therefore, the function of automatic 78 6 F 8 A 0 7 8 7 adjustment of phase angle rotations, which is supposed to be invalidated, may not be invalidated, making it impossible to take an appropriate measurement (including the span calibration). This applies to the case in which the original density multiplier is smaller than the current set value (the initial value 1 in the initial operation). There are two ways of dealing with such a case. One is to automatically invalidate the function of automatic adjustment of phase angle rotations by provisionally setting a sufficiently small value such as about 0.5 for the density multiplier C so that Xmax is smaller than the upper density measurement range. Another is to forcibly invalidate the function of automatic adjustment of phase angle rotations. The latter's setting method is described below. (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid." Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Selecting the "OTHERS" setting menu (see Subsection 5.2.5) Initially, the menu list of menu numbers 5 to 8 is displayed. However, by pressing the [UP] key once, this display can be switched to the menu list of the next menu numbers 9 to 11. Use the [→] key to move the LCD indicator cursor to the menu number "11" of "11: OTHERS" and then press the [SET] key to select the menu of "11: OTHERS." (3) Verifying or changing ON/OFF of automatic adjustment of phase angle rotations (See Subsection 5.2.16) Press the [DN] key once (or the [UP] key five times) to display "NA: N AUTO ADJUSTMENT". On this screen, it is possible to verify whether the automatic adjustment of phase angle rotations is valid (ON) or invalid (OFF). Here, if it is necessary to alter the setting, press the [SET] key to switch to the setup display of the automatic adjustment of phase angle rotations. Each time the [UP] or [DN] key is pressed, the set value is alternated between ON and OFF. Set the value to OFF and then press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. (4) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. 9.3.7 Actions after invalidating the automatic adjustment of phase angle rotations After invalidating the automatic adjustment of phase angle rotations to make it possible to take measurements appropriately even at high density in excess of Xmax, implement the span calibration in accordance with Section 6.5 and set the density multiplier to an appropriate value. While referring to Table 9.3.2, use this reset density multiplier to calculate the maximum density Xmax, which can be applied to the function of automatic adjustment of phase angle rotations and judge whether this Xmax is greater than the value of the upper density measurement range that is set. 79 6 F 8 A 0 7 8 7 If Xmax is greater than the upper density measurement range, the function of automatic adjustment of phase angle rotations is applicable. Therefore, return the function of automatic adjustment of phase angle rotations which is set to "OFF" in Subsection 9.3.6 to“ON”. If Xmax is smaller than the upper density measurement range, the function of automatic adjustment of phase angle rotations is invalid. Therefore, it is unnecessary to return the function of automatic adjustment of phase angle rotations which is set to "OFF" in Subsection 9.3.6 to “ON”. 9.3.8 Return to the normal through manual input of the phase angle rotations If the function of automatic adjustment of phase angle rotations is not applicable whereas the piping system (where the density meter is installed) is temporarily made empty thus causing the number of phase angle rotations to jump to a faulty number, the number of phase angle rotations fails to return to an appropriate value even when the piping system (where the density meter is installed) is refilled with the matter to be measured, thus allowing the measured density to remain in error. In this connection, it is necessary to reset the phase angle rotation to an appropriate value through manual input. The setting method is described below. (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid." Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Selecting the "ANGLE ROTATION" setting menu (see Subsection 5.2.5) In the state that the menu list of menu numbers 5 to 8 is displayed, use the [→] key to move the LCD indicator cursor to the menu number "8" of "8: ANGLE ROTATION" and then press the [SET] key to select the menu of "8: ANGLE ROTATION". (3) Verifying or changing the number of phase angle rotations (see Subsection 5.2.13) Press the [DN] key once (or the [UP] key twice) to display "N: ROTATION". On this screen, it is possible to verify the number of phase angle rotations. Here, press the [SET] key to switch to the setup display of the number of phase angle rotations and enter an appropriate value (note). At the initial digit, use the [UP] or [DN] key to select whether to attach the "-" symbol or not. Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. Note: In many cases, an appropriate value for the number of phase angle rotations N is 0. In the event that the density or the fluid temperature is high, this value may be 1. In the event that the density or the fluid temperature is low, it may be -1. Set either of 0, 1 and -1 and then verify that the measured density at this time has returned to an appropriate value. (4) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. 80 6 F 8 A 0 7 8 7 10 VARIOUS FUNCTIONS 10.1 Various Functions and their Outlines The Insertion Type Density Meter LQ300A00****** is equipped with various functions to be used more appropriately in various processes and in various situations. Depending on the process being applied or the method of using the meter, some functions may not be necessary. Based on the descriptions below, choose the functions you need. Table 10.1.1 describes the functions equipped in this meter and outlines. Table 10.1.1 Various Functions Function Name 1) External synchronized operation 2) Moving average 3) Change-rate limit 4) Electric conductivity correction 5) Additives correction 6) Linearizer 7) Density multiplier switching by external signal Application and Outline Perform this external synchronized operation in the event that the pump to the tank or the piping system on which the density meter is installed is operated intermittently and the object of measurement does not flow continuously or in the event that the tank or the piping system (where the density meter is installed) is temporarily made empty. Use this function in the event of requiring the averaged output to be used for density control, etc. The function is useful for suppressing the deflection width of the output. In the event of a sudden change in the density or a sudden variation in the output due to intrusion by bubbles, etc., this function is used to exclude these signals to restrain the sudden output change. This function is used in the event that the electric conductivity of the matter to be measured has changed substantially. Since this does not usually become a real problem, it does not need this function usually. When using this function, however, it is necessary to separately prepare a electric conductivity meter, install it on a proper location and input the electric conductivity signal into the density meter. In the event that the brand (with varying components and compound ratio) of the matter to be measured is switched from one to another, this function is used to omit the span calibration in terms of each brand by registering beforehand the list in which the sensitivity and compound ratio of the respective components are input (up to ten lists can be registered) and then selecting the list number. Since the density meter has a satisfactory linear relationship between its actual density and instrument output, a linearization correction is normally unnecessary. Therefore, this function is provided as a measure to deal with special cases. This function is to switch around up to four density multipliers by means of ON/OFF of two external voltage signals(DI). The function can be used to facilitate the density measurement of up to four different types of matters (brand) which differ in measurement sensitivity. 81 Remarks Refer to Section 6.7. See Section 10.2. See Section 10.3 See Section 10.4. See Section 10.5. See Section 10.6. See Section 10.7. 6 F 8 A 0 7 8 7 10.2 Moving Average 10.2.1 Function of moving average Assuming that the moving average times is "n", this function is to calculate and output the mean value of n preceding measured values each time. The function is used when an averaged output is required such as for density control. This function is also useful for suppressing the deflection width of output. The value that can be set as the moving average times "n" is 1 to 99. Setting 1 for "n" means that no moving average takes place. 10.2.2 Setting of the moving average times (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid." Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Selecting the parameter setting menu (see Subsection 5.2.10) In the state that the menu list of menu numbers 5 to 8 is displayed, use the [→] key to move the LCD indicator cursor to the menu number "5" of "5: SET PARAMETERS" and then press the [SET] key to select the menu of "5: SET PARAMETERS." (3) Verifying or setting the moving average times (see Subsection 5.2.10) Press the [DN] key three times (or the [UP] key eleven times) to display "ma: AVERAGING TIMES". On this screen, it is possible to verify the set value of the moving average times. If it is necessary to change the setting, press the [SET] key here to switch to the setup display of the moving average times and enter an appropriate value. Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. (4) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. 10.2.3 Cautions in using the moving average function Setting an excessively large value for the moving average times will result in deteriorated responsiveness. Therefore, make sure to set a value appropriate to the process situation and the required responsiveness. 82 6 F 8 A 0 7 8 7 10.3 Change-rata limit 10.3.1 Outline of change-rate limit function In the event of a sudden change in the density or a sudden variation in the output due to intrusion by bubbles, etc., this function is used to exclude these signals to restrain the sudden output change. By setting two measurement conditions of permissible variation width and limit times, the conditions for change-rate limit are set. It is possible to set 0.00 to 9.99(%TS) as the permissible variation width and 0 to 99 times as the limit times. Setting the limit times to zero means that no change-rate limit is imposed. 10.3.2 Examples of operating the change-rate limit function The change-rate limit function is described with examples below. The setting conditions shall be as follows. • Width of change-rate limit function: 0.5%TS • Times of change-rate limit function: Twice The conditions that are set as above mean the following. 1) All the variations within 0.5%TS are permitted and output without modification. 2) Variations exceeding 0.5%TS are limited up to twice, outputting the immediately preceding signal in place of the relevant signals. 3) Variations in excess of 0.5%TS which continue three times are judged to be signal variations resulting from actual density variations, thus outputting the 3rd signal without modification. Density signal (%TS) Example 1: Operation for temporary and sudden signal variation Density signal (%TS) 3.0 2.5 2.0 1.5 1.0 0.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 0.0 Signal No.. 10 Signal No.. Fig.10.3.2 Output Signal After Variation Factor Restriction Fig.10.3.1 Original Signal 83 10 6 F 8 A 0 7 8 7 Fig.10.3.1 shows the original signal before the change-rate limit is processed. No.1 to No.4 are varying within a small width; however, only signals No.5 and No.6 are varying in excess of 0.5%TS deviation from the immediately preceding signal No.4. No.7 to No.10 are back to a small width of variation. In the event that the above-set change-rate limit is applied to such signals, the output signals are as shown in Fig.10.3.2. Since signals No.5 and No.6 are varying in excess of 0.5%TS with regard to signal No.4, signal No.4 is output instead with regard to No.5 and No.6. Signal No.7 is output without modification. Signals No.8 to No.10, which are also within the variation width of 0.5%TS with regard to the respective immediately preceding signals, are output without modification. Example 2: Signal change in the shape of steps Density signal (%TS) Density signal (%TS) 3.0 2.5 2.0 1.5 1.0 0.5 0.0 3.0 2.5 2.0 1.5 1.0 0.5 0.0 10 Signal No. Signal No. 10 Fig.10.3.4 Output Signal After Variation Factor Restriction Fig.10.3.3 Original Signal Fig.10.3.3 shows the original signal before the change-rate limit is processed. The numeric values along the horizontal axis refer to the signal numbers. No.1 to No.4 are varying within a small width; however, signal No.5 is varying in excess of 0.5%TS with No.6 to No.10 remaining in a state not very different from No.5. In the event that the above-set change-rate limit is applied to such signals, the output signals are as shown in Fig.10.3.4. Since signals No.5 and No.6 are varying in excess of 0.5%TS with regard to signal No.4, signal No.4 is output instead with regard to No.5 and No.6. Signals No.7 to No.10, which are within the variation width of 0.5%TS with regard to the respective immediately preceding signals, are output without modification. 10.3.3 Cautions in using the change-rate limit factor (1) Setting the change-rate limit width The value can be set within the range of 0.00%TS to 9.99%TS. If the width is set to as little a value as the normally indicated deflection width, restricted signals will increase and indications will vary in the shape of steps. Therefore, set a sufficiently large value so that the variation width is reliably judged to be in error. (2) Setting the times of change-rate limit Signals that are made faulty due to intrusion of large bubbles, etc. may affect two neighboring signals in relation to measurement timing. Therefore, although the change-rate limit has an effect even when it is applied only once, it is desirable to set the times of change-rate limit at least to two times in order to reliably exclude error signals. In the event of density variations in the shape of 84 6 F 8 A 0 7 8 7 steps as shown in Example 2, a delay increases in accordance with the set times. Set an appropriate value for the times in accordance with the responsiveness required of the plant. 10.3.4 Setting the change-rate limit (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid". Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Selecting the parameter setting menu (see Subsection 5.2.5) In the state that the menu list of menu numbers 5 to 8 is displayed, use the [→] key to move the LCD indicator cursor to the menu number "5" of "5: SET PARAMETERS" and then press the [SET] key to select the menu of "5: SET PARAMETERS". (3) Verifying or changing the change-rate limit width (see Subsection 5.2.10) Press the [DN] key two times (or the [UP] key twelve times) to display "dx: CHANGE RATE LIMIT". On this screen, it is possible to verify the set value of the change-rate limit width. If it is necessary to change the setting, press the [SET] key here to switch to the setup display of the change-rate limit width and enter an appropriate value for the width. Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. (4) Verifying or changing the times of change-rate limit (see Subsection 5.2.10) Continuing on from the operation in (3) above, press the [UP] key once to display "HL: LIMIT TIMES". On this screen, it is possible to verify the set value of the change-rate limit times. If it is necessary to change the setting, press the [SET] key here to switch to the setup display of the change-rate limit times and enter an appropriate value for the times. Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. Note: If the times of change-rate limit is set to zero, the change-rate limit function is made inactive. (5) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. 85 6 F 8 A 0 7 8 7 10.4 Electric Conductivity Correction 10.4.1 Standard conductivity correction factor The indication of the density meter varies with the conductivity of the measured object fluid; however, the variance is as small as approx. 0.15%TS to 1mS/cm change in conductivity and usually practically negligible, thus making it unnecessary to input the conductivity meter signal to perform electric conductivity correction. In the event that the conductivity change is large and thus its impact is not ignoble, make sure to use the electric conductivity correction function. The formula for this correction including the other corrections described in Chapter 9 is as follows. △θ={θ2 -α(Τ-Τ0)-δ(G-G0)-γ(E-E0) - β(A - A0)} -θ1 △θ : Phase difference (degrees) θ2 : Actual phase angle of measured object liquid (degrees) θ1 : Phase during zero water measurement (degrees) (Measured during zero calibration, and set in advance as a constant) α : Liquid temperature correction factor (degrees/°C) Τ : Liquid temperature of measured object liquid (°C) Τ0 : Liquid temperature during zero calibration (Measured during zero calibration, and set in advance as a constant) δ : RF correction factor G : RF data during measurement G0 : Zero point RF data (Measured during zero calibration, and set in advance as a constant) γ : Electric conductivity correction factor (degrees/(mS/cm)) : Electric conductivity of measured object liquid (mS/cm) E0 : Zero water conductivity (mS/cm) β : Atmospheric temperature correction factor (degrees/°C) : Atmospheric temperature of measured object liquid (°C) A0 : Atmospheric temperature during zero calibration (Measured during zero calibration, and set in advance as a constant) At the time of factory shipment, the [electric conductivity correction factor γ] is set to zero for all the products. If the conductivity change of the measured object fluid is large, input the electric conductivity signal in accordance with "Fig.3.5 External Connection Diagram" and then reset the [electric conductivity correction factor γ]. Table 10.4.1 shows the "standard values" of electric conductivity correction factors as well as the "density line slope (a)" required in the event of obtaining electric conductivity correction factors through calculation from measured values. The "standard values" shall be applicable when the range of the electric conductivity meter used for conductivity correction is 0 to 10 mS/cm. 86 6 F 8 A 0 7 8 7 Table 10.4.1 Standard Values of Electric Conductivity Correction Factor (γ) (Based on Electric Conductivity Meter with a Range of 0 to 10 mS/cm) and Slope of the Line (a) Item (a) γ (Standard Value) Multiplier 0.084 1.8 In the event of performing a electric conductivity correction on this density meter, it is a basic principle to externally connect and use a conductivity meter with a range of 0 to 10 mS/cm. In the event of using a conductivity meter of another range (0 - R mS/cm), obtain the conductivity correction factor in accordance with the following formula. γ=(R/10)×γ0 γ0 : Standard value of electric conductivity correction factor (see Table 9.1) R : Upper range of conductivity meter used For example, if the insertion type density meter, the standard value of the electric conductivity correction factor of the density meter is 2.7 and a conductivity meter with a range of 0 to 5 mS/cm is connected to this, γ=(R/10)×γ0 =(5×10)×1.8 =0.9 is used as the correction factor. [NOTE] ◆ In the event of implementing a electric conductivity correction, separately prepare a electric conductivity meter and install it on a location where the conductivity can be measured correctly (where the measurement object process is appropriate). ◆ The "standard values" of electric conductivity correction factors shown in Table 10.4.1 are criteria. It is necessary to use the linear relationship that exists between the conductivity and the output to survey and determine the electric conductivity correction factor in terms of each actual measured object fluid. See Subsection 10.4.2. ◆ In the event of not executing any electric conductivity correction, set the "electric conductivity correction factor (γ)" to zero. 10.4.2 How to obtain and set a correction factor Obtain and set a electric conductivity correction factor as appropriate to the applicable process in accordance with the following procedure. (1) To set the density multiplier to 1.000 (1-1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2: SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid." Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. 87 6 F 8 A 0 7 8 7 (1-2) Selecting the span calibration menu (see Subsection 5.2.5) The menu list of menu numbers 5 to 8 is displayed. Use the [→] key to move the LCD indicator cursor to the menu number "7" of "7: SPAN CALIBRATION" and then press the [SET] key to select the menu of "7: SPAN CALIBRATION." (1-3) Verifying or recording the density multiplier (see Subsection 5.2.12) For example, the set value of the current density multiplier C' is displayed as in "DATA: 1.265". Record this value. (1-4) Setting the density multiplier to "1.000" (see Subsection 5.2.12) Press the [SET] key to switch to the setup display of the density multiplier and reset the density multiplier to 1.000. Use the [→] key to move to the digit, and use the [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. (2) To suspend the electric conductivity correction function (with the conductivity correction factor set to 0.00) (2-1) Returning to the initial screen of the setting mode Continuing on from (1-4) above, press the [ESC] key once to return to the menu list display of the menu numbers 5 to 8 of the setting mode. (2-2) Selecting the linearizer /conductivity menu (see Subsection 5.2.5) Press the [UP] key once to switch to the menu list display of the next menu numbers 9 to 11. Use the [→] key to move the cursor of the LCD indicator to the menu number "9" of "9: LINEARIZ/CNDUCTVTY" and then press the [SET] key to select the menu of "9: LINEARIZ/CNDUCTVTY". (2-3) Setting the electric conductivity correction factor to 0.00 (see Subsection 5.2.14) Press the [UP] key five times (or the [DN] key three times) to display "r: CNDUCTVTY COEF". Press the [SET] key here to switch to the setup display of the electric conductivity correction factor and then input 0.00 for the electric conductivity correction factor. Use the [→] key to move to the digit, and use the [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. (3) To measure the electric conductivity of the measured object fluid (3-1) Selecting the monitoring menu (see Subsection 5.2.4) Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. Use the [→] key to move the cursor to the menu number "1" of the LCD indicator's "1: MONITORING MENU" and then press the [SET] key to select "1: MONITORING MENU". (3-2) Selecting the measured value data display menu (see Subsection 5.2.4) In the monitoring menu list of the menu numbers 1 to 3, use the [→] key to move the cursor to the menu number "2" of the LCD indicator's "2: MEASURED VALUES" and then press the [SET] key to select "2: MEASURED VALUES". 88 6 F 8 A 0 7 8 7 (3-3) Reading and recording measured conductivity and density values The externally installed conductivity meter is used to measure the conductivity (E1) of the measured object fluid while, at the same time, reading the measured density (M1) from the LCD indicator or from the LED display outside the converter. Take notes of each measured value. Next, while varying the conductivity of the measured object fluid, measure as well as take notes of the conductivity (E2) and the measured density (M2). At this time, take care to prevent the actual density of the measured object fluid from changing. E1,E2 : Conductivity (mS/cm) M1,M2: Measured density value (%TS) (4) To calculate the electric conductivity correction factor Obtain the electric conductivity correction factor (γ) in accordance with the following arithmetic expression. γ=ΔM/(a×ΔE) : Density line slope (see Table 9.1: varies with the aperture) ΔM : Measured density value difference (M2 – M1) ΔE : :Measured conductivity value difference (E2 – E1) For example, if the meter size is 150 mm, it follows that a = 0.056. At this time, let's assume that the conductivity and the measured density (specified value) are as follows respectively. 1st measurement: E1=1 mS/cm M1=4.0%TS 2nd measurement: E2=2 mS/cm M2=4.2%TS From here, it follows that ΔE =1 mS/cm ΔM=0.2 %TS and the conductivity correction factor is γ = 0.2/(0.056×1) = 3.57 (5) To correct the electric conductivity correction factor by means of the conductivity meter's range In the event that the range of the conductivity meter being used is other than "0 to 10 mS/cm", correct the conductivity correction factor in accordance with the conductivity meter range while referring to the method of calculating the correction factor in the event that the conductivity meter range is other than the standard described in Subsection 10.4.1. (6) To set the electric conductivity correction factor In the same manner as the operation described in (2), set the electric conductivity correction factor to the value calculated in (4) and (5). (7) To return the density multiplier to its original value In the same manner as the operation described in (1), return the density multiplier to its original value which has been previously recorded. (8) To return to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement 89 6 F 8 A 0 7 8 7 10.5 Additives Correction Factor 10.5.1 Additive Correction Function This function refers to handling the different brand of the pulp which contains various additives. If the physical property of the measured object fluid varies, it is necessary to set the density multiplier for a value appropriate to this difference. Even with multiple types of measured objects mixed together (mixed fluid), if their compound ratio is regarded to be consistent, it is possible to measure the density of the entirety or the density of a particular type among them. In measuring the density of such mixed fluid, each time the physical property and compound ratio of the objects included in the fluid differ (that is, the brand is different), it is necessary to set the density multiplier in accordance with the brand of the relevant mixed fluid. By selecting an applicable brand number from about ten brands registered in advance, this additive correction function calculates the density in accordance with the brand, thus making it possible to omit the span calibration in terms of each brand. Using this function in a simplified manner, by selecting the span calibration factor(density multiplier) in terms of each brand from the brand list registered in advance, it is possible to simplify the span calibration. For information on the simplified way of this function, refer to "10.5.5 Simplified way of using the additive correction function". ● The contents to be registered into the brand list are as follows. Table 10.5.1 Brand List Component Note 1 Comp. 0 (pulp) Comp.1 Comp.2 Comp.3 Comp.4 Comp.5 Sign s0 s1 s2 s3 s4 s5 Sensitivity (Note 2) Setting range Set at shipping -9.99 to +9.99 1.00 -9.99 to +9.99 0.00 -9.99 to +9.99 0.00 -9.99 to +9.99 0.00 -9.99 to +9.99 0.00 -9.99 to +9.99 0.00 Sign -R1 R2 R3 R4 R5 Ratio of mixture (Note 3) Setting range Set at shipping ---0.000 to 1.999 0.000 0.000 to 1.999 0.000 0.000 to 1.999 0.000 0.000 to 1.999 0.000 0.000 to 1.999 0.000 (Note 1) Component 0 is the main component pulp. Components 1 to 5 are the additives #1 to #5. (Note 2) Sensitivities for components #0 to #5 are to be registered for each formula of the 10 brand list. Usually, the sensitivity, s0 for pulp, is set to 1.000. The sensitivities for typical additives are listed in table 10.5.2. For other additives, please contact Toshiba, we measure the sensitivity when you provide us with a sample of an additive. A sensitivity is measured in the same procedures for the off-line span calibration for an additive, from (measured density reading/density by manual analysis). Table 10.5.2 Additives Calcium carbonate Titanium oxide Zinc oxide Talc Sensitivities 0.45 0.13 0.12 0.61 Note 3: For each formula in the list of 10 brand, the ratio of mixture for the components #1 to 5 is to be entered. A ratio of mixture is a ratio of a component against the pulp (component 0) in weight. 90 6 F 8 A 0 7 8 7 10.5.2 Density calculation Following calculation modes can be selected. (1) Additives correction ON (To be made) / OFF (Not to be made) (a) Set value at shipping the density meter: OFF (2) When additives correction is "ON" (to be made), you can select two calculation modes. (b) Total density of mixture including the additives (TOTAL) (c) Density of pulp only (MAIN) In the mode (2) above, each of the density outputs (LED display of the converter, and the current output in 4 to 20mA dc) can be either (b) or (c) separately. * Set value at shipping: Both the density display and the density current output are in "TOTAL" of (b) above. (a) Density without additives correction Following calculation is made (same density calculation as in section 9.1.3) Xa = C × (a × Δθ) +b where, Xa : Measured density value Δθ : Phase difference that varies in proportion to the actual density : Density line slope : Density intercept (normally zero). : Density multiplier (b) Additives correction to be made for getting Total Density of whole mixture including the additives (TOTAL) Xb = 1 + R1 + R2 + R3 + R4 + R5 × C × (a × Δθ ) + b s0 + s1 ⋅ R1 + s2 ⋅ R2 + s3 ⋅ R3 + s4 ⋅ R4 + s5 ⋅ R5 where, Xb s0 s1 s2 s3 s4 s5 Δθ : Density of the whole mixture : Sensitivity of pulp only : Sensitivity of additive #1, R1 : Mixture ratio of additive #1 : Sensitivity of additive #2, R2 : Mixture ratio of additive #2 : Sensitivity of additive #3, R3 : Mixture ratio of additive #3 : Sensitivity of additive #4, R4 : Mixture ratio of additive #4 : Sensitivity of additive #5, R5 : Mixture ratio of additive #5 : Phase difference that varies in proportion to the diameter : Density line slope determined by diameter : Intercept of the line (normally zero). : Density multiplier (c) Additives correction to be made for getting Pulp Only Density (MAIN) Xc = × C × ( a × ∆θ ) + b s0 + s1 ⋅ R1 + s2 ⋅ R 2 + s3 ⋅ R 3 + s4 ⋅ R 4 + s5 ⋅ R5 where, Xc : Density of Pulp Only Others are same as in (b) 91 6 F 8 A 0 7 8 7 (Note) When using the additives correction functions of (b) or (c), set the density multiplier C to 1.000. Following procedure is recommended for making span adjustment. At the beginning of the use of correction, for a whole mixture of a formula, compare the measured density readings you get in dry method (dry weight) and in manual analysis, and when required, make span adjustment by adjusting the density multiplier C of the whole mixture. 10.5.3 Procedures for using the additives correction function The procedure for the additives correction function is described as following steps. Obtain sensitivities of the components Refer to table 10.5.2 Select the formula list number for registering (parameters) Set sensitivities of pulp and additives (s0 to s5) You can set for up to ten formulas. Each of which can have up to five additives, to which sensitivities and ratios can be entered individually. Set mixture ratios of additives (R1 to R5) Refer to [6.4 Zero Point Calibration] Perform zero point calibration Set the density multiplier to 1.000 Select ON for additives correction Select calculation mode for additives correction (TOTAL or MAIN) Select the brand list number that corresponds with the formula (Parameter set) Let the liquid mixture of selected brand flow. Read the density indication(M), and simultaneously sample the substance to measure. Measure the density (A) of the sample by manual analysis Calculate C as below, then fine adjust C (density multiplier) C=(A/M)×1 (Default value of C is 1) When brand is changed Start measuring Density 92 6 F 8 A 0 7 8 7 10.5.4 How to set the additives correction function (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid.". Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Selecting the additives correction menu (see Subsection 5.2.5) Initially, the menu list of the menu numbers 5 to 8 is displayed. Press the [UP] key once to switch to the menu list display of the next menu numbers 9 to 11. Use the [→] key to move the cursor of the LCD indicator to the menu number "10" of "10: ADDITIVES CORRECT" and then press the [SET] key to select the menu of "10: ADDITIVES CORRECT". (3) Verifying and changing the various settings for additives correction (see Subsection 5.2.15) (3-1) Selecting the OFF/ON of the additives correction function Verify the set value of the initial menu "AF: ADDITIVES COMP." of the additives correction. "OFF" means that the additives correction function is unavailable, thus not displaying the detailed menu concerning the additives correction. When using the additives correction function, press the [SET] key to switch to the OFF/ON selection display of the additives correction. Each time the [UP] or [DN] key is pressed, the set value alternates between "OFF" and "ON". With the value set to "ON", press the [SET] key to verify it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. (3-2) Selecting a density display (see subsection 10.5.2) Continuing on from (3-1), press the [UP] key to switch to the display of "Ad: DISPLAY DENSITY". In this menu, decide whether the density display should be the density of the entire mixed fluid including the additives "TOTAL" or the density of the pulp only "MAIN". When changing the setting, press the [SET] key to switch to the selected display, use the [UP] or [DN] key to switch between "TOTAL" and "MAIN" and then press the [SET] key at the status to be set. (3-3) Selecting a density display (see Subsection 10.5.2) Continuing on from (3-2), press the [UP] key to switch to the display of "Ac: OUTPUT DENSITY". In this menu, decide whether the density current output of 4 to 20mA should be the density of the entire mixed fluid including the additives (TOTAL) or the density of the pulp only (MAIN). When changing the setting, press the [SET] key to switch to the selected display, use the [UP] or [DN] key to switch between "TOTAL" and "MAIN" and then press the [SET] key at the status to be set. (3-4) Selecting a parameter set number (a brand list number) Continuing on from (3-3), press the [UP] key to switch to the display of "Ap: PARAMETER SET NO.". In this menu, select a parameter set number. Press the [SET] key to switch to the setup display and then input the parameter set number. Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. 93 6 F 8 A 0 7 8 7 (3-5) Setting the sensitivity and the compound ratio Continuing on from (3-4), press the [UP] key to switch to the menu of "s0: MAIN OBJ SENS." and then, after switching to the setup display by pressing the [SET] key, input the sensitivity of the main object (component 0). Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. Continue on to switch to the next setup menu display with the [UP] key. And, in accordance with the same procedure, set the sensitivities s0 to s5 of components (additives) 1 to 5 as well as compound ratios R1 to R5 of components (additives) 1 to 5. (4) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. 10.5.5 Simplified Correction on Additives Previous section describes complete correction on additives in which sensitivities and ratios of mixture per additive were taken into account in calculation. By using only a sensitivity for the whole mixture (a mixture of pulp and additives], the additives correction can be simplified as described below. In this simplified correction, a density multiplier (sensitivity) is obtained separately for each formula and entered into the list of formula. When a formula is changed, you need to select a new formula number to change the density mulyiplier to continue measuring density. Up to ten formulas can be entered into the list. Procedures for a simplified correction is as follows. See the section 10.5.1 to 10.5.3 for basic information, and refer to section 10.5.4 Operations for correction. ● Procedures for simplified correction of additives. Set the density multiplier C to 1.000 Select Calculation Mode for additives correction...No (correction) Perform zero calibration See “6.4 Zero calibration” Carry out span calibration for each brand, and obtain sensitivity as below. Sensitivity = (Measured density reading)/(Density obtained by manual analysis) Enter the sensitivity of a formula into the sensitivity s0 of the component 0 in the formula list. See Note 1 Select (TOTAL)(total density of a mixture, with additives correction] for the calculation mode Select a brand list number that corresponds with the mixture to be measured. Run the fluid to measure and measure density When the brand is changed. (Note1) Set all sensitivities and ratios to 0.00 and 0.000 respectively for all of the components 1 to 5. (Or to the default values set at shipping.) 94 6 F 8 A 0 7 8 7 10.6 LINEARIZER SETTING 10.6.1 Linearizer function The Insertion Type Density Meter has an excellent linear characteristic between the actual density and the measured value. Depending on the kind of substance to be measured, there may not be a linear relationship between the values measured by the meter and those obtained by manual analysis. Particularly, in the measurement of low density substance of about 1%, the meter tends to show readings in higher value at or less than 0.5% or show lower for the density about 1.5% or higher. In such a case, the 1inealization is necessary because it is difficult to match meter-measured values with manual analysis values with a single density multiplier over a wide range of densities from low to high. Suppose there is a curve relationship such as that shown in figure 10.6. 1 between meter-measured values (using a density multiplier of 1.00) and manual analysis values when a certain substance is measured at varying degrees of density. To make linealization, the curve is approximated by three straight lines of A, B, and C. 1.5 Manual ly analyzed density % 手 分 析 値 • • 1.2 • • • • • • • • • 濃 0.8 度 % • • • • • • • 0.6 1.0 1.5 Instrument reading X0 (density multiplier 1.00) 計器測定値 XO (濃度補正係数 1.00 ) Figure 10.6.1 Linearizer setting Diagram Let the meter-measured value (XO) at the bend of the lines A and B (crosspoint) as density A, and the value at lines B and C to be density B. Also let the slopes of lines A, B, and C as K1, K2, and K3 respectively. 95 6 F 8 A 0 7 8 7 Meter-measured value XO (density multiplier 1.00) before linearization and meter-measured value X after linearization have the following relationship. For X 0 ≦ A For A < X 0 ≦ B For B < X 0 where C: Density multiplier. X = C( K 1 X 0 ) X = C{ K 1 A + K 2( X 0 − A)} X = C{ K 1 A + K 2( B − A )+ K 3( X 0 − B )} The procedures for making 1inearizer lines and setting them into the meter are as follows: (1) Create a graph Plot the relationships between the meter-measured value (X0) at a density multiplier of 1.00 and manual analysis value to make into a graph as shown in figure 10. 1. (2) Draw approximate straight lines Draw in three straight lines that approximate the relationships. (3) Read densities at crosspoints Read the meter-measured values (XO) at the cross-points of these lines and get cross-point densities A and B. (4) Get the slopes of the lines. Calculate the slopes of the straight lines as follows to determine K1, K2, and K3. K1 = d / a K2 = e / b K3 = f / c ● Defaults are set as : A = 0.60, B = 1.00, K1 = 1.00, K2 = 1.00, K3 = 1.00 Example of set values (Fig. 10. l ) A = 0.6 (%), B = 1.0 (%) K 1 = 0.8 / 0.6 = 1.33, K 2 = 0.4 / 0.4 = 1.00, K 3 = 0.3 / 0.5 = 0.6 96 6 F 8 A 0 7 8 7 10.6.2 Linearizer setting (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid.". Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Selecting the linearizer menu (see Subsection 5.2.5) Initially, the menu list of the menu numbers 5 to 8 is displayed. Press the [UP] key to switch to the menu list display of the menu numbers 9 to 11. Use the [→] key to move the cursor of the LCD indicator to the menu number "9" of "9: LINEARIZ/CNDUCTVTY" and then press the [SET] key to select the menu of "9: LINEARIZ/CNDUCTVTY". (3) Setting the density and the factor (see Subsection 5.2.14) The setup menus of density and factor are called one after another from the start of the menu development of "9: LINEARIZ/CNDUCTVTY". First of all, press the [SET] key at "LA: DENSITY A" and then, after the setup display of density A is displayed, input the value for density A. Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. Continue on to switch to the next setup menu display with the [UP] key. And, in accordance with the same procedure, set density B and factors K1, K2 and K3. (4) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. (5) Determining and setting the density multiplier Perform the density measurement after setting the linearizer and, in accordance with the span calibration in Section 6.5, determine and set the density multiplier C. 97 6 F 8 A 0 7 8 7 10.7 Density Multiplier Switching by External Signals 10.7.1 Density multiplier switching function by external signals When switching around multiple measurement objects fulid of differing measurement sensitivities to measure their respective sensitivities, it is possible to take appropriate density measurements by resetting the density multiplier to a value in accordance with the relevant measured object fluid each time the measured object fluid is changed. In the event that the measurement objects fluid are limited to no more than four types, this function can be used to save the trouble of resetting the density multiplier each time through manual input. Implement the span calibration in terms of each measured object fluid in advance, obtain and set the respective density multipliers C1 to C4 and then switch around the density multipliers to be used for density calculation by means of the external voltage signals of two points in accordance with the measurement objects fluid being switched around. Table 10.7.1 shows the relationship between the statuses of external voltage signals and selected density correction factors. Table 10.7.1 Status of External Voltage Signal DI2 DI3 Selected Density Multiplier C1 (Same as the normally used density multiplier C) C2 C3 C4 H: Voltage signals of 20 to 30VDC L: Signals of no more than 2VDC 98 6 F 8 A 0 7 8 7 10.7.2 Setting the density multiplier switching by external signals (1) Switching to the setting mode (see Subsection 5.2.5) First of all, press the [ESC] key of the converter several times (normally once although this varies with the operation status) to return to the initial menu display. Next, use the [→] key to move the LCD indicator cursor to the menu number "2" of "2 SETTING MENU" and then press the [SET] key to display the warning message saying "Test output will be valid.". Make sure that there is no problem and then press [→] to get into the setting mode. To get into [2: SETTING MENU], it is necessary to further enter the password "8000". Then, the output will be switched to the simulated output that is set beforehand. (2) Selecting the "OTHERS" setting menus (see Subsection 5.2.5) Initially, the menu list of menu numbers 5 to 8 is displayed. However, by pressing the [UP] key, this display is switched to the menu list of the next menu numbers 9 to 11. Use the [→] key to move the LCD indicator cursor to the menu number "11" of "11: OTHERS" and then press the [SET] key to select the menu of "11: OTHERS." (3) Selecting of density multiplier switching ON/OFF(see Subsection 5.2.16) Press the [UP] key once to display "DI: C CHANGE ON/OFF". Press the [SET] key here to switch to the setup display. Each time the [UP] or [DN] key is pressed, the set value alternates between "ON" and "OFF". Therefore, when using the function of density multiplier switching by external signals, set the value to "ON" and then press the [SET] key to verify it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. (4) Setting density multipliers C2, C3 and C4 Continuing on from (3), press the [UP] key once to switch to the display of "C2: DensityMultiplier". Switch to the setup display by pressing the [SET] key here and then input the density multiplier C2. Use the [→] key to move to the digit, and use the [UP] or [DN] key to alter the numeric value of the relevant digit. When entering input is completed, press the [SET] key to confirm it. The screen will be returned to the immediately preceding one; make sure that the value is correctly reset. Continue on to switch to the next setup menu display with the [UP] key and set C3 and C4 in accordance with the same procedure. When setting the density multiplier C1, refer to "6.5 Span Calibration". (5) Returning to the measuring mode Press the [ESC] key twice to return to the initial menu screen and return to the measuring mode from the setting mode to resume the normal measurement. 99 6 F 8 A 0 7 8 7 11.Specifications 11.1 General Specifications Measurement method: Microwave phase difference method Measurement range: The density measurement range is set by setting the lower (4mA) and upper (20mA) ranges of density measurement. The measured object fluid is required to be free from cavities and have fluidity. Please contact Toshiba for ranges other than those described below. Lower density measurement range: Upper density measurement range: Span range: Setting step: 0 to 49%TS 1 to 50%TS 1 to 50%TS 0.1%TS Note 1: The density measurement range above may change depending on the fluid to be measured. Therefore, we recommend you check the density of the fluid beforehand with a sample test. In addition, contact us about the following items beforehand because the fluid viscosity may limit the maximum flow rate. (1) Fluid to be measured (2) Density upper limit (3) Viscosity (4) Flow rate upper limit (5) Temperature upper limit. Note 2: TS (total solids) = Dissolved materials + Floating materials Note 3: Span = Density meter range upper limit - Density meter range lower limit Repeatability : ± 0.01%TS Note 1: Resolution measured in a single unit. Note 2: Refers to the value at the measuring point of 5% or greater of FS (full scale) in measuring a simulated reagent. Note3: Repeatability that can be confirmed using the simulated reagent: Confirmed repeatability ± 2%FS ± 4%FS * Measured values are taken at measurement points of 5% FS or above in the measurement using the simulated reagent. * Full-scale is the maximum value of the measurement range on the upper side of the density measurement range. * If the density distribution in the piping system is not even, manual analysis data and the indication value of the density meter may not be the same. Full-scale 2%TS or greater Less than 2%TS Linearity: When full-scale 2%TS or greater : ± 2%FS When less than full-scale 2%TS : ± 4%FS Note: Refers to the measuring point of 5% or greater of FS (full scale) in measuring a simulated reagent. 100 6 F 8 A 0 7 8 7 Electrical resolution: 0.001%TS Note 1: Resolution measured in a single unit. Note 2: Verifiable resolution in the simulated reagent: 0.1%TS The verifiable resolution value refers to the value which is verified through a test, of the density difference which can be resolved as a density meter output. Marginal errors in testing such as uneven density distribution and environmental variations, etc. are also included in this value. Ambient conditions: Temperature 0 to 50 °C Humidity 5 to 85%RH (No moisture condensation) Structure: (Water resistance: JIS C 0920, IEC IP 65) Note: Outdoor installation is also allowed. However, if the installation site may be exposed to direct sunlight, keep the converter away from the sunlight by setting up a shade. Vibration: The following vibration tests are performed without a problem. (1) Applying vibration of a resonant frequency in 5 to 150 Hz range with acceleration of 4.9 m/s2 in x, y and z directions for 30 minutes each totaling 90 minutes. No deterioration of performance or damage was found. Resonant frequency was 20 to 45 Hz (depending on vibration direction). (2) Applying vibration of 5 to 150 to 5 Hz with acceleration of 4.9 m/s2 for 3 minutes in each direction and this is repeated 10 times for each direction totaling 90 minutes, and no deterioration of performance nor damage was found. Mass: Approx. 20kg Maximum velocity: 5m/s (when viscosity is 1 Pa•s) Note: When the viscosity level increases, the maximum velocity will be limited. Contact Toshiba. (Example: In the case of 0°C water, 1.792 mPa•s) Microwave transmission power: approx. 1mW Note: This power is within the limit stipulated in the Radio Law. No license is required. 11.2 Detector Specifications Meter size: 250 mm or above (mounting piping material should be metal) Insertion probe area flange standard and maximum use pressure Insertion probe area flange standard JIS 10K (JIS B 2238 10K) Diameter 100mm (Sch20) Maximum use pressure 0 to 1 mPa Note 1: Refer to the mating piping flange (recommended): Note 2: Refer to the mounting short pipe (recommended): Note 3: As to the mounting flange, see “3, Installation ” to install the flange. Fluid temperature: Standard: 0 to 100 °C (No freezing and bubble are not contained) 101 6 F 8 A 0 7 8 7 Fluid conductivity: Fluid conductivity 15 mS/cm or less Note 1: When the conductivity of the fluid becomes 15 mS/cm or above, microwaves attenuate in the fluid and the correct density measurement cannot be made. Note2: Caution in handling fluids being measured. Fluids such as activated carbon containing carbon particles and metallic power containing high-quality conductive particles may affect the density measurement with their high-quality conductive particles. Avoid applying the detector to such fluids. Contact Toshiba for details. Material contacting liquid: Main pipe: SUS316L Temperature detector: SUS316L Applicator (antenna) window frame: Polyetheretherketone (PEEK) (Standard specification) Polysulfone(High-temperature specification) Applicator (antenna) window sealant: Fluoro rubber Note: Do not use the above materials contacting liquid on fluids which may cause corrosion, deterioration or quality change in them. Contact Toshiba for details. Non-applicable fluids: Strong sulfuric acid, strong nitric acid Applicators: A pair applicators provided for microwave reception/transmission Temperature detector: RTD (resistance temperature detector) (Pt 100) Mounting style: Applicators facing the upstream and positioned in parallel with flow direction. The piping must be filled with fluid. Note: See 3, “Installation” for details when mounting the density meter. Maximum velocity: Note: When the viscosity of the fluid increases, the maximum velocity will change. Contact Toshiba. 11.3 Converter Specifications Output signals: Density measurement output: 4 to 20mADC (load resistance 750 Ω or less; insulated output) Density meter fault or maintenance signal: Semiconductor contact output capacitance 125VAC, 0.1A (resistive load) When the density meter converter is in error or in setting mode, the contact will be open. 102 6 F 8 A 0 7 8 7 Communication signals: Digital signals are sent superimposed on the 4 to 20mADC signal line (based on the HART*1 protocol). *1 HART: Abbreviated from Highway Addressable Remote Transducer as the name of a industrial sensor communications protocol recommended by HCF (HART Communication Foundation). Note: Various operations can be remotely performed by connecting the cable pin of the communication hand-held terminal (optional) to the 4 to 20mADC signal line. For specification information on the unication hand-held terminal, please refer to the AF100 specifications. Input signals: Externally synchronized input signal: No-voltage "a" contact Note: This is the contact signal to operate the density meter synchronized with the external pumping operation. Use a contact with the capacitance of at least 24VDC and 1A. This is used when pumps are not operating continuously and the fluid may be drained out. This is to operate the density meter synchronized with the flow of the fluid to be measured such as a pumping operation. Contact closed: Measurement is made; Contact open: Measurement stopped Density multiplier switching signal: Voltage signal two points Input voltage H level 20 to 30VDC L level 2VDC or less Input resistance about 3 k ohms This signal is used to remotely switch four density multipliers, thus making it possible to easily deal with switching around four measured object fluid or mixed fluids (brands) of different components or compound ratios. Electric conductivity correction signal: 4 to 20mADC (to deal with conductivity 0 to 10mS/cm) In the event of implementing a electric conductivity correction, prepare a conductivity meter separately, install it on a location where the conductivity can be reliably measured and then input the conductivity correction signal. Density measurement output and display update cycle: About 1 second Moving average: Outputs the measured density in terms of every 1 second as the moving average of 1 to 99 times. This is used when an averaged output is necessary for density control, etc. Change-rate limit: permissible variation width 0.00 to 9.99%TS; limit times: 0 to 99 In the event of a sudden change in the density or a sudden variation in the output due to intrusion by bubbles, etc., this function is used to exclude these signals to restrain the sudden output change. The conditions for change-rate limit can be set by setting the permissible change width and the limit times. Additives correction function: Capable of handling up to ten brands, this function performs the sensitivity correction appropriate to the additives type and compound ratio in accordance with the parameters that are registered in advance. 103 6 F 8 A 0 7 8 7 Arresters: Mounted as standard on the current output and AC power supply lines. External display section: Equipped with the density display as standard. LED of 7 segments by 4 characters (00.00 to 99.99 %TS). Operation console (inside the converter): Used for verifying, changing and manipulating various data. Five control switches Display: LCD of 4 lines by 20 characters (dot matrix) Power supply: 100 to 240 VAC; 50/60 Hz (Allowable power supply voltage: 85 to 264 VAC) Power consumption: About 50 VA Case material: Steel plate Coating: Polyurethane 104 6 F 8 A 0 7 8 7 11.4 Model Number Table Table 11.1 Model Number Table TYPE CAT Code L Q 3 SPECIFICATION 9 10 12 13 14 15 LQ300 Density (Consistency) meter Standard Meter Size Insertion type (Suitable Pipe size 250mm (10”) or larger) Attachment hole flange for LQ300 insertion type Equipment for ANSI 150 (meter size 100mm (4”)) Equipment for DIN 10 (meter size 100mm (4”)) Equipment for BS 10 (meter size 100mm (4”)) Equipment for JIS 10K (JIS B 2238 10K) meter size 100mm (4”) Others Fluid Temperature High temperature type (0-100 deg. C) (32 to 212 deg. F) Power Supply 100-240Vac, 50/60Hz TYPE Insertion type Wetting parts Standard (316SS) Hastelloy C 276 Others Other A Standard Note 1: This specification is manufactured only when ordered. Contact about delivery time. Note 2: Sealing material: Silicon rubber, Applicators (antenna) protecting material: PEEK Contact beforehand if other materials are preferred for the sealing and for Applicator protection. Note 3: Contact beforehand if Code Z is necessary. 105 6 F 8 A 0 7 8 7 Table 11.2. Type Function code as converter direction toward the flow direction Converter direction toward the flow direction Description of Function code Figure 9-A None (standard) Figure 9-B FUNC. A Figure 9-C FUNC. B Figure 9-D FUNC. C Note: The LED display is located in the backside of Cable gland ports. Cable gland LED display LED display Converter Converter Flow Flow Cable gland Applicator Applicator Fig. 9-A: Function code: None Fig. 9-B: Function code: A LED display Cable gland Cable gland Converter Converter Flow Flow Applicator Applicator LED display Fig. 9-D: Function code: C Fig. 9-C: Function code: B 106 6 F 8 A 0 7 8 7 Appendix Attached Figure 1. [Unit: mm] Center of gravity position 重心位置 231 8 - φ 19 hole JIS10K, JIS10K, 100A 100A flange 57 フランジ 107 6 F 8 A 0 7 8 7 Operation Manual For The Insertion Type Density Meter Type LQ300A00****** Feb. 2002 Address: 1st Edition (A) Toshiba Corporation, 1-1, Shibaura 1-chome, Minato-ku, Tokyo 105-8001, Japan Phone: +81-3-3457-8302 © Toshiba Corporation, 2002 108 All Rights Reserved.
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