Honeywell R-1234yf Solstice yf Refrigerant America User Guide

User Guide for Honeywell models including: R-1234yf, Solstice yf Refrigerant America

Solstice® yf Refrigerant User Guide Solstice® yf Refrigerant User Guide Table of Contents October 24, 2014 Honeywell Solstice® yf Refrigerant User Guide PART 1 | GENERAL INFORMATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 The Next Generation Refrigerant for Automotive Air Conditioning (Brochure) . . . . . . . . . . . . . . . . 3 Solstice yf Refrigerant Fact Sheet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Guideline for Use and Handling of Solstice yf . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 Honeywell Solstice yf Refrigerant MSDS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 Honeywell Solstice yf: Cool for all Concerned (Brochure). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 Solstice yf Refrigerant Properties and Materials Compatibility . . . . . . . . . . . . . . . . . . . . . . . . . . . 27 Solstice yf Refrigerant Packaging Guide (Americas) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34 PART 2 | CUSTOMER PROCESS AND PROCEDURES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 Receiving Loaded ISO Tanks (Flow Chart and Procedure) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 Prepare Tank and Equipment for Initial Offload . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 Offloading into a Fixed Bulk Storage Asset. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45 Unloading Procedure and Operation / Maintenance Manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49 Honeywell STOP Process . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56 Cylinder Return Process . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58 Receiving Full Cylinders. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61 Commission Tank for Initial Offloading . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63 Checklist for Commissioning Tank for Initial Unloading . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69 PART 3 | QUALITY AND ANALYTICAL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71 Certificate of Analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73 Customer Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74 Laboratory Equipment Recommendation for HFO Refrigerants QA/QC Analyses . . . . . . . . . . . . 75 Sampling Cylinder Preparation for HFO Refrigerants QA/QC Analyses . . . . . . . . . . . . . . . . . . . . 77 Sampling Cylinder Preparation Rack Schematic. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80 Sampling Manifold Design from Swagelok . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81 Collecting Samples from ISOs and Cylinders . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82 Connection of Sample Cylinder to Gas Chromatograph. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87 Visual Inspection for Appearance, Particulates and Solids in HFO Refrigerants . . . . . . . . . . . . . 88 Determination of Moisture in HFO Refrigerants. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89 Determination of Acidity in HFO Refrigerants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91 Determination of Non-Volatile Residue in HFO Refrigerants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93 Determination of Chloride in HFO Refrigerants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95 Determination of HFO Refrigerants Assay. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97 Determination of Non-Condensable Gases in HFO Refrigerants . . . . . . . . . . . . . . . . . . . . . . . . . 99 Scheme for Non-Condensable GC Injection Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 102 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Table of Contents Scheme for Non-Condensable GC Sampling Manifold. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 Process Map Distribution and QC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 104 Sample Size Summary Chart. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105 PART 4 | CYLINDER SPECIFICATIONS AND DRAWINGS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 107 10 lb (4.5 kg) Non Returnable Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 109 25 lb (11.3 kg) Non Returnable Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 113 10 lb (4.5 kg) Returnable Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 116 25 lb (11.3 kg) Returnable Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 119 100 lb (45.3 kg) Returnable Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 122 950 lb (430 kg) Returnable Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 125 1750 lb (794 kg) Returnable Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 128 ISO Container Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 131 25 lb (10 kg) Reclaim Cylinder Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 142 Cylinder Labels and Tags. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 145 PART 5 | VALVE SPECIFICATIONS AND DRAWINGS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 155 CGA 166 Valve Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157 CGA 670 Valve Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 162 CGA 670 Single Phase Valve Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 163 Epsilon Valves (Skid Pump Connections) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 164 Fitting of Valves to Gas Cylinders (ISO Standard 13341) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 174 PART 6 | REGULATORY INFORMATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187 Transportation Regulation of Hazardous Materials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189 U.S. EPA SNAP Final Rule: EPA-HQ-OAR-2008-0664 2011-6268 . . . . . . . . . . . . . . . . . . . . . . . 190 CAFE Regulatory Announcement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 223 PART 7 | AUXILIARY EQUIPMENT PROVIDERS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 233 Auxiliary Equipment and Suppliers: Category Listing and Websites. . . . . . . . . . . . . . . . . . . . . . 235 Hoses and Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 237 - CPS Gauges and Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 238 - Errecom Hose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 239 - Mastercool Gauge Manifold . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 243 - Yellow Jacket (CGA 166 LH Adapter) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 246 Leak Detection. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 249 - CPS Leak Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 250 - Robinair Leak Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 252 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Table of Contents - RTI Leak Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 262 - Techno Tools Leak Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 264 - Yellow Jacket Leak Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 273 Pumps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 283 - Haskel Pump for Hose Recovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 284 Recovery, Recycle, Recharge (RRR) Machines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 287 - CPS RRR Machine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 288 - Ecotechnics ECK Twin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 290 - Launch UK RRR System. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 295 - Robinair Service Equipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 297 - RTI Mahle RRR Machine. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 321 Refrigerant Identification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 323 - Neutronics Refrigerant Identifier . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 324 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Table of Contents Part 1 General Information 1 Solstice®® yyffRuesferigaenrdahnat nUdsleinrgG, ueindgeineering and QA guidelines Title of part Slinoelsttwicoe®ofytfitRleeiffringeeerednetd Table of Contents Doc Number: # Part 1 - Page 2 © 2013 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: # Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 3 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 4 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 5 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 6 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 7 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 8 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 9 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide The Next-Generation Refrigerant for Automotive Air Conditioning Table of Contents Part 1 - Page 10 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Solstice® yf Refrigerant Fact Sheet Table of Contents Part 1 - Page 11 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Solstice® yf Refrigerant Fact Sheet Table of Contents Part 1 - Page 12 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Guidelines for Use and Handling of Solstice® yf Table of Contents Part 1 - Page 13 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Guidelines for Use and Handling of Solstice® yf Table of Contents Part 1 - Page 14 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Guidelines for Use and Handling of Solstice® yf Table of Contents Part 1 - Page 15 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Guidelines for Use and Handling of Solstice® yf Table of Contents Part 1 - Page 16 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Honeywell Solstice® yf Refrigerant MSDS Table of Contents Part 1 - Page 17 Honeywell Solstice® yf Refrigerant MSDS: www.1234facts.com/msds © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Table of Contents © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 19 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 20 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 21 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 22 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 23 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 24 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 25 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cool for All Concerned Table of Contents Part 1 - Page 26 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Solstice® yf Properties and Materials Compatibility Table of Contents Part 1 - Page 27 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Solstice® yf Properties and Materials Compatibility Table of Contents Part 1 - Page 28 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Solstice® yf Properties and Materials Compatibility Table of Contents Part 1 - Page 29 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Solstice® yf Properties and Materials Compatibility Table of Contents Part 1 - Page 30 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Solstice® yf Properties and Materials Compatibility Table of Contents Part 1 - Page 31 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Solstice® yf Properties and Materials Compatibility Table of Contents Part 1 - Page 32 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Solstice® yf Properties and Materials Compatibility Table of Contents Part 1 - Page 33 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Solstice® yf Refrigerent Packaging Guide (Americas) Table of Contents Part 1 - Page 34 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Solstice® yf Refrigerent Packaging Guide (Americas) Table of Contents Part 1 - Page 35 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Table of Contents Part 1 - Page 36 Table of Contents Part 2 Customer Process and Procedures 2 38 www.honeywell.com Solstice® yf Refrigerant User Guide Receiving Loaded ISO Tanks Driver arrives at facility Flow Chart Table of Contents Document NA-1234yf-2.1 Part 2 - Page 39 Step 1 - Check In Driver - report in at gate. Site traffic control - instructs where and how to park on the weight scale Step 2 - Full Weight Driver - Weigh per the site specific procedures and obtain full weight ticket Step 3 - Fill Station Driver - Proceed to designated fill station and verify product and paper work with authorized customer employee Step 4 - Unload Authorization Site authorized employee Verify receiving tank has unfilled capacity to receive the full load and proper tank is being unloaded into. Step 5 - Connect Hose and Valve Alignment Driver - Follow delivery connection procedure. Customer Employee - Opens Valves to the tank for unloading to proceed Step 6 - Unload Driver - Open proper valves on the delivery vessel to unload and start the pump Step 7 - Disconnect Customer - verify unload complete (tank level rise) Driver - Stop Pump, align valves, disconnect and store hoses Step 8 - Scale Out Driver - Obtain "light weight", Calculate Net Weight Delivered Customer - Confirm values Delivery Complete Driver Departs © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Receiving Loaded ISO Tanks Table of Contents Part 2 - Page 40 1. RECEIVING LOADED ISO TANKS 1.1 Reception a. Truck arrives at gate and is admitted by traffic control 1.2 ISO Weight (Full) a. Receiving facility performs daily scale procedures prior to weighing ISO b. Park ISO chassis and tractor on the scale per receiving facilities direction c. Weigh ISO and receive the "full weight" value from the customer's facility 1.3 Product and Documentation Verification a. Receiving facility will verify all shipping documents such as: · Bill of Lading (BOL) · Certificate of Analysis (COA) · Consignment Note (CMR) b. Facility contact checks the scale weight verses the BOL weight and notifies Honeywell of any discrepancies > +/- 5%. Immediately notify Honeywell of any abnormalities using the STOP procedure as outlined in procedure Honeywell STOP Procedure and provide supporting documentation such as digital photos. 2. VERIFICATION AND HANDOVER OF DOCUMENTATION 2.1 Driver parks the ISO tank at the unloading spot/station per site personnel instructions 2.2 Driver presents the shipping paperwork to the sites authorized unloading contact 2.3 Facility contact verifies the product paperwork ensuring that the product listed matches product entered into the scale and what was scheduled for delivery Immediately notify Honeywell of any abnormalities using the STOP procedure as outlined in procedure Honeywell STOP Procedure and provide supporting documentation such as digital photos. 3. UNLOADING AND SCALE OUT 3.1 Facility primary contact instructs driver where to hook up to unload 3.2 Driver connects the appropriate liquid and vapor hoses to the unload station 3.3 Driver unloads the contents of the ISO 3.4 Driver safely disconnects and stores the hoses at the facilities location or on the delivery vessel. 3.5 Driver proceeds to the facility scale for "light weight" scale reading 4. HEEL WEIGHT CHECK 4.1 ISO Weight (Light) a. Park ISO chassis and tractor on the scale per receiving facilities direction b. Weigh ISO and receive the "light weight" value from the customer's facility c. Driver shares light weight with the receiving, tank farm or traffic department contact (should be the same contact that received the full weight for comparison to the Bill Of Lading). 4.2 "Complete" offload verification a. Utilizing the following math, ensure a "normal" heel is all that remains in the ISO. · Full Weight Light Weight = Net Weight Delivered · (Light Weight / Full Weight) x 100 = % Heel Remaining b. Driver shares the Net Weight Delivered and the % Heel Remaining with the receiving tank farm or traffic department contact. c. The % Heel Remaining should be less than 5% d. If more than 5% remains, use the STOP process © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.1 Solstice® yf Refrigerant User Guide Receiving Loaded ISO Tanks Table of Contents Part 2 - Page 41 Immediately notify Honeywell of any abnormalities using the STOP procedure as outlined in procedure Honeywell STOP Procedure and provide supporting documentation such as scale tickets or digital photos. EXAMPLE: Full Weight 30,000 lbs minus Light Weight 1,500 lbs equals Net Weight Delivered 28,500 lbs Light Weight 1,500 lbs divide Full Weight 30,000 lbs % Heel Remaining multiply 100 equals 5% © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-123yf-2.1 Solstice® yf Refrigerant User Guide Prepare Tank and Equipment For Initial Offload Table of Contents Doc Number: NA-1234yf-2.2 Part 2 - Page 42 Approximate ISO Dimensions 20 ft 10 ft 20 ft 9 ft Chassis and Tractor dimensions may vary 58 to 65 ft All suction piping from the hose ~60" connection to the pump should be less than 40" from grade. © 2014by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Prepare Tank and Equipment For Initial Offload Table of Contents Part 2 - Page 43 Typical R-1234yf Pump and Unloading Configuration ISO Tank Sits at grade + 60 Inches. Hoses should flow "downhill" toward the Fill Station box. Close Up Fill Station Connections should not be higher than 40" from Grade Elevation. Holding Tank Discharge piping from the unloading pump may flow "uphill" to The holding tank (i.e. in a pipe rack). Unload Pump No rise in piping prior to pump suction. May cause vapor lock and prevent unloading 40'' © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.2 Solstice® yf Refrigerant User Guide Prepare Tank and Equipment For Initial Offload Table of Contents Part 2 - Page 44 PRIOR TO THE FIRST LOAD BEING DELIVERED TAKE THE FOLLOWING STEPS TO PREPARE THE TANK: 1. Pressure test a. Pressure up with Nitrogen to 90% of the lowest pressure rated piece of equipment in the system. (Note: This could change with each system so no specific pressure is recommended) b. Monitor the system for a minimum of 24 hours to ensure no pressure loss has occurred on the system. c. If loss of pressure occurs, leak check joints, flanges, fittings etc with soap and water Note: fluctuations in ambient temperature change may cause pressure increase/decrease. A steady decrease is the sign of a leak. Open all Valves and connections to get a true SYSTEM tightness. 2. Nitrogen Purge (this could be accomplished by releasing the nitrogen used to pressure test through all the "bleed" valves on the tank and associated piping). Note: It is recommended that Step 1 and this step occur two to three times. This will help to "drive" a lot of the moisture out of the low lying points and joints and make the next step easier to accomplish. 3. Pull vacuum down to 2,000 microns (measured at the tank, not at the pump) a. When the vacuum pump is shut down or valved off, the vacuum at the tank should hold for a minimum of 60 minutes. b. In good conditions (warm days and nights) this process could take 1 to 2 days. This is vacuum pump size dependant, must use a 12 cfm or larger vacuum pump. Caution: If a total of a liter of water is present in the system, this time could go as long as 3 days and up to a week (depending on ambient temperature), step 2 will help prevent this from occurring Caution: If water is present, or during winter, it may be necessary to use a heater with insulating blankets and a tent tarp to elevate the tank temperature and drive off water and/or frost. The fittings and pipes also need to be heated or the water will just move to the coldest portions. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.2 Solstice® yf Refrigerant User Guide Offloading into a Fixed Bulk Storage Asset Flow Chart Table of Contents Doc Number: NA-1234yf-2.3 Part 2 - Page 45 Stage transport vessel at an approved location Step 1 Confirm Analytical Site Quality Department Verifies that the material is within specification or accepts based on HON COA Step 2 Confirm Available Capacity Site Operations Verifies that the receiving vessel can safely hold the contents of the delivered vessel Step 3 Ensure Safety Policies are followed Driver / Unloader Utilize the appropriate PPE for unloading 1234yf and ensure all equipment is properly grounded prior to unloading Step 4 Visual Inspection Driver / Unloader Ensure all hoses are free of contamination and are in safe working condition · Within Test date · No Visible damage Step 5 Prepare Hoses and Equipment Site Operations If dedicated hoses and equipment are not utilized, prepare equipment to eliminate contamination Step 6 Unload Product Driver / Unloader - Verify correct flow path and unload vessel completely Step 7 Recover Hoses Driver / Unloader Recover all hoses and equipment to minimize loss. Disconnect Hoses and store properly for next delivery. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Offloading into a Fixed Bulk Storage Asset Table of Contents Part 2 - Page 46 OFFLOADING INTO A FIXED BULK STORAGE ASSET 1. Verify that a COA is included in the shipping paperwork. The COA certification date may not be greater than 90 days old. 2. Verify that the fixed bulk storage asset has sufficient available space to receive the full contents of the ISO. Fixed bulk storage assets should not be filled above 85% of their total capacity 3. Ensure site personnel are informed/trained in the handling of refrigerants are wearing all required PPE 4. Position the ISO in the designated area for 1234yf transfers. If this area is not marked appropriately, STOP and seek guidance from the responsible Health and Safety professional on site. 5. Check grounding equipment is in good working order, free of abrasions, gouges, kinks or any line breaks 6. Ground the ISO tank, transfer pump and fixed bulk storage asset 7. Under ideal conditions the hoses used will be as short as possible to minimize the opportunity for introduction of non condensable gases and moisture into the transfer lines and tanks. 8. Visually inspect hoses to ensure they are safe for use, check for: a. Fraying b. Gouges c. Kinks d. Any other defects 9. Hoses and pumps should be stored indoors or in a covered area to prevent accumulation of moisture; pump should have caps applied over hose connection points 10. Visually inspect each connection to ensure moisture is not present. If present, manually remove with a clean, dry cloth 11. Connect the couplings to the liquid line of the ISO tank 12. Connect the hose from the coupling to the pump 13. Ideally the hoses and pump should be dedicated for specific product usage. To prepare the hose: a. Connect all hoses, valve, couplings etc. b. Ensure the valves going into the bulk storage tank are closed c. Leave the internal valves and the manual valves for the ISO closed d. Connect to a vacuum source to the point shown below and pull to 2 mbar, holding for 1 minute e. hoses have been completely evacuated, close valves and disconnect vacuum source 14. Close (ensure that) the bleed valve used to pull the vacuum is closed 15. Open the valve(s) from the ISO tank vapor line to the fill box 16. Open the valve(s) from the ISO tank liquid line to the fill box 17. Open the valve(s) for the vapor line to the bulk tank starting inside the fill box 18. Open the valve(s) for the liquid line through the pump to the bulk tank starting inside the fill box 19. Turn on the pump 20. Using a hand held gas leak detector, frequently monitor the pump, bulk tank, all lines and connections for leaks 21. Offload the appropriate contents of the ISO tank. A partial offload may be requested only when the bulk tank is installed on a scale or other means of estimating offload amount are present 22. Stop the pump 23. Close the bulk storage liquid fill valves do not disconnect the hoses (leave the vapor line to the storage open) 24. Close the internal valve and valves "B" and "C" shown below 25. Begin hose recovery procedures to minimize and/or prevent product loss: a. Connect the suction of recovery pump to the liquid sample valve, pictured below as a vacuum connection valve, on the liquid discharge line of the ISO b. Connect the discharge of the recover pump to the vapor sample valve, pictured below as a vacuum connection valve, on the vapor equalization line of the ISO c. Open both sample valves © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.3 Solstice® yf Refrigerant User Guide Offloading into a Fixed Bulk Storage Asset Table of Contents Part 2 - Page 47 Vacuum can be pulled at these connection ports for the liquid and the vapor hoses. d. Verify flow of product, should be pulling product out of the liquid hoses from the liquid fill line on the storage, through the pump and back into the vapor side of the ISO. See diagram below for the proper valve arrangement. · Valve C is Closed · Valve D is Open · Valve B is Closed · Valve A is Open e. Open the valves for the recovery pump f. Engage the pump to recover the product g. Recover product to 3mbar of total pressure on the recovery pump h. Close all valves i. Disconnect all piping and equipment j. Close all valves, Disconnect all piping and equipment © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.3 Solstice® yf Refrigerant User Guide Offloading into a Fixed Bulk Storage Asset Vapor Valves and Hoses Table of Contents Part 2 - Page 48 Close Up A B C D Liquid Valves and Hoses Valves "A" and "C" are a part of the ISO. Valves "B" and "D" are attached to the Hoses. DISCLAIMER Although all statements and information contained herein are believed to be accurate and reliable, they are presented without guarantee or warranty of any kind, expressed or implied. Information provided herein does not relieve the user from the responsibility of carrying out its own tests and experiments, and the user assumes all risks and liability for use of the information and results obtained. Statements or suggestions concerning the use of materials and processes are made without representation or warranty that any such use is free of patent infringement and are not recommendations to infringe on any patents. The user should not assume that all toxicity data and safety measures are indicated herein or that other measures may not be required. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.3 Solstice® yf Refrigerant User Guide Unloading Procedure and Operation/Maintenance Manual Table of Contents Doc Number: NA-1234yf-2.4 Part 2 - Page 49 10522 SUCCESS LANE DAYTON, OHIO 45458 937 245 1915 937 748 5249 FAX www.questengineering.net "Committed to the Quest for Higher Performance" Refrigerant R1234yf ISO Container Unloading Pump Station · MACHINE DESIGN/BUILD · MACHINE VISION · SYSTEMS INTEGRATION · DATA ACQUISITION · TURNKEY PROJECTS UNLOADING PROCEDURE AND OPERATION/MAINTENANCE MANUAL February 2013 SERIAL NUMBER's: 12043-1 thru 12043-5 Manufactured for: Honeywell Specialty Materials 101 Columbia Road © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Unloading Procedure and Operation/Maintenance Manual Table of Contents Part 2 - Page 50 TABLE OF CONTENTS 1. System Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 51 2. System Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 51 3. Unloading Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 51 4. Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 52 5. Drawings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 53 QUEST Dwg 12043-E01, 460/115VAC Power Dist. QUEST Dwg 12043-ENV, Envelope Drawing 6. Component Part Numbers . . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 55 ........................................................................................ 7. Component Information. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 55 Pump (attached as PDF) Motor (attached as PDF) 8. Recommended Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . Page 55 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.4 Solstice® yf Refrigerant User Guide Unloading Procedure and Operation/Maintenance Manual Table of Contents Part 2 - Page 51 QUEST ENGINEERING Refrigerant R1234yf ISO Container Unloading Pump Station 1. SYSTEM OVERVIEW The Refrigerant R1234yf ISO Container Unloading Pump Station described in this document is intended for use to transfer refrigerant R1234yf from an ISO container to a customer's bulk tank. 2. SYSTEM SPECIFICATIONS Pump: Flow rate: Motor: Pressure: Hoses: sliding vane 45 GPM at 50 psi differential 5hp, 480/3/60, 6.83 amps, 215T farme 1150 rpm 400 psig max, 125 psi max differential (2) 2" hoses, 15 feet long, stainless steel braid, PTFE lined (1) 1-1/2" hose, 15 feet long, stainless steel braid, PTFE lined 3. R1234YF ISO UNLOADING PROCEDURE Proper PPE consisting of face shields and gloves are required. 3.1 Position the ISO container chassis close enough to the unloading station to attach the hoses. The hoses should not be under tension or undue strain at the connections. The hoses are approximately 15 feet long. 3.2 Attach static ground cable on unloading station to static ground point on truck chassis. 3.3 Remove hoses as needed from hose storage tubes. Always use caution to avoid kinks in the hoses. 3.4 Remove any safety plugs or caps on the hose ends. 3.5 Connect 2" liquid hose from the customer's existing truck unload station to the liquid port on the ISO container. 3.6 Connect the 1-1/2" vapor hose from the customer's existing truck unload station to thevapor port on the ISO container. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.4 Solstice® yf Refrigerant User Guide Unloading Procedure and Operation/Maintenance Manual Table of Contents Part 2 - Page 52 3.7 Open vapor valve (slowly) at the truck unload station. 3.8 Open vapor valve (slowly) on ISO container to allow pressure to equalize between the tanks. If the tank pressures are unequal (pressure difference greater the 10 psi), you should hear vapor traveling in the line. If not, the ISO container internal excess flow valve may have closed due to excess vapor flow. In this case, close the vapor valve on ISO container. Wait 5-10 minutes for the excess flow valve to open. Again slowly open the vapor valve to allow tank pressures to equalize. When the pressures are equalized between the two vessels proceed to the next step. 3.9 Open the liquid valve (slowly) on the ISO container. Check for any leaks at connections. 3.10 Open the liquid valve (slowly) at the truck unload station and the valves on the liquid lines to and from the pump. Check for any leaks at connections a second time. 3.11 Make sure electrical disconnect switch on electrical enclosure at pumping station is in OFF position. 3.12 Connect power cord of pumping station to power source. 3.13 Turn electrical disconnect switch on unloading position to ON position. 3.14 Select FWD or REV on electrical enclosure. 3.15 Quickly start and stop the pump motor to check pump rotation. An arrow indicating correct rotation is located on the pump casing. If rotation is correct, proceed with unloading, checking for leaks at all times. If rotation is not correct, switch pump rotation at the enclosure and check rotation again. When rotation is correct, proceed with unloading. 3.16 Verify the flow indicator on the unloading station indicates flow is going to bulk tank. The flow indicator can also be used to indicate when liquid flow has stopped and the ISO container is empty. 3.17 When the flow stops the hose may jump or vibrate. This is a signal the ISO container is empty. 3.18 Stop the pump at this point, turn disconnect switch to OFF position and unplug the power cable from the power source. 3.19 Close the liquid valves on the ISO container and the truck unload station. 3.20 Close the vapor valves on the ISO container and the truck unload station. 3.21 Disconnect the vapor line hose and return to hose storage tube. Do not drop the hoses. The fittings are very expensive and can be damaged. Replace any safety plugs or caps that were on the hoses originally. 3.22 Disconnect the 2" liquid line hose and return to the hose storage tube. 3.23 Detach static ground cable from chassis and allow it to retract to unloading station. 4. MAINTENANCE Item Maintenance Required Frequency Hoses Check for leaks/wear Each use Strainer Remove and clean Annually, or as needed Pump Lubricate bearings(refer to mfr's manual) Check for leaks Six month Each use Motor Lubricate bearings(refer to mfr's manual) Annually, or as needed Drive belt Check wear, alignment, tension Six months © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.4 5. DRAWINGS Solstice® yf Refrigerant User Guide Unloading Procedure and Operation/Maintenance Manual Table of Contents Part 2 - Page 53 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.4 Solstice® yf Refrigerant User Guide Unloading Procedure and Operation/Maintenance Manual Table of Contents Part 2 - Page 54 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.4 Solstice® yf Refrigerant User Guide Unloading Procedure and Operation/Maintenance Manual Table of Contents Part 2 - Page 55 6. PARTS LIST Pump - Corken part number ZX2000HGBFFU Motor WEG part number 00512XT3E215T Flow Indicator Corken part number FC200AF Pressure Gauge Ashcroft 25 1009AW02L Drive Belt Gates part number BX70 Pump Station Connection OPW Epsilon part number ZE32AS32A01101 2" Hose Connection OPW Epsilon part number ZE32DS32A05301-Q 1" Hose Connection OPW Epsilon part number ZE16HS16A01301 7. COMPONENT INFORMATION PUMP (PDF Document attached, separate file) MOTOR (PDF Document attached, separate file) 8. RECOMMENDED SPARE PARTS Item MFR Part Number Pump Corken ZX2000HGBFFU Pump, repair kit Corken 3193-XB1 Pump, mech seal Corken 4431-XB2 2" Epsilon coupler OPW ZE32DS32A05301-Q 2" Epsilon coupler, seal kit OPW ZK32HM002002 2" Epsilon adaptor OPW ZE32AS32A01101 2" Epsilon adaptor, seal kit OPW ZK32AM001 2" Epsilon adaptor, face seal OPW ZE100397-040 1" Epsilon coupler OPW ZE16HS16A01301 1" Epsilon coupler, seal kit OPW ZK16HM001 Drive Belt Gates BX70 Quantity 1 1 2 1 2 1 2 2 1 1 2 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.4 Solstice® yf Refrigerant User Guide Honeywell STOP process Flow Chart Table of Contents Doc Number: NA-1234yf-2.5 Part 2 - Page 56 Issue Identified Applies to anything from a Safety Concern to incorrect paper work Step 1 STOP Be aware of your surroundings from abnormal conditions or inappropriate actions and STOP once identified. Step 2 Identify Potential Solutions Where appropriate, use your expertise and knowledge to identify potential solutions. Step 3 Implement Corrective Actions Where the solutions are within your job responsibilities, implement the corrective actions to bring the issue back into standard. If not see next step. Step 4 Escalate to Supervisor Do not extend solutions beyond your area of control, escalate to the next level of management, communicate potential solutions and ask for assistance to implement Step 5 Update Standards to prevent future issues Where appropriate implement corrective actions to eliminate all future occurrences of the abnormal condition or action. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Honeywell STOP process Table of Contents Part 2 - Page 57 Safety Bulletin - STOP USING THE "STOP" PROCESS IS AN EXPECTATION OF EMPLOYEES, TOLLERS AND DISTRIBUTORS Response Time Standards Step Total 30 min 30 min 60 min 90 min 2 hr 3.5 hr >3.5 hr Person Escalating the Question Staff: Identify the root cause and apply the solution. If a solution is not available within 30 minutes or support required, inform next level support. Person Providing the Response Not applicable Maintenance: Production Manager: Plant Manager: Safety Manager: Identify the root cause. If cause not identifiable in 60 minutes or support needed, escalate. Present the root cause preferably along with the solution to the person originally escalating the question within 60 minutes. Honeywell Supply Chain: Identify the root cause. If cause not identifiable in 60 minutes or support needed, escalate. Present the root cause preferably along with the solution to the person originally escalating the question within 2 hours. Honeywell Leadership: Identify the root cause utilizing all available assets until identified and a solution created. Not applicable TRUE EMERGENCIES should be handled using local emergency response, not the STOP Process © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.5 Solstice® yf Refrigerant User Guide Cylinder Return Process Flow Chart Table of Contents Doc Number: NA-1234yf-2.6 Part 2 - Page 58 Identify an Empty or Warranty Return Cylinder(s) to be returned Step 1 Tag and Label Cylinder DOT tags are required for transport Tag if Warranty or Defective Tags can be obtained from Schneider Logistics 1-866-681-5160 Step 2 Palletize Cylinders Ensure that the cylinders are properly and securely palletized to safely ship. Step 3 Schedule Shipment with Schneider Logistics Contact Schneider Logistics at 1-866-681-5160 Provide with the proper information outlined in the procedure. Step 4 Receive Schedule Pick up from Schneider Be sure Bill of Lading is correct and sign. If incorrect contact Schneider immediately © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cylinder Return Process Table of Contents Part 2 - Page 59 EMPTY AND WARRANTY 1. Freight paid by Honeywell on the following: a. All Warranty returns b. Empty ton, half ton,100lb, 25lb, and 10lb cylinders 2. Estimated Credit Processing Time: a. Cylinder Deposit (for Empty, and/or Warranty) - 30 days b. Credit for Product (Warranty) - 60 days 3. Shipment Requirements: a. Make sure DOT tags are attached. DOT tags are required for shipment (if missing please contact Schneider Logistics @ 1-866-681-5160) b. For warranty/defective returns Warranty Return Cylinder Tag must be attached (please contact Schneider Logistics @ 1-866-681-5160) c. Palletize properly, 8 to 12 100lbs cylinders per pallet. Cylinders must be standing up, and insure red arrows are facing up. d. 10lb & 25lb cylinders must be returned palletized and standing upright. e. Empty cylinders are sent to the Honeywell Danville plant* f. Warranty/Defective cylinders are sent to Honeywell Danville plant* *Schneider Logistics will arrange for shipment and will determine where the cylinders should be sent. 4. Instructions for scheduling a cylinder return a. Contact Schneider Logistics at 1-866-681-5160 and have the following information available when placing your call: · Customer name, address, telephone number, fax number, and, e-mail address · Type of return: Warranty and/or empty cylinders · Did you purchase cylinders from Honeywell? · Do you have the proper DOT tags, and Warranty return cylinder tags? · Number of empty cylinders being returned · Size of cylinder (ton, half ton,100lb, 25lb, or 10lb cylinder) · Provide product last contained in each cylinder · Ton cylinder serial number (optional) · Customer's internal reference number (optional). b. Schneider Logistics will provide the following: · Pickup time, date, and name of carrier. - Please allow 48 hours for full-truck loads - Next day before 3:00pm for LTL shipments (request must be made by 3:00 pm CST the previous day to insure pick up) · Fax or e-mail you copy of the Bill of Lading - Please review, verify accuracy, and sign Bill of Lading. - Please contact Schneider Logistics for any corrections or changes to the B/L, and retain a copy for your files Please note that material returned without proper tags may delay credit © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.6 Solstice® yf Refrigerant User Guide Cylinder Return Process Table of Contents Part 2 - Page 60 5. Guidance for Palletizing Cylinders: Due to the flammability classification of this product, cylinders must be palletized in a way to prevent accidental release and the possibility of creating a flammable atmosphere. a. Cylinders must be palletized with the valve facing the upright position. b. The number of cylinders that may be palletized varies, please follow the recommended guidelines. Type of Cylinder 100 lb (45.3 kg) 25 lb (10 kg) 10 lb (5 kg) Maximum Cylinders per Pallet 11 (4 on each side x 3 in the middle) 40 60 c. Since the 100 lb Cylinders are not stackable, this is one suggestion for securely palletizing the cylinders (visual aids follow) 1. Ensure all the cylinders are labeled correctly 2. Once cylinders are placed on the pallet in the upright position, surround the base of the cylinders with boards and nail them to the pallet. 3. Fabricate a box to entirely cover the valve caps of the group of cylinders and place the box on top of and fully covering the cylinder caps. 4. Place steel banding surrounding the boards and cylinders in both directions of the pallet 1. Labels 2. Boards 3. Box 4. Banding 4. Banding © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.6 Solstice® yf Refrigerant User Guide Receiving Full Cylinders Flow Chart Driver arrives at facility Table of Contents Doc Number: NA-1234yf-2.7 Part 2 - Page 61 Step 1 - Check In Driver - report in at gate. Site traffic control - instructs where to park at a fork truck accessible receiving bay Step 2 - Verify Shipping Documents Site traffic control Check Bill of Lading, Certificate of Analysis, Quantities, etc... Step 3 - Unload Cylinders Site authorized employee Using site safety procedures, secure the truck and unload the truck. Driver Comply with all site safety standards regarding the 3rd party truck management (shut down the truck, hand over the keys, etc.) Step 4 - Visual Inspection Customer Employee Inspect jugs and cylinders while offloading for: · Obvious signs of leakage · Damage to cylinders Step 5 - Damage Notification Driver & Site Employee's Utilizing the HON STOP procedure, notify Honeywell of any abnormalities Step 6 - Confirm Receipt Customer verify quantity received matches delivery paperwork Step 7 - QA/QC Customer CoA is accepted or analysis is preformed as appropriate Utilizing the HON STOP procedure, notify Honeywell of any abnormalities © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Receiving Full Cylinders Table of Contents Part 2 - Page 62 RECEIVING FULL CYLINDERS 1. Truck arrives on site and reports to traffic control 2. Product and Documentation Verification a. Customer employee - begins filling out the proper site receiving documentation b. Customer employee - physically verifies the following: · The presence of all required paperwork: - Bill of Lading (BOL) - Consignment Note (CMR) - Certificate of Analysis (COA) · A two way product match: - The labels and tags located on the cylinders - The product on the paper work match 3. Offload truck and store tanks in designated areas. While offloading, watch for obvious signs of leaking or tank damage Immediately notify Honeywell of any abnormalities using the STOP procedure as outlined in procedure Honeywell STOP Procedure and provide supporting documentation such as digital photos. 4. Net weight is received by the warehouse 5. CoA review or analysis is performed by the quality department as appropriate Immediately notify Honeywell of any abnormalities using the STOP procedure as outlined in procedure Honeywell STOP Procedure and provide supporting documentation such as digital photos. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.7 Solstice® yf Refrigerant User Guide Commission Tank for Initial Offloading Flow Chart Step 1 - Ensure Proper Valve Alignment Close Valves at ends of the system. Open ALL other valves in the system Step 2 - Pressure Test with Nitrogen Use Dry Nitrogen to pressure test the entire system up to 90% of the lowest Relieve Valve set point Step 3 - Purge Nitrogen and Moisture vapor Purge the nitrogen from all the low point bleeds and end points to "push" the moisture out of the system Step 4 - Vacuum Evacuate the System Pull vacuum on the entire system, down to at least 2,000 microns. Step 5 - Repeat for a total of three cycles Hold the vacuum on the third and final evacuation Note: Cycle 2 and 3 require less nitrogen for purge step. Table of Contents Doc Number: NA-1234yf-2.8 Part 2 - Page 63 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Commission Tank for Initial Offloading Table of Contents Part 2 - Page 64 1. PRESSURE TEST AND EVACUATION PROCESS Perform pressure tests and evacuation procedures on all lines and equipment that will contain R1234yf. For all steps ensure that all auxiliary equipment utilized in this procedure, including connections and hoses, are rated for greater than 500 psig and certified to hold a 500 micron Hg vacuum. 1.1 Pressure test a. Ensure that you have enough nitrogen on site to pressure up the entire system, this could take at least 4 "cylinder banks" of nitrogen per testing cycle b. Make certain ALL valves are open to the lines and equipment to be tested. Some valves may be air operated and may even need a signal from a panel to open the valve. It is important to ensure all valves are in the open position. There are a lot of valves on the bottom of the tank to open, be sure to get them all. You can use the pressure gauges to monitor pressures. There should also be bleed points to relieve the pressure during the purge step(s). © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.8 Solstice® yf Refrigerant User Guide Commission Tank for Initial Offloading Table of Contents Part 2 - Page 65 c. Pressure test the entire system to 10% less than the lowest rated relief valve setting in the system with dry nitrogen. Primary Tank RV will typically be located on top of the tank. There may be other RV's in the system. The fill box, pictured here, is a good place to connect the nitrogen bank and the recommend location for pulling vacuum. Use the hose provided and connect to the 1" vapor Epsilon fitting. The other hose end can be fitted with a connection for the nitrogen bank or vacuum pump. NOTE: Do not use the 2" liquid connection for vacuum, the flow check will prevent the vacuum flow path. d. Perform leak test on lines and equipment using leak detection solution (Cal Blu is recommended). e. If necessary, repair leaking lines and equipment. f. Repeat steps 2-4 until no leaks are detected. g. Hold N2 pressure for one hour. Residual moisture contained in the system will evaporate into the nitrogen during this period. Compressed air should not be used for leak checking, you will adding moisture to the vessel and will significantly extend evacuation time. Honeywell does not recommend using compressed air. h. Once the lines and equipment are deemed to be leak free continue to the next step. 1.2 Purge Nitrogen through the low point bleeds and ends of the system a. Open the valves at the ends of the system (Fill Box and Assembly Line) and under the holding tank. Pay particular attention to open the low points in the system, especially under the holding tank. · This could be a loud process © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.8 Solstice® yf Refrigerant User Guide Commission Tank for Initial Offloading Table of Contents Part 2 - Page 66 b. Monitor a pressure gauge on the system once the gauges read 50 to 100 PSIG, begin to close the valves at the end of the lines working toward the holding tank. c. Continue to bleed the nitrogen in the system down to a slight positive pressure on the system, 5 to 10 psig. 1.3 Evacuate lines and equipment to less than 2,000 microns a. Utilize an adequately sized vacuum pump to evacuate the system. Remember the tank is typically 6,500 gallon capacity and the systems normally have a lot of piping to be evacuated. While a smaller vacuum pump(s) can be used , we recommend at least one 80 SCFM vacuum pump to pull down the system (shown below). This size pump should pull down the entire system in 4-6 hours. If it takes longer than 6 hours, you probably have a leak in the system (a valve open to atmosphere, loose hose connections and small bleeds like the one behind this pressure gauge are likely leak sources) or residual water in the tank. Small "bleed" port © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.8 Solstice® yf Refrigerant User Guide Commission Tank for Initial Offloading Table of Contents Part 2 - Page 67 b. Hook up the vacuum pump to the vapor line at the fill box and pull vacuum on the entire system. c. Ensure that the entire system is open from the fill box to the end of the line inside the assembly plant. d. Pull vacuum until 2,000 microns vacuum is attained and continue evacuating for two hours. Residual water will vaporize during evacuation to below 2000 microns. We recommend a digital Micrometer that should be connected to a bleed port under the tank, not at the vacuum pump. The micrometer pictured is capable of reading high readings approx. 75,000 microns. Most meters will not start reading until the system is less than 12,000 microns. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-2.8 Solstice® yf Refrigerant User Guide Commission Tank for Initial Offloading Table of Contents Part 2 - Page 68 e. Shut down the vacuum pump and close off the valve at the fill box "locking in" the vacuum f. The system should hold less than 2,000 microns for one to two hours. · If the lines and equipment do not pass the vacuum check (step F), look for possible sources of leaks at all connections, including welds, hoses, valves, etc. Likely sources of leak points are hoses and connections, ensure the vacuum pump(s) and hose(s) are isolated from the system being tested. · If the evacuation pressure plateaus or slows significantly you may have free water in the tank. Add insulating blankets and start heating the tank to drive off water or frost. Once the tank and lines are above freezing, break the vacuum with dry nitrogen and start evacuation over. 1.4 Repeat all steps above two (2) more times to ensure the system is ready to charge. 1.5 On the third and final evacuation, keep the system under vacuum until the unloading of the 1234yf product takes place. Vapor form the 1234yf ISO will be used to break the vacuum during the initial unloading. 1.6 If the tank initial fill is to be postponed/delayed, Honeywell recommends filling with +30 psig of dry nitrogen (NOT compressed air) until Commissioning takes place. a. Vacuum will have to be pulled down to 2,000 microns and held for one to two hours prior to filling with Solstice 1234yf. The entire process could take 3-6 days to complete Disclaimer Although all statements and information contained herein are believed to be accurate and reliable, they are presented without guarantee or warranty of any kind, expressed or implied. Information provided herein does not relieve the user from the responsibility of carrying out its own tests and experiments, and the user assumes all risks and liability for use of the information and results obtained. Statements or suggestions concerning the use of materials and processes are made without representation or warranty that any such use is free of patent infringement and are not recommendations to infringe on any patents. The user should not assume that all toxicity data and safety measures are indicated herein or that other measures may not be required. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-2.8 Solstice® yf Refrigerant User Guide Checklist for Commissioning Tank for Initial Unloading Table of Contents Doc Number: NA-1234-2.9 Part 2 - Page 69 Piping installed completely from the Fill Box to the Fill Station inside the Assembly Plant (Ensure Scope of Work was completed) Ensure tank is properly marked with Chemical Name, HMIS ratings, etc. Valve Closed at filling station cabinet inside Assembly Plant All Valves Open "walking back" to 1234yf Holding Tank discharge pump All Valves Open under the 1234yf Holding Tank · Pay careful attention to air accuted valves · Pay careful attention to any control valves · You may have to activate the control pannel · You may have to activate the Emergency Shut Down system Ensure one Relief Valves (RV's) is in the open position Document the Set Pressure on the RV All Valves Open "walking back" to the skid pump (the liquid unload line) All Valves Open " walking back" to the fill box (the vapor equalize line) ISO Delivery Scheduled, Please indicate the date for the ISO delivery Complete Pressure Test and Evacuation Procedure (SOP NA-1234yf-2.8) · Purchase or ensure the site has Nitrogen for pressure testing · Rent or ensure that you have the proper vacuum pump to evacuate · Rent or ensure that you have hoses and connections · This proces may take 3 to 6 days (Initial when cycle step is complete) Pressure test preformed (at 10% less than RV set points) Pressure test held for 1 hour minimum Nitrogen Purged through low points and ends of the piping system Vacuum (measured at the 1234yf holding tank) reached 2000 microns Vacuum (measured at the 1234yf holding tank) held 2000 microns for 2 hours Contractor Preforming work Signature: Customer Accepting work Signature: Hold vacuum (and equipment) until ISO arrives for unloading Vacuum (measured at the 1234yf holding tank) held 2000 microns for 2 hours Yes No Initial © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Part 2 - Page 70 Table of Contents Part 3 Quality and Analytical Information 3 72 www.honeywell.com Solstice® yf Refrigerant User Guide Certificate of Analysis Table of Contents Part 3 - Page 73 Street Address City, State, Zip, Country Phone: +XX XXX-XXX-XXXX Distributor Location Master Lot Number: Packaged Lot Number: Customer: if applicable Honeywell SolsticeTM yf Refrigerant 2,3,3,3-Tetrafluoroprop-1-ene (Automotive Grade) Certificate Of Analysis Delivery Date: Packaged Date: Order Number: if applicable Purity 1225yeZ 1234zeE Other unsaturates (total) Moisture Acidity Residue Non Condensible Gases Appearance Particles or Solids Specification 99.5 wt.% min 150 ppm by wt. max 500 ppm by wt. max 40 ppm by wt. max 20 ppm by wt. max 1 ppm by wt. max 100 ppm by v/v max 1.5 Vol. % max Clear, Colorless Visually Clean Results Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Certified by_______________________ Laboratory Analyst The test results herein reported represent the analysis regularly performed in accordance with our documented quality control programs. Section 3.1 - Certificate of Analysis (Sample) © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Customer Specification Table of Contents Part 3 - Page 74 FLUORINE PRODUCTS Customer Specification No. CS SolsticeTM 1234yf-1 Rev. 4 T Honeywell SolsticeTM 1234yf (Automotive Grade) Alternate Name(s): Chemical Formula: CAS Number: R-1234yf CH2CFCF3 754-12-1 Parameter Limit1 2,3,3,3-Tetrafluoroprop-1-ene 99.5% (w/w), min. Moisture 20 ppm (w/w), max. Acidity as HCl 1 ppm (w/w) as HCl, max. Non-volatile residue 100 ppm (v/v), max. Particulates and Solids Visually clean to pass Density @25°C 1.08 to 1.10 Kg/L Non-condensable gases in vapor phase @25°C 1.5% (v/v) max. Appearance (clear, colorless liquefied gas) Visual to pass test Impurities: Maximum Quantity in Liquid Phase Detected by This Method (E) 1,3,3,3-Tetrafluoroprop-1-ene, 1234ze(E) (Z) 1,2,3,3,3 Pentafluoroprop-1-ene, 1225ye(Z) Total unspecified unsaturated compounds Total organic impurities 1,000 ppm (w/w), max. 150 ppm (w/w), max. 40 ppm (w/w), max. 5,000 ppm (w/w), max. 1 All analyses shall be performed on the liquid phase of the sample, unless noted otherwise. Test Method RDAM-618 Rev. 1 Solstice-1234yf-52 Solstice-1234yf-2 Solstice-1234yf-6 Visual Inspection Solstice-1234yf-50 Solstice-1234yf-8 Visual Inspection RDAM-618 Rev 1. RDAM-618 Rev. 1 RDAM-618 Rev. 1 RDAM-618 Rev. 1 Approved by: Coordinator of Specifications Fluorine Products Date: 08/22/12 Specification History: CS SolsticeTM 1234yf Rev. 4, revised 08/22/12. Added parameter for (E) 1,3,3,3-Tetrafluoroprop-1-ene,1234ze(E). CS SolsticeTM 1234yf Rev. 3, revised 12/13/11. Revised Spec due to Name Change from HFO-1234yf to SolsticeTM 1234yf. CS HFO-1234yf -1 Rev 2, revised 04/28/10. Revised GC method. The method RDAM-618T has been revised and is now RDAM-618 Rev. 1. CS HFO-1234yf -1 Rev 1, revised 02/17/10. Removed Chlorides parameter. Removed limit for Acidity as HCl, mg KOH/gm. New, issued 07/16/09. This is a Controlled Document when embossed as follows: Honeywell - CONTROLLED DOCUMENT. Page 1 of 1 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Laboratory Equipment Recommendation for HFO Refrigerants QA/QC Analyses Table of Contents Part 3 - Page 75 Laboratory Equipment Recommendation for HFO Refrigerants QA/QC Analyses This document describes the recommended equipment needed for HFO Refrigerants QA/QC analyses procedures. The details of the laboratory layout, wiring and plumbing designs as well as gas supply and chemical reagents are not included in this document. 1. SAMPLING CYLINDERS , QTY: VARY 1.1 Stainless steel, carbon steel or Aluminum cylinders, which are certified for refrigerant service and have pressure rating greater than 15 bar with relief valve, should be used. 1.2 The internal volume should be more than 300 mL but less than 1 L (300 mL < Volume < 1000 mL). for gas and vapor sampling cylinders. Qty: 4-6 1.3 The internal volume should be 1L for ISO sample retaining cylinders. QTY:12-14 2. LARGE DRYING OVEN, QTY:1 2.1 Internal depth should be larger than sampling cylinder length and diameter. 2.2 Temperature control range: room temperature to 200 oC 3. VACUUM PUMP, QTY:1 3.1 The maximum vacuum should be 29.5 inches of Hg (10 torr) or better. 3.2 Free air displacement at 1 aatmosphere should be greater than 2 CFM or 60 L/min. 4. CYLINDER PREPARATION MANIFOLD, QTY: 1 4.1 The manifold should have two or more sampling cylinder inlet connections. 4.2 The manifold should have a minimum of one Helium supply port, and one vacuum port. 4.3 The manifold should have one Pressure-Vacuum gauge, 30'' Hg vacuum to 30 PSIG (-100 to 200 kPa gauge), this gauge may be dial or electronic. 5. GC SYSTEM, QTY: 1 5.1 Assay determination using traditional GC system a. Equipped with a flame ionization detector (FID) b. Chromatography data system: Capable of electronic integration and processing the chromatographic data. c. Gas chromatographic column: 1% SP-1000, 60/80 Carbopack B column. 24 ft, 1/8'' Stainless steel column or equivalent. d. Gas inject syringe (2 mL) or auto injection valve with sampling loop (1mL) 5.2 Non- condensable gas analysis using traditional GC system a. Equipped with a thermal conductivity detector (TCD), and capable of oven temperature programming. b. Chromatography data system: Capable of electronic integration and processing the chromatographic data. c. Gas chromatographic column (Packed): Poropak QS, 80-100 mesh 6ft, 1/8'' Stainless steel column, or equivalent. d. Gas inject syringe (2 mL) or auto gas injection valve with sampling loop (1mL) 6. KARL FISCHER ANALYZER, QTY:1 6.1 KF coulometric titration system (contains a removable drying tube for venting refrigerant, anode and cathode solutions, septum, and water vaporizer) 6.2 Drierite, 20-40 mesh 6.3 Desiccator, containing Drierite 6.4 Needle attachment assembly for cylinder sampling. Please refer to AHRI standard 700-2006, 2008 appendix C, Part 2 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Laboratory Equipment Recommendation for HFO Refrigerants QA/QC Analyses Table of Contents Part 3 - Page 76 7. SCALES, QTY: VARY 7.1 op loading scale 4000g with 0.1g resolution, Qty:1 7.2 Analytical scale, 320g with 0.1mg resolution, Qty:1 8. GENERAL LAB GLASSWARE AND SUPPLIES, QTY: VARY 8.1 Gas Dispersion tube, polyethylene, Qty:1 8.2 Hot plate with stir, Qty:1 8.3 Amber-glass bottle, 300 mL, for Silver Nitrate solution, Qty:1 8.4 Assorted graduated cylinders 8.5 Assorted beakers 8.6 Assorted volumetric flasks 8.7 Deionized water supply system Revised: v101, Jim Tu, 10/16/2012 modify required GC equipments to matching current method. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Sampling Cylinder Preparation for HFO Refrigerants QA/QC Analyses Table of Contents Part 3 - Page 77 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Sampling Cylinder Preparation for HFO Refrigerants QA/QC Analyses HFO-Refrigerants-1 Material: Analyte: Technique: Specific Method: Supersedes: Also Required: HFO Refrigerants Sampling Cylinder Preparation for HFO Refrigerants QA/QC Analyses Vacuum and Purge HFO-Refrigerants-1 None None PURPOSE To describe sampling cylinder preparation procedure for HFO Refrigerants QA/QC analyses. SCOPE All cylinders used for sampling HFO Refrigerants analyses should be prepared per this procedure. Procedure written for 50 c.c. to 1 liter sampling cylinders. SAFETY 1. 2. HFO Refrigerants is a compressed liquefied gas which becomes very cold as it volatilizes. See MSDS. Please review the all materials' MSDS. Wear safety glasses and safety shoes at all time. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. EQUIPMENT 1. Large drying oven controlled at 50°C 2. Vacuum pump, capable of achieving 29.5 in Hg of vacuum (1600 Pa abs. or 12 Torr) 3. Helium, industrial grade, feeding pressure 35 PSIA (240 kPa abs.) 4. Preparation manifold with pressure (0-30 PSIA, 0-200 kPa abs.) and vacuum gauge 5. Preferred solvent: SolsticeTM 1233zd 6. Alternative Solvents: methylene chloride, acetone or hexane, reagent grade 7. Graduated cylinder, 100mL 8. Balance PROCEDURE Preparation of new sampling cylinders for HFO Refrigerants service 1. Inspect new sampling cylinder for any rust, water and/or oil residue. Clean any visible contaminations. 2. Place sample cylinder in the oven at 50°C, with valves completely open, for no less than one hour. 3. Remove cylinder from the oven and connect cylinder to the preparation manifold. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Sampling Cylinder Preparation for HFO Refrigerants QA/QC Analyses Table of Contents Part 3 - Page 78 4. Evacuate cylinder to at least 29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 20 minutes. 5. Shut off vacuum, fill the cylinder with helium to 25 PSIA (175 kPa abs.), and then close the cylinder valve for 5 minutes. 6. Open cylinder valve and evacuate cylinder to at least 29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 10 minutes. 7. Repeat steps 5 and 6 two more times. 8. Close cylinder valves, and the cylinder is ready for sampling. Preparation of used sampling cylinders for HFO Refrigerants service 1. Connect cylinder to the preparation manifold. 2. Vent residual HFO Refrigerants from the cylinder to ambient pressure. 3. Evacuate cylinder to at least - 29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 3 minutes. 4. Shut off vacuum, fill the cylinder with Helium to 25 PSIA (175 kPa abs.), and then close the cylinder valve for 30 seconds. 5. Open cylinder valve and evacuate cylinder to at least - 29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 1 minute. 6. Repeat steps 4 and 5 two more times. 7. Close cylinder valves, and the cylinder is ready for sampling. Contaminated sampling cylinders cleaning procedures * This section is for the contaminated new sampling cylinders and for used sampling cylinders are contaminated with oil residues during the service. [Use SolsticeTM Performance Fluid (1233zd) preferred solvent] **The following steps are the cleaning procedures for using SolsticeTM Performance Fluid (1233zd) (preferred). 1. Connect the sampling cylinder valve to 1233zd container with clean fittings and tubings. 2. Open the sampling cylinder valve, and then fill the cylinder with about 32 grams of 1233zd solvent (~25 mL of 1233zd). 3. Close sampling cylinder valve, and detach the cylinder from 1233zd container. 4. Carefully swirl the cylinder to rinse the cylinder interior wall for 30-60 seconds. 5. Carefully empty the 1233zd from the sampling cylinder to a waste container. a. The cylinder will have built up vapor pressure. Open the cylinder valve carefully. b. Position the sampling cylinder upside-down to help 1233zd liquid flow out from the cylinder. 6. Repeat steps 1 - 5 three more times so total of approximately 100 mL of 1233zd solvent is used for rinsing the cylinder. 7. Disassemble the cylinder valve, and then inspect the cylinder for any visible oil residue. If any oil residue is still visible, reinstall the cylinder valve, and then repeat steps 1 - 5 one more time. If the oil residue is still visible, discard the cylinder. 8. Reassemble the cylinder valve per cylinder/valve manufacturer procedures. 9. Evacuate cylinder to at least 29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 5 minutes. 10. Shut off vacuum, fill the cylinder with helium to 25 PSIA (175 kPa abs.), and then close the cylinder valve. Check for leak around the cylinder valve. 11. Open cylinder valve and evacuate cylinder to at least -29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 5 minutes. 12. Fill the cylinder with helium to ambient pressure. 13. Disconnect the cylinder from the manifold with cylinder valve completely opened. Place the cylinder in the 50°C oven for no less than one hour. 14. Prepare the cleaned cylinder as NEW sampling cylinder for service. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Sampling Cylinder Preparation for HFO Refrigerants QA/QC Analyses Table of Contents Part 3 - Page 79 [Use Alternative Solvents] *** The following steps are the cleaning procedures for using alternative solvents, such as methylene chloride, acetone or hexane. 1. Disassemble the cylinder value from the contaminated cylinder per cylinder/valve manufacturer procedures. 2. Fill the cylinder with 25 mL of solvent. 3. Carefully swirl the cylinder to rinse the cylinder interior wall for 30-60 seconds. 4. Pour alternative solvents from the cylinder to a waste container. 5. Repeat steps 2 - 4 three more times so total of ~100 mL of solvent is used for rinsing the cylinder. 6. Inspect the cylinder for any visible oil residue. If any oil residue is still visible, repeat steps 2 - 4 three more times. If the oil residue is still visible, discard the cylinder. 7. Reassemble the cylinder valve per cylinder/valve manufacturer procedures. 8. Evacuate cylinder to at least 29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 5 minutes. 9. Shut off vacuum, fill the cylinder with helium to 25 PSIA (175 kPa abs.), and then close the cylinder valve. Check for leak around the cylinder valve. 10. Open cylinder valve and evacuate cylinder to at least 29.5 in.Hg of vacuum (1600 Pa abs. or 12 Torr) for 5 minutes. 11. Fill the cylinder with helium to ambient pressure. 12. Disconnect the cylinder from the manifold with cylinder valve completely opened. Place the cylinder in the 50°C oven for no less than one hour. 13. Prepare the cleaned cylinder as NEW sampling cylinder for service. Written by; Jim Tu Date: April 17, 2012 Date: Sep. 21, 2012, Revised by: Jim Tu, Revision on changing 1234yf to HFO Refrigerants and added cleaning procedures for contaminated cylinders. Date: Nov. 12, 2012, Revised by: Jim Tu, Revision on adding 1233zd as preferred solvent. Added Acetone and Hexane as alternative solvents. Date: Nov 14, 2012, Revised by: Jim Tu, Added metric units and modified procedure description texts for clarification. Corrected the oven temperature in equipment section. Approved by: John L. Welch Date: April 17, 2012 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Sampling Cylinder Preparation Rack Schematic Table of Contents Part 3 - Page 80 Sampling Cylinder Preparation Rack Schematic Vent Vacuum Pump Connections to Sampling Cylinders Helium Supply Manifold P Pressure/Vacuum Guage 3-5 Control Valves 1. VACUUM PUMP 1.2 Capable of achieving 29.5 in Hg of vacuum (1600 Pa abs. or 12 Torr) or better 1.1 Free air displacement at 1 atmosphere should be greater than 2 CFM or 60 L/min 2. HELIUM, INDUSTRIAL GRADE, FEEDING PRESSURE 35 PSIA (240 KPA ABS.) 3. PRESSURE/VACUUM (0-30 PSIA, 0-200 KPA ABS.) GAUGE © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Sampling Manifold Design from Swagelok Sampling Manifold Design from Swagelok Table of Contents Part 3 - Page 81 Sampling manifold design from Swagelok 1. VACUUM PUMP IS NOT INCLUDED IN THE DESIGN. 2. SIX CYLINDER CONNECTIONS, ONE HELIUM, ONE NITROGEN AND ONE VACUUM PORT. 3. WELDED MANIFOLD WITH VCR FITTINGS. 4. PARTS NUMBER 4.1 Valves: SS-4BK-VCR (Swaglok) 4.2 Pressure transducer: PX309-200AI (OMEGA ENGINEERING, Inc.) - 0-200 PSIA - 4-20 mA output - 2 wire cable internal excitation pressure transducer 4.3 Digital meter : DP25B-E ((OMEGA ENGINEERING, Inc.) - 4 digits meter - Resolution: 0.1 PSIA © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Collecting Samples from ISOs and Cylinders Flow Chart Table of Contents Doc Number: NA-1234yf-3.6 Part 3 - Page 82 Step 1 Ensure vessel to be sampled is in the proper area for the sampling process. The area should be marked for 1234yf. Step 2 - Proper PPE and Equipment Ensure use of proper PPE for handling 1234yf, and make sure the pumps and other electrical equipment utilized, or in the area, are properly classified. Step 3 - Verify Grounding Ensure equipment and vessel are properly grounded. Step 4 - Connect Hoses, Pumps, Sample Cylinders, etc. Visually inspect all hoses, connections and sample cylinders for any obvious mechanical defects. Attach hoses to accomplish the proper flow path for liquid and vapor samples. Step 5 - Obtain Desired Sample Clear the gas line of any liquid to obtain a "clean" vapor or gas sample. Circulate the liquid with a pump to obtain a representative liquid sample. Step 6 - Secure ISO or Cylinder and Analyze Sample Shut off all pumps and valves to secure the vessel or cylinder. Complete the analytical. Step 7 - Recover the Hoses Back to the Vessel Minimize product loss by utilizing proper recovery process for all connections. Step 8 - Disconnect and Store Equipment Properly Disconnect all hoses and fittings and store in a clean, dry area for future use with 1234yf products. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Collecting Samples from ISOs and Cylinders Table of Contents Part 3 - Page 83 1. EQUIPMENT REQUIRED 1.1 Sample bottles must meet the following specifications: a. Valves: All materials must be compatible with 1234yf per the compatibility matrix b. Pressure Rating: The bottle must have a minimum pressure rating of 18 bar or 260 PSI c. Acceptable Bottle Composition: · Stainless Steel · Aluminum · Carbon Steel 1.2 Gas Leak Detectors are needed for this procedure: a. Should be portable, hand held devices b. Must be calibrated for 1234yf 2. ISO TANKS 2.1 Vapor Sample a. Ensure site personnel are wearing all PPE required for handling 1234yf. b. Inspect the area to ensure the presence of only properly certified equipment. Remove any spark generating device from the immediate sampling area. c. Position the ISO in the designated area for safely handling R1234yf. If the area is not marked to handle 1234yf, STOP immediately and consult the onsite HS&E professional. d. Visually inspect hoses to ensure that they are safe for use. Check for · Fraying · Gouges · Kinks · Any other defects e. Pump preparation: Ideally the pump should be dedicated for specific product usage. · Connect all hoses, valve, couplings etc., except the connection, to the liquid phase · Open the valves from the gas phase to the liquid phase to purge the pump · Connect the hose of the pump to the liquid phase · Open all valves · "Bump" start and immediately stop the pump until all liquid is out of the gas phase · Stop the pump · Close all valves and disconnect the pump f. Take a sample from the gas phase by using a flow-through cylinder. · Connect the sample hose to the vapor line · Connect the other end of the hose to a flow through cylinder · Open the valves to the flow through cylinder and purge for 10 seconds · Close the valves of the flow-through cylinder, farthest away from the ISO first and then moving toward the ISO. 2.2 Liquid phase samples a. Connect the gas phase line to the discharge of the properly certified pump. b. Connect the liquid phase line to the suction of the pump. c. Leaving the valves to the ISO closed, pull a slight vacuum on the hoses and the pump to remove any air introduced to the system during the hose connections. d. Open the valve to the liquid line, through the pump and into the vapor side of the ISO. e. Continue to vent air until the gas monitor detects the presence of gas. f. Turn on the pump. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-3.6 Solstice® yf Refrigerant User Guide Collecting Samples from ISOs and Cylinders Table of Contents Part 3 - Page 84 · Circulate using the following guidance: Pump Capacity 1,700 kg/hr Quantity in ISO Tank 10 MT < 10 MT Duration 30 minutes 15 minutes · Note that the above circulation times will have to be adjusted based on the capacity of available pumps. g. Stop the pump. h. Connect the sample cylinder, prepared per the procedure in Section 3, on the discharge side of the pump, but prior to the ISO. · Start the pump · Open the sample cylinder valve · Fill with a minimum of 1,000 g · Close the valve to the sample cylinder and the sample valve on the pump · Stop the pump · Disconnect the sample bottle Bleed Valves for the ISO Liquid and Vapor valves. i. Begin hose recovery procedures to minimize and/or prevent product loss. · Connect the suction of recovery pump to the liquid sample valve, pictured above as a bleed valve connection, on the liquid discharge line of the ISO · Connect the discharge of the recover pump to the vapor sample valve, picture above as a bleed connection valve, on the vapor equalization line of the ISO © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-3.6 Solstice® yf Refrigerant User Guide Collecting Samples from ISOs and Cylinders Table of Contents Part 3 - Page 85 · Open both sample valves · Verify flow of product, should be pulling product out of the liquid hoses from the liquid fill line on the storage, through the pump and back into the vapor side of the ISO. See diagram below for the proper valve arrangement - Valve C is Closed - Valve D is Open - Valve B is Closed - Valve A is Open · Open the valves for the recovery pump · Engage the pump to recover the product · Recover product to 3mbar of total pressure on the recovery pump · Close all valves · Disconnect all piping and equipment · Close all valves. Disconnect all piping and equipment Vapor Valves and Hoses Close Up A B C D Liquid Valves and Hoses Valves "A" and "C" are a part of the ISO. Valves "B" and "D" are attached to the Hoses. 3. CYLINDERS 3.1 Cylinders returned from end customer whose valves exhibit no evidence of tamper (i.e. the pilot plate of the CGA670 has not been damaged or removed) do not require analysis. 3.2 Tanks returned from Distributor no analysis required. 3.3 Tanks returned whose valves exhibit evidence of tamper (i.e. the pilot plate of the CGA670 has been damaged or removed) recover the 1234yf to a bulk tank and pull the cylinder pressure to less than 0.5 bar. If sampling is required a. Ensure site personnel are wearing all PPE required for handling 1234yf. b. Inspect the area to ensure the presence of only properly certified equipment. Remove any spark generating device from the immediate sampling area. c. Position the ISO in the designated area for safely handling R1234yf. If the area is not marked to handle 1234yf, STOP immediately and consult the onsite HS&E professional. d. Evacuate a clean sample cylinder; ensure to use proper sample cylinder preparation. e. Attach an adapter to the cylinder valve for the appropriate sample you are attempting to collect. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: NA-1234yf-3.6 Solstice® yf Refrigerant User Guide Collecting Samples from ISOs and Cylinders Table of Contents Part 3 - Page 86 · For Ton Cylinders the valve closest to the 12 o'clock position for vapor sample and closest to the 6 o'clock position for the liquid sample. · For all other cylinders, use the valve marked "vapor and liquid" for the proper sample. f. Under ideal conditions, the sampling hose used will be as short as possible to minimize the opportunity for introduction of Non-Condensable Gases and moisture into the line. g. Visually inspect sample cylinder hose to ensure that it is safe for use. Check for · Fraying · Gouges · Kinks · Any other defects h. Connect a sample cylinder to the adapter. i. Position a gas detector near the sample cylinder. j. Open the corresponding tank valve. k. Slightly open the hose connection at the sample cylinder to vent the hose. Vent until gas detector detects gas. l. Tighten the connection. m. Open the sample bottle valve to fill. n. Draw 30g vapor sample/600g liquid sample. o. Close the cylinder valve and the tank valve. p. Disconnect the sample hose and the sample adapter. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: NA-1234yf-3.6 Solstice® yf Refrigerant User Guide Connection of Sample Cylinder to Gas Chromatograph Table of Contents Part 3 - Page 87 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Visual Inspection for Appearance, Particulates and Solids in HFO Refrigerants Table of Contents Part 3 - Page 88 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Visual Inspection for Appearance, Particulates and Solids in HFO Refrigerants Material: Analyte: Technique: Specific Method: Supersedes: Also Required: HFO Refrigerants Appearance Particulates and Solids Visual Inspection HFO-Refrigerants-10 None None HFO-Refrigerants-10 PURPOSE This method describes the visual inspection of HFO Refrigerants. SCOPE This method is for use with virgin HFO Refrigerants. PRINCIPLE The HFO Refrigerant is inspected visually for any abnormal appearance, particulates and solids. SAFETY PRECAUTIONS 1. Consult the MSDS for each chemical used in this method prior to using the method for analysis. Follow the guidelines specified by the MSDS. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. SPECIAL APPARATUS AND REAGENTS Note: EQUIVALENTS MAY BE SUBSTITUTED. 1. 500 mL Pyrex Erlenmeyer Flask PROCEDURE 1. Fill flask with at least 100 mL of product directly from the bulk container, filled cylinder or storage tank of the lot that is being tested. 2. Visually check sample in flask for any foreign products in the material. This includes rust, dirt, oil, discoloration, etc. 3. Any amount of foreign material in the product will result in the lot/cylinder failing visual inspection. 4. The failing cylinder will need to be filtered and retested prior to approval. Written: Jim Tu Date: 04/25/2012 Revised: Jim Tu Date: 07/12/2012 Approved: John L. Welch © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Determination of Moisture in HFO Refrigerants Table of Contents Part 3 - Page 89 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Determination of Moisture in HFO Refrigerants HFO-Refrigerants-52 Material: Analyte: Technique: Specific Method: Supersedes: Also Required: HFO Refrigerants Moisture (Water vapor) Coulometric Karl Fisher Titrimetry HFO-Refrigerants-52 None None PURPOSE The purpose of this method is to determine the water in virgin HFO Refrigerants SCOPE This test method is for use with virgin HFO Refrigerants PRINCIPLE The moisture of HFO Refrigerants is determined by taking a known quantity of sample and titrating it with Karl Fisher reagent in a coulometric titrator to an electronic endpoint. APPLICABILITY This method is applicable to the determination of moisture as ug/g (ppm) in virgin HFO Refrigerants SAFETY PRECAUTIONS 1. HFO Refrigerants see MSDS. 2. HYDRANAL® - COULOMAT A and HYDRANAL® -COULAMAT C are proprietary, pyridine free, methanolic solutions for coulometric Karl Fisher titrators. See MSDS. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. SPECIAL APPARATUS AND REAGENTS Note: EQUIVALENTS MAY BE SUBSTITUTED. 1. Mitsubishi CA-06 Karl Fisher Titrator. 2. Sample cylinder, stainless steel, 125mL (Optional- Only used if sample has to be taken from a larger cylinder). 3. 1/8 inch stainless steel needle valve. 4. 1-1/4 inch to 1/8 inch reducing fitting. 5. 1/8 inch stainless steel tubing, approximately 9 inches. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Determination of Moisture in HFO Refrigerants Table of Contents Part 3 - Page 90 6. ¼ inch refrigeration fitting. 7. Heat gun. 8. HYDRANAL® -COULOMAT A #34807 anode solution, 500mL. Available from Fisher Scientific. 9. HYDRANAL® -COULOMAT CG #34840 cathode solution, 5ml. Available from Fisher Scientific. 10. HYDRANAL® Water Standard 0.10. PROCEDURE 1. Prepare the instrument according to the manufacturer's instructions. If the Mitsubishi CA-06 Karl Fisher titrator is used, add 5 mL of Coulomat CG to cathode's inner compartment. Add 100 mL of Coulomot A to the anode compartment of the cell. Turn instrument on. Press <Titr Current> and allow instrument to stabilize (< 0.05 ug/sec reading on the display). Set Titration parameters: Delay-5 min. Sens: 0.1 2. Check the instrument using PROCEDURE LQA1-18 and HYDRANAL® Water Standard 0.10. 3. Weigh the cylinder to the nearest 0.1 grams and record the weight as #1. 4. Attach needle assembly to cylinder. Make sure needle valve is in the closed position. Open main sample valve. 5. Install the needle into the titration cell solution making sure it does not touch either the anode or the cathode. 6. Heat the needle section of the needle assembly with the heat gun for a least 1 minute to remove water vapor. 7. Titrate away any water that came from the needle assembly by pressing the titration button. 8. When the display reads, "Stable," and the ug/sec reading is less than 0.1, press <START>. Continue applying heat to the needle and immediately introduce sample into the Karl Fisher vessel. Bubble sample at a rate of 1.5 to 1.8 liters per minute. As soon as sample starts entering the vessel, remove drying tube from the titration vessel to keep pressure from building up in the vessel. 9. Close sample valve after 4.0 minutes. Let the sample that is left in the needle assembly bubble into the vessel. Twenty to 30 grams of sample should be introduced. Replace the drying tube after the entire sample is in the vessel. 10. Remove the needle assembly by closing the needle valve and disconnecting it from the cylinder. Reweigh the sample cylinder to the nearest 0.1 grams and record as weight #2. 11. Record the Micrograms (ug) of moisture present in the sample. Calculate result. 12. Repeat steps 3 - 9 until three results agree within ± 10 percent of each other. Report the average of these three results. CALCULATION Moisture (ug/g) = Titration data (ug)* Wt.#1-Wt.#2 Report results to the nearest 0.1 ug/g. The minimum report is 2.5 ug/g * Titration data from instrument (Step 10). PRECISION AND ACCURACY A study conducted at the Buffalo Research Lab on a sample of HFC-134a with an average water content of 9.0 ug/g showed the standard deviation to be 1.48 ug/g with a relative standard deviation of 16.5 percent. A spiking recovery conduct with the above mentioned sample showed the recovery to be 97.2 percent when conducted around the samples at 20 ppm. Written: John L. Welch Date: 10/07/2008 Revision: Jim Tu Date: 07/122/2012 Approved: John L. Welch © 2013 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Determination of Acidity in HFO Refrigerants Table of Contents Part 3 - Page 91 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Determination of Acidity in HFO Refrigerants HFO-Refrigerants-2 Material: Analyte: Technique: Specific Method: Supersedes: Also Required: HFO Refrigerants Acidity Alkalimetric Titration HFO-Refrigerants-2 None None PURPOSE This method describes the determination of acidity in HFO Refrigerants. SCOPE This test method is for use with virgin HFO Refrigerants. PRINCIPAL The acidity of HFO Refrigerants is determined by bubbling a known quantity of sample through water. Any acidity imparted to the water is titrated with standardized sodium hydroxide. SAFETY PRECAUTIONS 1. Consult the MSDS for each chemical used in this method prior to using the method for analysis. Follow the guidelines specified by the MSDS. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. SPECIAL APPARATUS AND REAGENTS Note: EQUIVALENTS MAY BE SUBSTITUTED. 1. Buret, Micro, 5 mL with 0.01 mL graduations and a PTFE stopcock. 2. Gas dispersion tube, polyethylene. Bel-Art Products No.F 13691 or equivalent. 3. Evaporating dish, porcelain, 525 mL capacity or equivalent. 4. Water. All water used in the preparation of reagents and in the procedure is either distilled or deionized. 5. Sodium hydroxide, 0.1 N solution standardized. Prepare and standardize as directed in ASTM E200-91or obtain from Fisher, Cat. No. SS276-1 and standardize as directed in ASTM E200-91. 6. Sodium hydroxide 0.01 N solution. Pipet 100.0 mL of 0.1 N sodium hydroxide solution (Reagent from step 6) into a 1000-mL volumetric flask, dilute to the mark with water and mix. The final solution will have a normality 1/10 the normality of the step 6 reagent, or obtain from Fisher, Cat. No. SS284-1 and standardize as directed in ASTM E200-91. © 2013 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Determination of Acidity in HFO Refrigerants Table of Contents Part 3 - Page 92 7. Hydrochloric acid, approximately 0.1 N solution. Prepare and standardize as directed in ASTM E200-91or obtain from Fisher, Cat. No. SA54-4 and standardize as directed in ASTM E200-91. 8. Hydrochloric acid, approximately 0.01 N solution. Transfer 100.0 mL of the 1.0 N hydrochloric acid (Reagent from step 8) into a 1000-mL volumetric flask and dilute to the mark with water and mix. The final solution will have a normality 1/10 the normality of the step 8 reagent. An alternative is to obtain from Fisher, Cat. No. SA62-1. 9. Bromothymol blue indicator, 1.0 g/L solution. Dissolve 0.1 g of bromothymol blue, sodium salt, in 100mL of water. Store solution in a dropping bottle. PROCEDURE 1. Place approximately 150 mL of water in the gas dispersion tube or other suitable vessel. Add 6-8 drops of bromothymol blue indicator. 2. Weigh the sample cylinder to the nearest 0.1 gram and record the weight as A. Support the cylinder so that the sample will be drawn from the liquid phase. 3. Connect the sample cylinder and the outlet to the gas dispersion tube. Keep the connections as short as possible. 4. Adjust the water solution to the green endpoint with 0.01 N sodium hydroxide or 0.01 N Hydrochloric Acid as required (Note 1). 5. Bubble sample through the dispersion tube at a rate of 1-2 liters per minute until at least 100 grams of sample has been added. 6. A positive result for acidity will result in conversion of the indicator from blue-green to yellow (pH <7.6). A negative result for acidity will result in no change in the indicator color or a change to blue. (Note 2) 7. If positive result is detected, pour the contents of the dispersion tube into a 525-mL porcelain dish and titrate the solution to the green endpoint with 0.01 N sodium hydroxide from a 5-mL micro buret. 8. Reweigh the sample cylinder to the nearest 0.1 gram and record this weight as B. CALCULATION Acidity as ug/g HCl = mL NaOH x normality NaOH x 36,460 A-B Report results to the nearest 0.1 ug/g. The minimum reportable result shall be 0.5 ug/g NOTES 1. 2. The volume of NaOH or HCl used for this adjustment should not be included in the titration in procedure Step 4. If the solution remains green or turns blue after sample introduction, no acidity is present in the sample and the minimum reportable amount must be reported. PRECISION AND ACCURACY Studies are planned. Written: John L. Welch Date: 10/07/2008 Revision: Jim Tu Date: 07/12/2012 Approved: John L. Welch © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Determination of Non-Volatile Residue in HFO Refrigerants Table of Contents Part 3 - Page 93 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Determination of Non-Volatile Residue in HFO Refrigerants HFO-Refrigerants-6 Material: Analyte: Technique: Specific Method: Supersedes: Also Required: HFO Refrigerants Total Non-Volatile Residue Gravimetric HFO-Refrigerants-6 None None PURPOSE The purpose of this method is to determine the total residue in HFO Refrigerants. SCOPE This test method is for use with HFO Refrigerants. PRINCIPLE The total residue of HFO Refrigerants is determined by taking a known quantity of sample and evaporating it in a tared weighing dish, the residue is dried at 105°C, and reweighed. The increase in weight of the dish is the weight of total residue. APPLICABILITY This method is applicable to the determination of total residue as ug/g (ppm) in HFO Refrigerants. SAFETY PRECAUTIONS 1. HFO Refrigerants are compressed liquefied gas which becomes very cold as it volatilizes. See MSDS. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. SPECIAL APPARATUS AND REAGENTS Note: EQUIVALENTS MAY BE SUBSTITUTED. a. Sample cylinder with cylinder valve, 300-500 mL capacity. Aluminum, steel or stainless steel with adaptor to 1/8'' Swagelok fitting. b. Needle valve, 1/8'' Swagelok fitting, SS-SS2 or equivalents. c. 6'' (15 cm) 1/8'' Stainless steel tubing. d. Aluminum dishes, 110 mm diameter, Fisher Catalog 08-732-108, or equivalent. e. Heat gun. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Determination of Non-Volatile Residue in HFO Refrigerants Table of Contents Part 3 - Page 94 PROCEDURE 1. Collect about 100-150 grams of HFO Refrigerant in the clean, dry sample cylinder assembly from the liquid phase of a sample container. Weigh the assembly to 0.1g and record as (A). 2. Attach assembly needle valve to sampling cylinder and connect the valve outlet to the 1/8'' tubing. 3. Weigh one clean and dry aluminum dish to 0.0001g and record the tare weight of sample as (B). 4. Place the aluminum dish and sampling cylinder in a fume hood. Reverse the cylinder so the HFO Refrigerant is flowing out as liquid. Position the 1/8'' tubing outlet pointing to the center of the aluminum dish. Make sure the needle valve is set at minimum flow position. Open the cylinder valve slowly and allow the HFO Refrigerant flow into the aluminum dish. Adjust the needle valve so the liquid flow rate is about 20-50 mL/minute. Adjust flow rate carefully so HFO Refrigerant does not splash out from the aluminum dish and the 1/8'' tubing is not touching the HFO Refrigerant in the dish. Allow about 100 mL of HFO Refrigerant flow into aluminum dish. Close the cylinder valve. 5. Gently heat the needle valve and 1/8'' tubing with heat gun to make sure no residual HFO Refrigerant is between the needle valve and cylinder valve nor in the tubing. 6. Allow HFO Refrigerant to be evaporated from aluminum dish and place the dish in a 105°C oven for 30 minutes. 7. Allow the sampling to cool to room temperature and the moisture to evaporate from the cylinder surface. Disassemble the needle valve and 1/8'' tubing. Reweigh the sampling cylinder to 0.1g and record as (C). 8. Remove the dish from the oven, cool in a desiccator, reweigh the dishes to 0.0001g and record the final weights as (D). CALCULATION ug/g (ppm) Total Residue = [D-B] x 1,000,000 [C-A] Report result to the nearest 0.1 ug/g The minimum report is 1 ug/g Where: A = Gross weight of the sampling cylinder with liquid HFO Refrigerant, in grams B = Tare weight of the aluminum dish, in grams C = Final weight of the sampling cylinder, in grams D = Final weight of the aluminum dish, in grams PRECISION AND ACCURACY Studies are planned. Written: John L. Welch Date: 10/07/2008 Revision: Jim Tu Date: 07/12/2012 Date: 9/24/2012: Revised the procedure so the methylene chloride is not needed for this analysis. Date:11/15/2012: Correct Fisher catalog part number for aluminum dishes © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Determination of Chloride in HFO Refrigerants Table of Contents Part 3 - Page 95 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Determination of Chloride in HFO Refrigerants HFO-Refrigerants-4 Material: Analyte: Technique: Specific Method: Supersedes: Also Required: HFO Refrigerants Chloride Silver Nitrate Precipitation HFO-Refrigerants-4 None None PURPOSE This method describes the determination of chloride in HFO Refrigerants. SCOPE This test method is for use with virgin HFO Refrigerants. PRINCIPLE The chloride of HFO Refrigerants is determined by bubbling a known quantity of sample through silver nitrate/methanol solution. Any chloride will be precipitation as silver chloride where visual turbidity could be observed. SAFETY PRECAUTIONS 1. Consult the MSDS for each chemical used in this method prior to using the method for analysis. Follow the guidelines specified by the MSDS. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. SPECIAL APPARATUS AND REAGENTS Note: EQUIVALENTS MAY BE SUBSTITUTED. 1. Amber-glass bottle, 300 mL 2. Research grade silver nitrate (AgNO3) 3. Research grade anhydrous methanol (CH3OH) 4. Concentrated nitric acid (HNO3) PROCEDURE Prepare alcoholic silver nitrate solution as follows 1. Add 8 grams of silver nitrate to 200 mL of anhydrous methanol in an amber-glass bottle. 2. Place stopper in bottle and mix contents until no more of the silver nitrate dissolves. 3. Allow remaining solids to settle and use the clear, supernatant liquid, filtered, if necessary. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Determination of Chloride in HFO Refrigerants Table of Contents Part 3 - Page 96 Sample analysis 1. Weigh a clean evacuated sample cylinder to the nearest 0.1 grams and record the weight as (A). 2. Collect about 10 to 30 g of HFO Refrigerants liquid in the sample cylinder. Weigh the sample cylinder and record the weight as (B). 3. Calculated the volume of HFO Refrigerants in the sample cylinder using following equation. Volumne = (B - A) Density of 1234yf@ambient T 4. Add the same volume of anhydrous methanol to a 100-mL test tube. 5. For every 5 mL of anhydrous methanol add 3 drops of alcoholic silver nitrate solution to the test tube. Add one drop of nitric acid. Swirl until mixed. 6. Bubble all HFO Refrigerants sample into the test tube slowly. At the end, swirl until well mixed. 7. Observe results. a. If solution is clear, test is NEGATIVE for inorganic chlorides. Report as passes test. b. If solution is cloudy, test is POSITIVE for inorganic chlorides. Report as fails test. PRECISION AND ACCURACY The sensitivity of the chloride turbidity test using 5 mL of HFO Refrigerants in 5 mL of methanol containing three drops of saturated AgNO3 is approximately 3 ppm1. 1. AHRI Standard 700-95, appendix C. Written: Jim Tu, 04/25/2012 Revised: Jim Tu, 07/12/2012 Approved: John L. Welch © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Determination of HFO Refrigerants Assay Table of Contents Part 3 - Page 97 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Determination of HFO Refrigerants Assay HFO-Refrigerants-7 APPLICATION This method describes the determination of purity and impurity profile for HFO refrigerants production samples by gas chromatography. PRINCIPLE A representative sample is injected into a gas chromatograph using a 2.0 mL gas tight syringe. The components present are detected with a flame ionization detector, identified by retention times, then quantified using peak area. SAFETY PRECAUTIONS 1. HFO Refrigerants are a compressed liquefied gas which becomes very cold as it volatilizes. See MSDS. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. APPARATUS: Note: EQUIVALENTS MAY BE SUBSTITUTED 1. Gas chromatograph equipped with a flame ionization detector (FID), Perkin-Elmer 9000, or equivalent. 2. Electronic interface, Perkin-Elmer 900 or equivalent. Totalchrom software version 6 and a personal computer for data reduction and output. 3. 2.0 mL Gas tight syringe (sample size 1.0mL). 4. Column: 1percent SPTM-1000, 60/80 Carbopack B column, 24 ft, 1/8'', stainless steel column. (available through SUPELCO) INSTRUMENT CONDITIONS: Carrier Flow (helium) FID Hydrogen Flow FID Air Flow 450 mL/minute Injector Temperature Injection Volume Detector Temperature Sensitivity 20, -3 Oven Temperature Program: Initial Temperature Initial time Temperature Ramp Temperature 2 Hold Equilibration Time: 20 mL/minute (approx. 60 psi) 45 mL/minute 200°C 1.0mL 250°C 35°C 5 minutes 10°C/minute 200°C 10 minutes not less than 0.5 minute © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Determination of HFO Refrigerants Assay Table of Contents Part 3 - Page 98 STANDARDIZATION - VOLUME % The volume percent gas standards will be provided by Honeywell. SAMPLE PREPARATION A 1.0 mL gas sample of the vaporized liquid HFO Refrigerants from a tedlar bag is injected into a GC using a 2-mL gas tight syringe. PROCEDURE 1. After GC has stabilized, inject the HFO Refrigerants sample and collect chromatographic data using above conditions. 2. Calculate Volume percent based upon the data from the known standard Written by: Jim Tu 7/9/2012 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Determination of Non-Condensable Gases in HFO Refrigerants Table of Contents Part 3 - Page 99 Honeywell International, Inc. Performance Materials and Technologies Buffalo Research Laboratory Buffalo, New York 14210 716-827-6245 Determination of Non-Condensable Gases in HFO Refrigerants HFO-Refrigerants-8 Material: Analyte: Technique: Specific Method: Supersedes: Also Required: HFO Refrigerants Non-Condensable gases Gas Chromatography HFO-Refrigerants-8 None None PURPOSE The purpose of this method is to determine the non-condensable gases in virgin HFO Refrigerants as air. SCOPE This test method is for use with virgin HFO Refrigerants PRINCIPLE A measured volume of sample from the vapor phase of a sample cylinder is chromatographed with the area counts of the air peak being compared to those of standards similarly chromatographed. LIMITATIONS AND INTERFERENCES Care must be taken to inject only sample vapor. Injections of liquid phase will yield significantly lower results (non-condensable gases are only marginally soluble in HFO Refrigerants liquid, can damage the test gauge and overload the column. All compound identities are based on retention time and interfering compounds can be misidentified. APPLICABILITY This method is applicable to the gas chromatographic determination of non-condensable gases in virgin HFO Refrigerants. SAFETY PRECAUTIONS 1. HFO Refrigerants are a compressed liquefied gas which becomes very cold as it volatilizes. See MSDS. This method may involve the use of hazardous materials, operations and equipment. This method does not purport to address all of the safety problems associated with its use. It is the responsibility of whomever uses this method to establish appropriate safety practices and to determine the applicability of regulatory limitations prior to use. SPECIAL APPARATUS AND REAGENTS Note: EQUIVALENTS MAY BE SUBSTITUTED. a. Gas chromatography: Hewlett-Packard 5890, equipped with a thermal conductivity detector. b. Electronic integrator or data station: Perkin-Elmer Turbochrom. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Determination of Non-Condensable Gases in HFO Refrigerants Table of Contents Part 3 - Page 100 c. Gas chromatographic column: stainless steel 6 foot x 1/8 inch containing Porapak QS, 80-100 mesh. available from Supelco. d. Flow meter. e. Six-port gas sample valve port and loop, 1-mL from Valco. f. Gas handling manifold with vacuum test gauge (0-760mmHg), Ashcroft (302084SD02L15#A). g. Helium, chromatographic grade. h. Precision vacuum pump, Model DD-90 (0.1mmHg). Fisher Scientific Cat. No. 01-182-13. i. Certified gas mixture standard 1.5 volume percent air balanced helium. Available from specialty gas supply company. PROCEDURE Operating Conditions. Gas Chromatographic conditions Detector Carrier gas Injection Port Temp Detector Temp. Column Temp. Max. Column Temp. Sample Size Detector sensitivity TCD helium 20 mL/min. 175°C 220°C 35°C for 8 minutes, ramp temperature 20°C/minute to 200°C 250°C 1 mL loop containing 600mmHg of sample High Totalchrom conditions Delay Time Run Time Sampling Rate Range Autozero Bunch Factor Noise Threshold Area Threshold Width Ratio Valley-to-peak Ratio Peak Height Ratio Adjusted Height Ratio Valley Height Ratio 0.00 min. 14.5 min. 1.25 points/ second 0 OFF 1 points 1 uV 5.00 uV 0.100 0.100 5.000 4.000 3.000 COMPONENT INFORMATION Components retention time can be acquired by certified gas mixture standard. PROCEDURE 1. Using the appropriate regulator, connectors and tubing, attach the standard cylinder to the sample manifold in an upright position. 2. With the standard cylinder valve closed, evacuate the sampling manifold, loop and lines. 3. Close the vacuum valve, open the cylinder valve, and then purge the sample loop and lines with standard gas. 4. Close cylinder valve, and then open vacuum valve. 5. Repeat steps 2 - 4 two more times then evacuate. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Determination of Non-Condensable Gases in HFO Refrigerants Table of Contents Part 3 - Page 101 6. Turn off vacuum valve. Open the cylinder valve and charge 600 mm Hg of standard to the sample loop. Allow the pressure to stabilize, and then inject the standard. 7. Determine and record the area counts of the air peak. 8. Analyze the standard three times and determine the average area counts. 9. Remove standard cylinder and repeat steps 18 for the HFO Refrigerants sample cylinder. Analyze the sample in duplicate. CALCULATIONS 1. Calculate the Volume percent of air in the sample using the following equation Vol.% Air = Vol % Air Standard x Average Area counts Air in Sample Average Area counts of Air peak of the standard Total non-condensable = Vol. % Air Report results to the nearest 0.1%. Minimum reportable result is 0.1% Written: John L. Welch Date: 10/07/2008 Revision: Jim Tu Date: 07/12/2012 revise the column length to match AHRI Standard 700-2006, Appendix C and revise the total non-condensable as Air vol.% Date 9/24/2012 remove figure 1 which is no longer applicable. Approved: John L. Welch © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Scheme for Non-Condensable GC Injection Valve Table of Contents Part 3 - Page 102 Scheme for Non-Condensable GC Injection Valve Plug From Sampling Manifold 1 mL Sampling Loop To Non-Condensable GC Pack Column Helium Carrier 6 Way Sample Injection Valve © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Scheme for Non-Condensable GC Sampling Manifold Table of Contents Part 3 - Page 103 Scheme for Non-Condensable GC Sampling Manifold To Vacuum Pump Pressure Guage 0-780 mmHg P Vent Sample In Vent 1 psig Check Valve Plug To GC and Loop 1 mL Sampling Loop To Non-Condensable GC Pack Column Helium Carrier 6 Way Sample Injection Valve © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Process Map Distribution and QC Table of Contents Part 3 - Page 104 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Sample Size Summary Chart Table of Contents Part 3 - Page 105 Analyses Level Summary Sample type Required Analyses Frequency/ When Retain Sample? Incoming virgin bulk materials (ISO container) Level 1 Every container at receiving Yes Bulk storage and One per lot or intermediate Level 2 new materials No material cylinders are added ISO heel from OEL filling Level 2 One per lot No Day tank Level 1 As needed No Cylinder size 1L / liquid (Also the retained sample) 300ml-1L / gas 300ml-1L / liquid 300ml-1L / gas 300ml-1L / liquid 300ml-1L / gas 500ml-1L / liquid 300ml-1L / gas Analysis Assay, Moisture, Non-Volatile Residue, Acidity, Chlorides Non Condensable Gas Assay, Moisture, Non-Volatile Residue Non Condensable Gas Assay, Moisture, Non-Volatile Residue Non Condensable Gas Assay, Moisture, Non-Volatile Residue, Acidity, Chlorides Non Condensable Gas 1234yf sampling amount 1000g ~20g 250-280g ~20g 250-280g ~20g 350-380g ~20g Down Packaged containers less than 450 kg, 1000 lb but greater than 100 kg only Returned cylinders from OEM producers Returned cylinders from aftermarket customers with tamper evident seals HFO Refrigerants cylinders without tamper evident seals or cylinders with the tamper seal broken Level 3 Level 3 Level 2 +1 per lot +1 per lot +1 per lot 300ml-1L / liquid Assay, Moisture, No 300ml-1L / gas Non Condensable Gas 300ml-1L / liquid Assay, Moisture, No 300ml-1L / gas Non Condensable Gas 300ml-1L / liquid Assay, Moisture, Non-Volatile Residue No 300ml-1L / gas Non Condensable Gas 100-130g ~20g 100-130g ~20g 250-280g ~20g For down packaged containers smaller than 100 kg. Perform analyses from the containers directly Level 2 One per lot No Down packaged containers 450 kg, 1000 lb or greater Level 3 The rest of the lot No Bulk ISO shipment Level 1 Every ISO before shipment Yes 300ml-1L / liquid Assay, Moisture, Non-Volatile Residue 300ml-1L / gas Non Condensable Gas 300ml-1L / liquid Assay, Moisture 300ml-1L / gas Non Condensable Gas 1L / liquid (Also the Assay, Moisture, Non-Volatile Residue, retained sample) Acidity, Chlorides 300ml-1L / gas Non Condensable Gas 250-280g ~20g 100-130g ~20g 1000g ~20g Reworked material As needed Every container No Bulk heel for N/A return of the ISO As Requested by Honeywell to Honeywell Notes: 1) For ISO, bulk tanks and down packaged containers greater than 100 kg, use sampling cylinders for QA/QC analysis. 2) For down packaged containers smaller than 100 kg., perform analyses from the containers directly. 3) For ISO retain sample, the QA/QC analyses will be performed from the sampling cylinder and then the sampling cylinder becomes retained sample cylinder. Created by: Jim Tu 10/23/2012 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. 106 www.honeywell.com Table of Contents Part 4 Cylinder Specifications and Drawings 4 108 www.honeywell.com Solstice® yf Refrigerant User Guide 10 lb (4.5 kg) Non Returnable Cylinder Specification Table of Contents Document S-7863-YF Part 4 - Page 109 Regions: North America (ex Canada) Water Capacity: 15 lbs / 6 Liters Features: DOT39 Compliant CG-7 with a Pressure Relief Device for flammables Valve Outlet: CGA 166 Thread Pattern: 0.500 16 ACME 2G LH EXT (Left Handed Threads) © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide 10 lb (4.5 kg) Non Returnable Cylinder Specification Table of Contents Part 4 - Page 110 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Steel Cylinder, 15 lbs. water capacity, DOT-39/TC-39M JUG, Non-Returnable Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: S-7863-YF Page 1 of 3 2/18/13 New J color Rev 3 1234yf Danville 2. Detail Requirements: a. Capacity: 415 cu. in. (15.4 lbs. w.c.) minimum. b. Material: ASTM 620, Class I, drawing quality aluminum killed low carbon steel. c. Construction: Two drawn steel shells, circumferentially welded or brazed, with welded foot ring or extruded feet and steel valve body with welded carrying handle. Service Pressure: 260 psig Test Pressure: 325 psig All cylinders are to be designed, constructed, inspected, leak checked, burst-tested and date coded in accordance with DOT-39 /TC-39M specifications and CGA "Recommended Safe Practices for DOT-39 Fluorocarbon Steel Cylinders." Deviations from these DOT/TC specifications and CGA recommendations are not authorized. No modifications in the design of the cylinder, valve, relief device or unit carton may be made without prior authorization from Honeywell. d. Valve and Pressure Relief Device: Each cylinder to be equipped with a refillable valve and relief device as follows: Valve: Steel valve body with 0.500-16 ACME-2G-LH-EXT. (CGA 166) threaded outlet, welded into top center of cylinder. A solid stem of glass-filled nylon to be crimped into the valve body. Design of this valve is such that once the stem has been torqued closed, the non-refillable mechanism is activated, thereby preventing refill and allowing only discharge of contents © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: S-7863-YF Solstice® yf Refrigerant User Guide 10 lb (4.5 kg) Non Returnable Cylinder Specification Table of Contents Part 4 - Page 111 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Steel Cylinder, 15 lbs. water capacity, DOT-39/TC-39M JUG, Non-Returnable Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: S-7863-YF Page 2 of 3 2/18/13 New J color Rev 3 1234yf Danville 2. Detail Requirements: Pressure Relief Device: CGA CG-7 reseating relief device to be welded into upper shoulder of cylinder. Relief device operating range: 340-520 psig. Cylinders to be shipped with valves open and outlets sealed with push-on plastic caps. e. Tare Weight (approximate): 3 1/2 lbs. f. Dimensions (approximate): 7 1/2" O.D. x 14 1/2" O.H. g. Interior: Must be dry, clean and free of rust, oil, water and other foreign matter. h. Markings: Cylinders and unit cartons to be legibly date coded in accordance with CGA "Recommendations". Cylinder to bear required DOT-39/TC-39M markings. i. Painting & Printing: Cylinders to be thoroughly dried in preparation for painting. Paint to be uniformly applied to exterior surface, relief disc cup and handle. Paint color and silk screen decoration are as follows: Solstice 1234yf - Cylinder to be painted white, valve opening to be protected from overspray. A contrasting 2" wide red [Pantone 485C] band is to be painted around the circumference of the cylinder positioned just below the cylinder shoulder radius at the top of the cylinder, per SAE J2844, AHRI Guideline N-2008: 4.8. Silk screen to be centered with valve outlet. Silk screen and paint must be thoroughly dried before cylinder is packed into shipper © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: S-7863-YF Solstice® yf Refrigerant User Guide 10 lb (4.5 kg) Non Returnable Cylinder Specification Table of Contents Part 4 - Page 112 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Steel Cylinder, 15 lbs. water capacity, DOT-39/TC-39M JUG, Non-Returnable Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: S-7863-YF Page 3 of 3 2/18/13 New J color Rev 3 1234yf Danville j. Carton: Each cylinder to be packed into a single unit carton, positioned so that the valve outlet points toward the die cut circular hole. Top flaps to be folded shut; bottom flaps to be stapled or glued. Cylinders/cartons to be unitized for shipment on four-way entry wooden pallets, measuring 36" x 48". Cartons, to be unprinted natural kraft and constructed to Honeywell's specification no. S-6805-8. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: S-7863-YF Solstice® yf Refrigerant User Guide 25 lb (11.3 kg) Non Returnable Cylinder Specification Table of Contents Doc Number: S-1234-YF Part 4 - Page 113 Regions: North America (ex Canada) Water Capacity: 29.7 lbs / 13.6 Liters Features: DOT39 Compliant CG-7 with a Pressure Relief Device for flammables Valve Outlet: CGA 166 Thread Pattern: 0.500 16 ACME 2G LH EXT (Left Handed Threads) © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide 25 lb (11.3 kg) Non Returnable Cylinder Specification Table of Contents Part 4 - Page 114 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: 30 lb. Non-Returnable, Non-Refillable, Steel Cylinder (JUG) (9½ inch) Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: S-1234-YF Page 1 of 2 2/18/13 J color 1234yf Rev 3 2. Detail Requirements: a. Capacity: 840 cu. in. (30.4 lbs. w.c.) nominal b. Material: ASTM 620, Class I, drawing quality aluminum killed low carbon steel. c. Construction: Two drawn steel shells, circumferentially welded or brazed, with welded foot ring or extruded feet and steel valve body with welded carrying handle. Service Pressure: 260 psig Test Pressure: 325 psig All cylinders are to be designed, constructed, inspected, leak checked, burst-tested and date coded in accordance with DOT-39 specifications and CGA "Recommended Safe Practices for DOT-39 Fluorocarbon Steel Cylinders." Deviations from these DOT specifications and CGA recommendations are not authorized. No modifications in the design of the cylinder, valve, pressure relief device or unit carton may be made without prior authorization from Honeywell. d. Valve and Pressure Relief Device: Each cylinder to be equipped with a non-refillable valve and pressure relief device as follows: Valve: Steel valve body with .500-16 ACME-2G-LH-EXT. (CGA 166) threaded outlet, welded into top center of cylinder. A solid stem of glass-filled nylon to be crimped into the valve body. Stem must be in the open position to allow for evacuation and filling of the cylinder. Design of this valve is such that once the stem has been torqued closed, the non-refillable mechanism is activated, thereby preventing refill and allowing only discharge of contents from the cylinder. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: S-1234-YF Solstice® yf Refrigerant User Guide 25 lb (11.3 kg) Non Returnable Cylinder Specification Table of Contents Part 4 - Page 115 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: 30 lb. Non-Returnable, Non-Refillable, Steel Cylinder (JUG) (9½ inch) Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: S-1234-YF Page 1 of 2 2/18/13 J color 1234yf Rev 3 2. Detail Requirements: Pressure Relief Device: CGA CG-7 reseating relief device to be welded into upper shoulder of cylinder. Relief device operating range: 340-520 psig. Cylinders to be shipped with valves open and outlets sealed with push-on plastic caps. e. Tare Weight (approximate): 6 lbs. f. Dimensions (approximate): 9½"O.D. x 16 ½" O.H. g. Interior: Must be dry, clean and free of rust, oil, water and other foreign matter. h. Markings: Cylinders and unit cartons to be legibly date coded in accordance with CGA "Recommendations". Silk screen to bear required DOT-39 markings i. Painting & Printing: Cylinders to be thoroughly dried in preparation for painting. Paint to be uniformly applied to exterior surface, relief disc cup and handle. Paint color and silk screen decoration are as follows: Solstice 1234YF- Cylinder to be painted white, valve opening to be protected from overspray. A contrasting 2" wide red [Pantone 485C] band is to be painted around the circumference of the cylinder positioned just below the cylinder shoulder radius at the top of the cylinder, per SAE J2844, AHRI Guideline N-2008: 4.8 Silk screen to be centered with valve outlet Silk screen and paint must be thoroughly dried before cylinder is packed into shipper carton. j. Carton: Each cylinder to be packed into a single unit carton, positioned so that the valve outlet points toward the die cut circular hole. Scored top flaps to be folded inward, securing the handles. Top flaps to be stapled twice or glued. Bottom flaps may be stapled or glued. Cylinders/cartons to be unitized for shipment on four-way entry wooden pallets, measuring 36" x 48", or 38" x 48", in accordance with instructions from receiving location. Cartons are to be constructed to Honeywell specification no. S-6807-13. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: S-1234-YF Solstice® yf Refrigerant User Guide 10 lb (4.5 kg) Returnable Cylinder Specification Table of Contents Doc Number: M-8110-yf Part 4 - Page 116 Regions: North America Water Capacity: 15 lbs / 6 Liters Features: Light weight and plastic handles for easy transport, dual phase valve for gas or liquid discharge Valve Outlet: CGA 166 Thread Pattern: 0.500 16 ACME 2G LH EXT (Left Handed Threads) © 2014y Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide 10 lb (4.5 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 117 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 15.5 lbs. Water Capacity DOT 4BA400/TC/EN Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8110-YF Page 1 of 2 2/18/13 8110-YF Rev 1 J color Solstice® 1234yf 2. Detail Requirements: a. Capacity: 15.5 lbs. water, minimum. b. Material: Open hearth or electric steel of with minimum wall thickness of .082". Compositions of steel to be in accordance with DOT 4BA/TC/EN specifications. c. Construction: Two drawn steel shells circumferentially welded, with welded foot ring and collar. Construction to comply with DOT 4BA specifications for a service pressure of 400 psig. and Transport Canada (TC) 4BA specifications for a service pressure of 400 psig d. Opening: Top head to have ¾"-14 NGT opening. e. Valve and Pressure Relief Device: Option A: Neriki air-activated liquid/vapor valve #DCU-2-018-1A with .500-16ACME-LH-EXT (CGA 166) outlet and replaceable pressure relief valve #3EA-003-2 installed. Valve inlet CGA ¾-14NGT Taper 1/16 The start-to-discharge pressure of the relief valve must be between 600 and 800 psig; the flow rating pressure shall not exceed 800 psig. Each valve to be assembled with a securely clamped polyethylene dip tube extending to the base of the cylinder. Valve to be installed such that the outlet faces the handle opening. f. Tare Weight: 11. lbs. (approximate) with valve. g. Dimensions: (Approximately) 7 ½" O.D. x 14 3/4" from bottom of foot ring to top of collar. h. Interior: Must not contain in excess of 1.5 grams of particulate matter (rust, slag, scale and other solids) and must show no evidence of moisture or oil © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: M-8110-yf Solstice® yf Refrigerant User Guide 10 lb (4.5 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 118 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 15.5 lbs. Water Capacity DOT 4BA400/TC/EN Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8110-YF Page 2 of 2 2/18/13 8110-YF Rev 1 J color Solstice® Refrigerants 1234yf 2. Detail Requirements: i. Markings: Collar to bear required DOT 4BA 400 markings and the following: - "Honeywell" - Tare weight including valve - Water capacity j. Painting: Solstice 1234YF- Cylinder to be painted white, valve opening to be protected from overspray. A contrasting 2" wide red [Pantone 485C] band is to be painted around the circumference of the cylinder positioned just below the cylinder shoulder radius at the top of the cylinder, per SAE J2844, AHRI Guideline N-2008: 4.8. k. Test Reports: Copies of complete cylinder test reports are to be supplied to Honeywell Fluorine Products 101 Columbia Turnpike Morristown, NJ. 07962 Attn: Insert the Name of the buyer from the PO Cylinder manufacturer will also maintain copies of these reports. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: M-8110-yf Solstice® yf Refrigerant User Guide 25 lb (11.3 kg) Returnable Cylinder Specification Table of Contents Doc Number: M-8100-yf Part 4 - Page 119 Regions: North America Water Capacity: 29.7 lbs / 13.6 Liters Features: Light weight and plastic handles for easy transport, dual phase valve for gas or liquid discharge Valve Outlet: CGA 166 Thread Pattern: 0.500 16 ACME 2G LH EXT (Left Handed Threads) © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide 25 lb (11.3 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 120 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 30.0 lbs. water capacity DOT 4BA400/TC4BAM28/EN Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8100yf 2/18/13 New J color 1234yf Danville Page 1 of 2 Rev 1 2. Detail Requirements: a. Capacity: 30.0 lbs. water b. Material: Open hearth or electric steel with minimum wall thickness of 0.090 in. c. Construction: To comply with DOT/TC 4BA/EN specifications for a service pressure of 400 psig. Collar to be heavy gauge 270 degree style with a 1/4" hole drilled opposite the opening; foot ring to be heavy gauge. Foot rings and collars to be nestable for stacking. d. Opening: Top spud to have 3/4 in.-14NGT opening. e. Valve and Pressure Relief Device: Option A: Neriki air-activated liquid/vapor valve #DCU-2-018-1A with .500-16ACME-LH-EXT (CGA 166) outlet and replaceable pressure relief valve #3EA-003-2 installed. Valve inlet CGA ¾-14NGT Taper 1/16 The start-to-discharge pressure of the relief valve must be between 600 and 800 psig; the flow rating pressure shall not exceed 800 psig. Each valve to be assembled with a securely clamped polyethylene dip tube extending to the base of the cylinder. Valve to be installed such that the outlet faces the handle opening. f. Tare Weight: Approximately 18.8 lbs. g. Dimensions: 9 in. diameter x 20 in. height. h. Interior: Must be dry, clean, and free of rust, oil, water and other foreign matter. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: M-8100-yf Solstice® yf Refrigerant User Guide 25 lb (11.3 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 121 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 30.0 lbs. water capacity DOT 4BA400/TC4BAM28/EN Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8100yf 2/18/13 New J color 1234yf Danville Page 2 of 2 Rev 1 2. Detail Requirements: i. Markings: Collar to bear required DOT/TC 4BA/EN markings and manufacturer's registered symbol and serial number. Purchaser's identification to be included as follows: "Honeywell" Tare weight of cylinder, including valve, to be stamped on collar. j. Painting: Solstice® 1234YF- Cylinder to be painted white, valve opening to be protected from overspray. A contrasting 2" wide red [Pantone 485C] band is to be painted around the circumference of the cylinder positioned just below the cylinder shoulder radius at the top of the cylinder, per SAE J2844, AHRI Guideline N-2008: 4.8. k. Test Reports: Cylinder test reports are to be sent to: Honeywell Fluorine Products 101 Columbia Road Morristown, NJ. 07962 ATTN: The Buyers Name associated with the PO © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: M-8100-yf Solstice® yf Refrigerant User Guide 100 lb (45.3 kg) Returnable Cylinder Specification Table of Contents Doc Number: M-8120-yf Part 4 - Page 122 Regions: North America Water Capacity: 123 lbs / 55.8 Liters Features: Manageable size cylinders in tight spaces and good capacity for lower production environments Valve Outlet: CGA 670 Dual Phase Thread Pattern: 1.030 14 NGO LH EXT (Left Handed Threads) © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide 100 lb (45.3 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 123 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 123 lbs. Water Capacity DOT 4BW400/TC4BWM27/EN Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8120-YF Page 1 of 2 2/18/13 New Rev 1 J color 1234yf 2. Detail Requirements: a. Capacity: 123 lbs. water, minimum. b. Material: Open hearth or electric steel of prescribed analysis. c. Construction: Longitudinally welded shell with ellipsoidal head welded to each end, with welded foot ring and 3 1/8"-11 TPI spud welded on top for valve cover. Construction to comply with U.S. Department of Transportation (DOT) and Transport Canada (TC) 4BW specifications for a service pressure of 260 psig. d. Opening: Top spud to have ¾"-14 NGT opening. Cylinders to be equipped either with a specified valve and dip tube or a steel plug, installed wrench tight to prevent accumulation of moisture and contamination. Cylinders to be supplied with valve covers. e. Valve and Pressure Relief Device: Option A: Neriki air-activated liquid/vapor valve #D-7CU-502-2 with.1.030-14NGO--LH-EXT (CGA 670) outlet and replaceable pressure relief valve #3EA-003-2 installed. Valve inlet CGA ¾-14NGT Taper 1/16 The start-to-discharge pressure of the relief valve must be between 600 and 800 psig; the flow rating pressure shall not exceed 800 psig. Each valve to be assembled with a securely clamped polyethylene dip tube extending to the base of the cylinder. Valve to be installed such that the outlet faces the handle opening. f. Tare Weight: 65 lbs. (approximate) with valve and cap. g. Dimensions: (Approximate) 10" O.D. x 48" from bottom of foot ring to top face of threaded opening. h. Interior: Must not contain in excess of 1.5 grams of particulate matter (rust, slag, scale and other solids) and must show no evidence of moisture or oil. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: M-8120-yf Solstice® yf Refrigerant User Guide 100 lb (45.3 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 124 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 123 lbs. Water Capacity DOT 4BW400/TC4BWM27/EN Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8120-YF Page 2 of 2 2/18/13 New Rev 1 J color 1234yf 2. Detail Requirements: i. Markings: Shoulder to bear required DOT/TC 4BW/EN markings and manufacturer's registered symbol and serial number. Owner's registered symbol to be stamped on shoulder, opposite the DOT/TC markings, as follows: "Honeywell" Tare weight of cylinder (include 1¾ lbs. for valve) to be stamped on shoulder. j. Painting: Solstice® 1234YF- Cylinder to be painted white, valve opening to be protected from overspray. A contrasting 2" wide red [Pantone 485C] band is to be painted around the circumference of the cylinder positioned just below the cylinder shoulder radius at the top of the cylinder, per SAE J2844, AHRI Guideline N-2008: 4.8. k. Test Reports: Cylinder test reports are to be sent to: Honeywell Fluorine Products 101 Columbia Road Morristown, NJ. 07962 Attn: The purchasing contact indicated on the PO © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: M-8120-yf Solstice® yf Refrigerant User Guide 950 lb (430 kg) Returnable Cylinder Specification Table of Contents Doc Number: M-7863-yf Part 4 - Page 125 Regions: North America Water Capacity: 1000 lbs Features: Easy to maneuver with a fort truck contains enough capacity for higher production environments Valve Outlet: CGA 670 Single Outlet (x2) Thread Pattern: 1.030 14 NGO LH EXT (Left Handed Threads) © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide 950 lb (430 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 126 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 1000 lbs. Water Capacity DOT 4BW400/TC4BWM27 Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-7863yf 2/18/13 New J color 1234yf Danville Page 1 of 2 Rev 1 2. Detail Requirements: a. Capacity: 1000 lbs. water, nominal b. Material: Open hearth or electric steel of prescribed analysis. c. Construction: Longitudinally welded shell with ellipsoidal head welded to each end, mounted on 4-way entry pallet skid. Construction to comply with U.S. Department of Transportation (DOT) and Transport Canada (TC) 4BW specifications for a service pressure of 400 psig. d. Openings: Top head to have three (3) 3/4" x 14 NPT openings and two (2) 1" x 11½ NPT openings. Bottom head to have one (1) 3/4" x 14 NPT opening. e. Pressure Relief Device & Valves: To be equipped with two (2) spring loaded relief valve(s), sized in accordance with CGA Pamphlet S-1.1 for use in refrigerant 1234yf and assembled with refrigerant grade neoprene seat. Two (2) Neriki valves, one (with red handle) to be assembled with polyethylene dip tube, to be installed in 3/4" openings in top head. The valves should have a CGA670 outlet connection with a thread pattern of 1.030-14 NGO-LH-EXT (Left Handed Threads). Unused holes to be plugged. f. Tare Weight: 500 lbs. (approximate) g. Dimensions: 30" O.D. x 60" H (approximate) h. Interior: Must be dry, clean, and free of rust, oil, water and other foreign matter. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: M-7863-yf Solstice® yf Refrigerant User Guide 950 lb (430 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 127 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Returnable Steel Cylinder 1000 lbs. Water Capacity DOT 4BW400/TC4BWM27 Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-7863yf 2/18/13 New J color 1234yf Danville Page 2 of 2 Rev 1 2. Detail Requirements: i. Markings: Collar to bear required DOT-4BW/ TC markings and manufacturer's registered symbol and serial number. Purchaser identification to be included as follows: "Honeywell" Tare weight of cylinder including valves to be included on collar. j. Painting: Solstice 1234YF- Cylinder to be painted white, valve opening to be protected from overspray. A contrasting 2" wide red [Pantone 485C] band is to be painted around the circumference of the cylinder positioned just below the cylinder shoulder radius at the top of the cylinder, per SAE J2844, AHRI Guideline N-2008: 4.8. k. Test Reports: Copies of cylinder test reports to be supplied to: Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962. Attention: To the buyer issuing the PO Cylinder manufacturer will also maintain copies of these reports. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: M-7863-yf Solstice® yf Refrigerant User Guide 1750 lbs (794 kg) Returnable Cylinder Specification Table of Contents Doc Number: S-7816-yf Part 4 - Page 128 Regions: North America Water Capacity: 1600 lbs Features: Utilized as a mini-Bulk tank, enough capacity for high production, requires special equipment to maneuver Valve Outlet: CGA 670, Single Outlet (x2) Thread Pattern: 1.030-14NGO-LH-EX © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide 1750 lbs (794 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 129 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: "Ton Cylinder" Multi Unit Tank Car Tank DOT-110A800W Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: S-7816yf 2/18/13 New J color 1234yf Danville Page 1 of 2 Rev 1 2. Detail Requirements: a. Capacity: 1600 lbs. water, minimum 1674 lbs. water, average b. Material: Carbon steel plate. Composition and thickness of steel to be in accordance with DOT-110A800W specification. c. Construction: Cylindrical steel shell with fusion-welded heads formed concave to pressure. Construction to comply with DOT-110A800W specification. d. Openings: Each head to have three equally spaced ¾"-14 NGT couplings (for pressure relief devices). One head to have two ¾"-14 NGT valve couplings spaced 4" apart on center line. Each valve coupling to be connected to a ¾" schedule 80 eduction pipe. Two valves, Neriki # D-7CU-602-1A , to be installed. e. Pressure Relief Device & Valves: Tank to be equipped with five fusible plugs. Neriki # S-1-010-1, with two installed on valve end and three on opposite end. One relief valve, Neriki # S-1-009-1, to be installed on valve end. f. Tare Weight: (average) 1425 lbs. (complete with fittings and bonnet) g. Dimensions: 30 5/16" O. D. x 81 ½" + ½" ¾" L. h. Interior: Must be dry, clean, and free of rust, oil, water and other foreign matter. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: S-7816-yf Solstice® yf Refrigerant User Guide 1750 lbs (794 kg) Returnable Cylinder Specification Table of Contents Part 4 - Page 130 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: "Ton Cylinder" Multi Unit Tank Car Tank DOT-110A800W Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: S-7816yf 2/18/13 New J color 1234yf Danville Page 2 of 2 Rev 1 2. Detail Requirements: i. Markings: Tank is to be marked on the valve end chime in accordance with 49CFR, Section 179.30018(a). Marking to include owner's registered symbol, as follows, and tare weight. "Honeywell" Brass owner's nameplate to be stamped with the following information: HONEYWELL--MORRISTOWN, NEW JERSEY (circumferentially in ¼" letters) DOT-110A800W (5/16" letters) SOLSTICE® (1/2" letters) SERIAL (1/4" letters) TEST DATE (1/4" letters) TARE LBS. (1/4" letters) j. Painting: Solstice® 1234YF- Cylinder to be painted white, valve opening to be protected from overspray. A contrasting 2" wide red [Pantone 485C] band is to be painted around the circumference of the cylinder positioned just below the cylinder shoulder radius at the top of the cylinder, per SAE J2844, AHRI Guideline N-2008: 4.8. k. Test Reports: Copies of complete test reports are to be supplied to Honeywell, Morristown, NJ office. Attn: To the buyer issuing the PO Tank manufacturer will also maintain copies of these reports. l. Miscellaneous: Tank to be shipped with all fittings and protective bonnet installed. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: S-7816-yf Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 131 Delivery Quantity: 33,000 lbs / 15,000 kg Water Capacity: 6,470 gals / 24,500 liters Features: Bulk Deliveries for OEM facilities Quest Unloading Skid Pump © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 132 Tank container full specification GENERAL Type ISO Type Length Width Regulation Manufacturer Date of manufacturer TANK VESSEL Max. allowable working pressure Vacuum pressure Test pressure RID design pressure Inside diameter Bafles FRAME Frame type Stacking FITTINGS Manhole position Manhole nominal diameter Number of closures Closure type Manhole gasket Spill box Callibration card Guaging fitting EURU504500-8 IM5 1 CC 20' 8' New GASCON 11-Oct-2011 Group # of compartments Height T-Code Nominal capacity Maximum gross weight Tare weight 27.50 bar 1.00 bar 36.30 bar 2386 mm Yes Material Design temperature Design code Internal lining Beam tank 170,000 kgs Walkway Collapsible handrall Grip lift At the rear 500 mm - 20 in 24 Bolt PTFE with SS core Yes with lids No No Gas tank 1 8' 6" T50 24,500 l 34,000 kg 7,670 kg CS- P460 NL1 modified 50 °C ASME sect. Vill div.2 - Stamp U2 Zinc No No No © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 133 Tank container full specification DISCHARGE Discharge Type Liquid Line Position Internal valve type Internal valve diameter Internal valve brand Valve type Valve diameter Valve brand Coupling type Coupling diameter Closure type Gasket between valves SAFETY DEVICES Safety devices Breather Relief valve 1 / Brand Relief valve 1 / Type Relief valve 1 / Diameter Relief valve 1 / Settings Flame trap Manometer Rupture disc 1 / Brand Rupture disc 1/Type Diameter Settings EURU504500-8 Bottom only Quantity: 1 At the rear Stainless steel 50 mm - 2 in Fort Vale Ball-SS 50 mm - 2 in Fort Vale ACME 82.55 mm - 3.25 in Cap 3"1/4 PTFE with SS core Gas Line Position Internal valve type Internal valve diameter Internal valve brand Valve type Valve diameter Valve brand Coupling type Coupling diameter Closure type Gasket between valves Quantity: 1 At the rear Stainless steel 50 mm - 2 in Fort Vale Ball-SS 50 mm - 2 in Fort Vale ACME 44.45 mm - 1.75 in Cap 1"3/4 PTFE with SS core 1 SRV + 1 BD in series No Protection cover No Fort Vale Stainless steel 80 mm - 3 in 27.50 bar - 399 psi Yes Flame trap No 0/40 bar - 0/580 psi Continental Disc SS 316L 80 mm - 3 in 30.25 bar - 438.00 psi © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. INSULATION Composition Insulation thickness APPROVALS CSC IMDG RID / ADR US DOT / CFR49 Exemption UIC TEST DATES CSC inspection Hydraulic test Air test Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 134 Tank container full specification EURU504500-8 Cladding Sunshield Not specified Yes Yes Yes Yes UN + U Stamp 2 SP 14301 Yes AAR600 FRA CTC Japanese fire approval MITI SQLO TPED Yes No Yes No Hydro tested Yes Yes Last 11 Oct 2011 11 Oct 2011 11 Oct 2011 Next 11 Oct 2016 11 Oct 2016 11 Apr 2014 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 135 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 136 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 137 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 138 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 139 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 140 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide ISO Container Specification Table of Contents Part 4 - Page 141 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide 25 lb (10 kg) Reclaim Cylinder Specification Table of Contents Doc Number: M-8005 Part 4 - Page 142 Regions: North America Delivery Quantity: Each (Delivered As Empties) Water Capacity: 27.5 lbs / 6 liters Features: Light Weight, Ergonomic Design, Dual Handle, CGA 166 Dual Outlet Valve Valve Outlet: CGA 166 Thread Pattern: 0.500 16 ACME 2G LH EXT (Left Handed Threads) © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide 25 lb (10 kg) Reclaim Cylinder Specification Table of Contents Part 4 - Page 143 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Recovered Refrigerant (Composite-metal) Returnable Steel Cylinder 30 lb. Water Capacity Nominal DOT SP14457 2. Detail Requirements: Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8005 Page 1 of 2 7/19/12 New J color 1234yf (Reclaim) RECOVERY CYLINDER Danville a. Capacity: 27.5 lbs. water actual (12.5 Liter/27.5# W.C.) b. Material: Steel Liner, Reinforced with polypropylene fiber winding pressure vessel, encased in HDPE shell. c. Construction: To comply with DOT SP 14457 specifications for service pressure of 400 psig. Must be nestable for stacking. Reference drawings: Amtrol/Alfa Numbers H013-04-00 d. Opening: Top spud to have 3/4 in. NPT opening. e. Valve and Pressure Relief Device: Dual Handle/dual port Cavagna (Omega) Model number for 400 psi rated cylinders is7601900356. The valve is to be equipped with a burst disc set to relieve at 620 psig (=40 psig or -40 psig) with CGA 166 (1/4" SAE Flare LH) outlets. Each valve to be assembled with a securely clamped polyethylene dip tube extending to the base of the cylinder. Valve to be installed such that the outlet faces the handle opening. Omega Drawing Number 1201101645 f. Tare Weight: Approximately 11 lbs. (5 kg) g. Dimensions: 12.2 in. (310 mm) diameter x 15.9 in. (404 mm) height. h. Interior: Must be dry, clean, and free of rust, oil, water and other foreign matter. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: M-8005 Solstice® yf Refrigerant User Guide 25 lb (10 kg) Reclaim Cylinder Specification Table of Contents Part 4 - Page 144 Honeywell Fluorine Products P.O. Box 1053 Morristown, NJ 07962-1053 Container Purchase Specifications 1. Type: Recovered Refrigerant (Composite-metal) Returnable Steel Cylinder 30 lb. Water Capacity Nominal DOT SP14457 2. Detail Requirements: Spec No.: Date: Supersedes Spec. No.: Change: Product: Location: M-8005 Page 2 of 2 7/19/12 New J color 1234yf (Reclaim) RECOVERY CYLINDER Danville i. Markings: Collar to bear required DOT/TC 4BA markings and manufacturer's registered symbol and serial number. Purchaser's identification to be included as follows: Tare Plate: Gross mass of complete cylinder, last permissible retest date. Bottom Plate: DOT SP14457, Registration symbol and serial number. Blank area for retest date, service pressure, water capacity, manufacture date, mass of cylinder, plus jacket without a valve. j. Coloring: Base and Handle inserts to be Pantone 485C. Remainder of cylinder to be "grey" k. Test Reports: Cylinder test reports are to be sent to: Honeywell Fluorine Products 101 Columbia Road Morristown, NJ. 07962 ATTN: The issuer of the PO © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: M-8005 Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 145 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 146 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 147 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 148 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 149 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 150 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 151 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 152 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Cylinder Labels and Tags Table of Contents Part 4 - Page 153 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. 154 www.honeywell.com Table of Contents Part 5 Valve Specifications and Drawings 5 156 www.honeywell.com Solstice® yf Refrigerant User Guide CGA 166 Valve Specification Table of Contents Part 5 - Page 157 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide CGA 166 Valve Specification Cylinder and Hose Connections SolsticeTM yf Refrigerant 0.500 16 ACME 2G LH CGA 166 Table of Contents Part 5 - Page 158 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide CGA 166 Valve Specification Cylinder and Hose Connections SolsticeTM yf Refrigerant 0.5 16 ACME LH fitting for SAE J2844 Table of Contents Part 5 - Page 159 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide CGA 166 Valve Specification Cylinder and Hose Connections SolsticeTM yf Refrigerant 0.5 16 ACME LH fitting for SAE J2844 Table of Contents Part 5 - Page 160 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide CGA 166 Valve Specification Cylinder and Hose Connections SolsticeTM yf Refrigerant 0.5 16 ACME LH fitting for SAE J2844 Table of Contents Part 5 - Page 161 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide CGA 670 Valve Specification Table of Contents Part 5 - Page 162 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide CGA 670 Single Phase Valve Specification Table of Contents Part 5 - Page 163 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 164 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 165 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 166 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 167 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 168 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 169 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 170 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 171 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 172 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Epsilon Valves (Skid Pump Connections) Table of Contents Part 5 - Page 173 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 174 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 175 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 176 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 177 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 178 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 179 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 180 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 181 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 182 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 183 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 184 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Fitting of Valves to Gas Cylinders (ISO Standard 13341) Table of Contents Part 5 - Page 185 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. 186 www.honeywell.com Table of Contents Part 6 Regulatory Information 6 188 www.honeywell.com Solstice® yf Refrigerant User Guide Transportation Regulation of Hazardous Materials Transportation regulation of hazardous materials For information on transportation of hazardous materials by highway, rail, vessel, and air, please contact Travis Williams. Travis Williams Honeywell International Inc Conversion Manager (225) 405-1865 travis.williams2@honeywell.com Table of Contents Part 6 - Page 189 To download The Code of Federal Regulation (CFR) please visit the US government website http://www.phmsa.dot.gov/hazmat/regs. The regulations for gases are not all located in one section. The Hazardous Material Regulation (HMR) are in Subchapter C, Parts 171, 172, 173, 174, 175, 176, 177, and 178 non-bulk packaging. Parts 172, 173, and 178 are the most referenced. © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Table of Contents US EPA SNAP Final Rule Doc Number: HFO-1234yf EPA-HQ-OAR-2008-0664 2011-6268 Part 6 - Page 190 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 191 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 192 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 193 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 194 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 195 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 196 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 197 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 198 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 199 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 200 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 201 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 202 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 203 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide US EPA SNAP Final Rule EPA-HQ-OAR-2008-0664 2011-6268 Table of Contents Part 6 - Page 204 © 2014 by Honeywell International Inc. All rights reserved. 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No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Doc Number: HFO-1234yf Solstice® yf Refrigerant User Guide CAFE Regulatory Announcement Table of Contents Part 6 - Page 223 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide CAFE Regulatory Announcement Table of Contents Part 6 - Page 224 © 2014by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide CAFE Regulatory Announcement Table of Contents Part 6 - Page 225 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. 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No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Table of Contents Part 7 Auxiliary Equipment Providers 7 The information provided herein is for informational purposes only and Honeywell does not endorse, guarantee, warrant or recommend any of the products or services offered by third parties. 234 www.honeywell.com Solstice® yf Refrigerant User Guide Auxiliary Equipment and Suppliers Table of Contents Doc Number: 1234yf Part 7 - Page 235 CATEGORY LISTING Hoses and Connections CPS Gauges and Fittings Errecom Hoses Mastercool Gauge Manifold Yellow Jacket (CGA 166 LH Adapter) Leak Detection CPS Leak Detector Robinair Leak Detector RTI Leak Detector Techno Tools Leak Detector Yellow Jacket Leak Detector Pumps Haskel Pump for Hose Recovery Recovery, Recycle, Recharge (RRR) Machines CPS RRR Machine Ecotechnics ECK Twin Launch UK RRR System Robinair Service Equipment RTI Mahle RRR Machine Refrigerant Identification Neutronics Refrigerant Identifier SUPPLIER WEBSITES This is a partial list of equipment suppliers. Beissbarth Brain Bee CPS Ecotechnics Errecom Fral Oksys Haskel Hella Nussbaum Launch UK Luvata Mastercool Motorscan KS electronics Neutronics Robinair RTI Snap On SPX Techno Tools Tecnomotor TEXA Waeco WIGAM Yellow Jacket www.beissbarth.com/bbcms/cms.php www.brainbee.it www.cpsproducts.com www.ecotechnics.it www.errecom.it/ENG/ www.fral-arm.com www.haskel.com www.hella-nussbaum.com www.launchtech.co.uk www.luvata.com www.mastercool.com www.motorscan.com www.neutronicsinc.com www.robinair.com www.rtitech.com www.snapon.com www.spx.com/en/ www.techno-tools.com www.tecnomotor.it www.texa.com www.airconservice.eu www.wigam.it www.airconservice.eu © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Table of Contents Hoses and Connections CPS Gauges and Fittings Errecom Hose Mastercool Gauge Manifold Yellow Jacket (CGA 166 LH Adapter) Solstice® yf Refrigerant User Guide CPS Guages and Fittings Table of Contents Part 7 - Page 238 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Errecom Hoses Table of Contents Part 7 - Page 239 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Errecom Hoses Table of Contents Part 7 - Page 240 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Errecom Hoses Table of Contents Part 7 - Page 241 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Errecom Hoses Table of Contents Part 7 - Page 242 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Mastercool Gauge Manifold Table of Contents Part 7 - Page 243 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Mastercool Gauge Manifold Table of Contents Part 7 - Page 244 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Mastercool Gauge Manifold Table of Contents Part 7 - Page 245 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Yellow Jacket (CGA 166 LH Adapter) Table of Contents Part 7 - Page 246 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Yellow Jacket (CGA 166 LH Adapter) Table of Contents Part 7 - Page 247 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Table of Contents Leak Detection CPS Leak Detector Robinair Leak Detector RTI Leak Detector Techno Tools Leak Detector Yellow Jacket Leak Detector Solstice® yf Refrigerant User Guide CPS Leak Detector Table of Contents Part 7 - Page 250 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide CPS Leak Detector Table of Contents Part 7 - Page 251 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Robinair Leak Detector Table of Contents Part 7 - Page 252 © 2014 by Honeywell International Inc. All rights reserved. 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All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Robinair Leak Detector Table of Contents Part 7 - Page 257 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Robinair Leak Detector Table of Contents Doc Number: # Part 7 - Page 258 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Robinair Leak Detector Table of Contents Doc Number: # Part 7 - Page 259 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. 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Table of Contents Recovery, Recycle, Recharge (RRR) Machines CPS RRR Machine Ecotechnics ECK Twin Launch UK RRR System Robinair Service Equipment RTI Mahle RRR Machine Solstice® yf Refrigerant User Guide CPS RRR Machine Table of Contents Part 7 - Page 288 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide CPS RRR Machine Table of Contents Part 7 - Page 289 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Ecotechnics ECK Twin Table of Contents Part 7 - Page 290 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Ecotechnics ECK Twin Table of Contents Part 7 - Page 291 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Ecotechnics ECK Twin Table of Contents Part 7 - Page 292 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Ecotechnics ECK Twin Table of Contents Part 7 - Page 293 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Ecotechnics ECK Twin Table of Contents Part 7 - Page 294 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Launch UK RRR System Table of Contents Part 7 - Page 295 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. Solstice® yf Refrigerant User Guide Launch UK RRR System Table of Contents Part 7 - Page 296 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. www.honeywell-refrigerants.com Solstice® yf Refrigerant User Guide Robinair Service Equipment Table of Contents Part 7 - Page 297 © 2014 by Honeywell International Inc. All rights reserved. No reproduction of these materials is permitted without prior written permission. 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Solstice yf Refrigerant (Americas) | technical guide

User Guide for the Americas

Honeywell International Inc.

References